9 results about "Diisononyl phthalate" patented technology

The application discloses a high-temperature-resistant polyvinyl chloride adhesive tape and a preparation method thereof, and belongs to the technical field of polymer materials and adhesive products. The high-temperature-resistant polyvinyl chloride adhesive tape comprises the following raw materials in parts by weight: synergistically modified polyvinyl chloride, diphenyl phosphine oxide, chlorinated polyethylene, diisononyl phthalate, antimony trioxide, calcium stearate, zinc stearate, an antioxidant and a leveling agent; the synergistically modified polyvinyl chloride is obtained by introducing catechol structures on the surface of polyvinyl chloride through dopamine self-polymerization deposition, forming a dynamic borate ester structure with 3-aminobenzoic acid, and constructing a Si-O-Si network structure through hydrolytic condensation reaction of octa(3-aminopropyl)silsesquioxane and N-(beta-aminoethyl)-gamma-aminopropyl triethoxysilane. The dopamine-borate ester-silicone synergistic network structure is constructed, and the diphenyl phosphine oxide is introduced for function regulation, so that the heat resistance, mechanical properties and dimensional stability of the polyvinyl chloride adhesive tape are significantly improved.

The invention provides a flame-retardant sealant and a preparation method thereof. The flame-retardant sealant comprises the following components in parts by weight: a silane modified polyether polymer, a plasticizer, a filler, fumed silica, a thixotropic agent, a moisture scavenger, a silane coupling agent and a curing agent, the plasticizer is selected from any one or a combination of at least two of diisodecyl phthalate, diisononyl phthalate, a polyether plasticizer and alkyl benzene sulfonate, and the filler comprises modified aluminum hydroxide. According to the flame-retardant sealant and the preparation method thereof, the specific components of the flame-retardant sealant are designed, and the flame-retardant sealant which has better flame retardance and better mechanical property, is relatively low in manufacturing cost and is more beneficial to large-scale commercial production can be prepared through the matching effect of all the components on the premise that a phosphorus flame retardant is not used.

The invention relates to a hybridoma cell strain capable of secreting a diallyl phthalate monoclonal antibody and application of the hybridoma cell strain, and belongs to the technical field of immunodetection. The monoclonal antibody secreted by the hybridoma cell strain has excellent affinity and sensitivity to diallyl phthalate, IC50 of the monoclonal antibody to the diallyl phthalate reaches 500 ng / mL, and the monoclonal antibody secreted by the hybridoma cell strain has excellent affinity and sensitivity to structural analogues of the diallyl phthalate. The invention relates to a method for preparing diisononyl phthalate, which is characterized in that the diisononyl phthalate, such as dimethyl phthalate, diethyl phthalate, dinonyl phthalate, butyl benzyl phthalate, diisobutyl phthalate, di (2-ethylhexyl) phthalate and diisononyl phthalate, are not subjected to cross reaction. Therefore, the monoclonal antibody provided by the invention can be used for preparing an immunodetection product of diallyl phthalate, and an efficient detection method and means are provided for residue detection of diallyl phthalate in food.

The present disclosure provides a ruthenium-containing catalyst and a preparation method and application thereof, and belongs to the technical field of catalysts. The present disclosure uses 3,3'-dibromo-4,4'-diphenylol, 1,3,5-tri(p-vinylphenyl)benzene and a ruthenium salt as main raw materials to perform a polymerization reaction, so as to obtain a ruthenium-containing catalyst with nanoscale pores formed inside; the obtained ruthenium-containing catalyst has good catalytic performance, thermal stability and chemical stability; the ruthenium-containing catalyst is used to catalyze diisononyl phthalate to hydrogenation, so as to prepare diisononyl cyclohexane-1,2-dicarboxylate; the catalytic effect of the ruthenium-containing catalyst is good, and the yield of diisononyl cyclohexane-1,2-dicarboxylate is high.

