Release agent, manufacturing method thereof and rotational moulding technology using release agent
A manufacturing method and release agent technology, applied in the direction of coating, etc., can solve problems such as difficult to remove oligomer agglomeration, produce fluorocarbons, and damage the environment, so as to reduce mold scale production, improve compactness, and shorten production The effect of cycle length
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Embodiment A1
[0050] A release agent, the preparation steps of the release agent are as follows:
[0051] S1: under normal temperature and pressure, add 20 parts of absolute ethanol into the reactor by mass fraction;
[0052] S2: add 50 parts of ethyl silicone oil and 20 parts of wax components into the reaction kettle for heating and stirring according to parts by mass, the heating temperature is 66°C, fully dissolve and then cool to normal temperature;
[0053] S3: add 20 parts of gas phase silica and 7 parts of sodium dodecyl benzene sulfonate in the reaction kettle by mass fraction and stop stirring after stirring.
Embodiment B1
[0076] A release agent, the preparation steps of the release agent are as follows:
[0077] S1: under normal temperature and pressure, add 20 parts of absolute ethanol into the reactor by mass fraction;
[0078] S2: add 50 parts of metered ethyl silicone oil and 20 parts of wax components into the reactor for heating and stirring by mass parts, and the heating temperature is 66 ° C, and it is fully dissolved and cooled to normal temperature;
[0079] S3: add 20 parts of fumed silica, 7 parts of sodium dodecylbenzene sulfonate and 5 parts of aluminum ethoxide into the reaction kettle by mass fraction and stop stirring after stirring.
[0080] The release agent obtained in Example A1 and Example B1 was subjected to an anti-dropping durability test.
[0081] Anti-shedding durability test: Use different sample release agents to perform rotational molding of the same product and the same mold. After each production cycle is completed, check the coverage of the release agent on the...
Embodiment C1
[0087] The steps are the same as in Example A1, and the proportions of each raw material in parts by mass are: 50 parts of ethyl silicone oil, 22 parts of fumed silica, 7 parts of sodium dodecyl benzene sulfonate, 20 parts of anhydrous ethanol, wax 20 components.
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