This invention discloses a high-performance sealant and its preparation method, belonging to the field of sealant technology. The method includes adding 10-20 parts of diisononyl phthalate to 100 parts of hydroxyl-terminated polybutadiene and stirring; adding 60-90 parts of filler and stirring; adding 18-43 parts of composite functional additives and stirring to obtain a premixed base material; adding 15-25 parts of polymethylene polyphenyl polyisocyanate and 4-8 parts of silane coupling agent; adding 0.1-0.3 parts of composite catalyst; and then adding an ultraviolet absorber and an antioxidant, stirring to obtain a catalytically modified mixture; vacuum degassing and curing to obtain a high-performance sealant. The high-performance sealant prepared by this invention improves flexibility and displacement resistance, significantly increases elongation at break, and achieves a displacement capacity level of 20. It can flexibly adapt to slight deformations in building structures caused by temperature fluctuations and foundation settlement, avoiding cracking and detachment, and maintaining good fireproof sealing performance over a long period.

The invention belongs to the field of waterproof coiled materials, and discloses an ultra-low-temperature-resistant PVC waterproof coiled material and a preparation method thereof. The invention discloses a PVC (polyvinyl chloride) composite material, which is prepared from the following raw materials in parts by weight: 100 parts of SG5 type PVC resin, 40 to 60 parts of diisononyl phthalate, 15 to 25 parts of ethylene-vinyl acetate copolymers, 10 to 20 parts of polyolefin elastomers, 3 to 6 parts of calcium-zinc composite stabilizers, 20 to 30 parts of ground calcium carbonate, 1 to 3 parts of stearic acid, 0.5 to 1.5 parts of antioxidants 1010, 0.3 to 0.8 part of ultraviolet light absorbers UV531 and 3 to 8 parts of silane coupling agent modified nano-montmorillonite. 6-15 parts of a composite toughening component; the composite toughening component is formed by compounding a poly (hexamethylene diamine adipate)-polyethylene glycol block copolymer and poly (butylene succinate) according to the weight ratio of (1: 0.8)-(1: 1.5); the technical problems that an existing PVC waterproof coiled material is insufficient in low-temperature toughness, prone to embrittlement in an ultralow-temperature environment, difficult to consider both mechanical properties and low-temperature properties, attenuated in long-term use performance and the like are solved, and the PVC waterproof coiled material is suitable for waterproof coiled materials.

The application belongs to the field of catalysts, and particularly discloses a DINP hydrogenation catalyst based on carbon sphere carriers, a preparation method and application thereof. The nickel-based DINP hydrogenation catalyst based on hollow mesoporous carbon spheres is used for diisononyl phthalate hydrogenation reaction, and the DINP conversion rate can be as high as 99.2%, and the DINCH selectivity can be as high as 99.3%.

The present application relates to a near-infrared highly-reflective PVC material and a preparation method therefor. The near-infrared highly-reflective PVC material comprises a base fabric layer and PVC coatings coating both sides of the base fabric layer. Raw materials for preparing the PVC coatings comprise in parts by weight: 95 parts of PVC paste resin, 45-65 parts of diisononyl phthalate, 1-2 parts of a stabilizer, 25-40 parts of an IR pigment, 3-4 parts of a flame retardant, and 1-2 parts of other auxiliaries, the IR pigment being obtained by modifying BASF Sicopal Black L0095 with dioctyl phthalate and EO / PO block polyether. The preparation method comprises preparation of the base fabric layer, material coating, and curing. In the present application, the BASF Sicopal Black L0095 pigment is modified by dioctyl phthalate and EO / PO block polyether (e.g., FTRT®500L1), thereby solving the problem of incompatibility between the pigment and a plasticizer. The optimized formula design ensures that the reflectivity of the material can stably reach or exceed 40%, which is particularly important to application scenarios (such as building film structures, tent houses, and military materials) in which efficient thermal insulation and cooling performance is required.

The invention provides a production device and a production method of diisononyl phthalate. The diisononyl phthalate production device comprises a feeding system, at least one esterification reaction kettle and a dealcoholization tower which are sequentially connected, the operation temperature of the esterification reaction kettle is 200-250 DEG C; and / or the operation pressure of the esterification reaction kettle is 0-0.05 MPaG; and / or the operation pressure of the dealcoholization tower is 6-12 KPaA. According to the invention, after the high-temperature liquid in the esterification reaction kettle enters the dealcoholization tower, the isononyl alcohol with a lower boiling point and water are quickly vaporized and then transferred into a subsequent separation system, so that the dealcoholization and dehydration purposes are realized under the condition that an external heat source is not arranged.