A kind of stevioside saponin decolorization resin and its preparation method and application

A decolorizing resin and stevioside technology, which is applied in the preparation of sugar derivatives, chemical instruments and methods, sugar derivatives, etc., can solve the problems of incomplete decolorization of stevioside saponin decolorization resin, low resin decolorization strength, poor anti-pollution ability, etc. , to achieve complete decolorization, low sugar loss and good resin strength

Active Publication Date: 2021-12-31
AMICOGEN CHINA BIOPHARM CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] In order to solve the technical problems of incomplete decolorization of the stevioside saponin decolorization resin, short resin life, poor anti-pollution ability, and low resin decolorization strength, the present invention provides a stevioside saponin decolorization resin and its preparation method and its use in stevioside saponin decolorization. Applications

Method used

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  • A kind of stevioside saponin decolorization resin and its preparation method and application
  • A kind of stevioside saponin decolorization resin and its preparation method and application
  • A kind of stevioside saponin decolorization resin and its preparation method and application

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Embodiment 1

[0035] A preparation method of steviol saponin decolorizing resin, characterized in that, comprising the synthesis of resin skeleton and the functionalization of resin, and the steps are as follows:

[0036] a) Preparation of raw materials: proportion by mass as follows

[0037] water box

[0038] 100 parts deionized water

[0039] 0.5 servings of PVA

[0040] NaCl 1 part

[0041] oil phase

[0042] 1 part of divinylbenzene

[0043] 22 parts vinyl acetate

[0044] Butyl acetate, n-heptane, 6 parts in total

[0045] b) Suspension polymerization: the above water phase and oil phase were suspended and polymerized at 60°C for 24h to obtain white balls;

[0046] c) Hydrolyze the above white balls in an aqueous sodium hydroxide solution to obtain an intermediate ball; the mass fraction of the aqueous sodium hydroxide solution is 10%, the hydrolysis temperature is 50°C, and the hydrolysis time is 24h.

[0047] d) After the above-mentioned intermediate ball is fully swollen in...

Embodiment 2

[0050] A preparation method of steviol saponin decolorizing resin, characterized in that, comprising the synthesis of resin skeleton and the functionalization of resin, and the steps are as follows:

[0051] a) Preparation of raw materials: proportion by mass as follows

[0052] water box

[0053] 100 parts deionized water

[0054] 1 serving of PVA

[0055] 2 parts NaCl

[0056] oil phase

[0057] 2 parts of divinylbenzene

[0058] 23 parts vinyl acetate

[0059] 7 parts n-heptane

[0060] b) Suspension polymerization: the above water phase and oil phase were suspended and polymerized at 80°C for 18h to obtain white balls;

[0061] c) Hydrolyze the above white balls in an aqueous sodium hydroxide solution to obtain an intermediate ball; the mass fraction of the aqueous sodium hydroxide solution is 20%, the hydrolysis temperature is 70°C, and the hydrolysis time is 16h.

[0062] d) After the above-mentioned intermediate ball is fully swollen in dioxane, add 5 times the ...

Embodiment 3

[0065] A preparation method of steviol saponin decolorizing resin, characterized in that, comprising the synthesis of resin skeleton and the functionalization of resin, and the steps are as follows:

[0066] a) Preparation of raw materials: proportion by mass as follows

[0067] water box

[0068] 100 parts deionized water

[0069] 4 servings of gelatin

[0070] oil phase

[0071] 3 parts of divinylbenzene

[0072] 24 parts vinyl propionate

[0073] Methyl isobutyl methanol 6 parts

[0074] b) Suspension polymerization: suspend the above water phase and oil phase at 100°C for 10 hours to prepare white balls;

[0075] c) The above-mentioned white balls were hydrolyzed in sodium hydroxide aqueous solution to obtain intermediate balls; the mass fraction of sodium hydroxide aqueous solution was 30%, the hydrolysis temperature was 100°C, and the hydrolysis time was 8 hours.

[0076] d) After the above-mentioned intermediate ball is fully swollen in methanol, add 10 times of th...

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PUM

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Abstract

The invention provides a stevioside saponin decolorizing resin and a preparation method thereof, including suspension polymerization, hydrolysis to prepare intermediate spheres, epoxy chlorohydrin to prepare epoxy spheres, amination, and its application in stevioside solution decolorization ;Introduce hydroxyl groups on the strong base group as the main decolorizing functional group to achieve better contact between the stevioside liquid and the resin surface, to ensure that the decolorizing group can react with the pigment more easily and remove it, so that the resin can decolorize completely , High yield, low sugar loss and good resin strength.

Description

technical field [0001] The invention relates to the application field of resin in plant extraction, in particular to a steviol saponin decolorizing resin used in the refining process of stevia, and a preparation method and application thereof. Background technique [0002] The decolorization step involved in the refining process of stevia, the earliest process is to use activated carbon decolorization, and then gradually evolved into the resin method. At present, the application of resin in stevia decolorization has problems such as large sugar consumption, poor anti-pollution performance of resin, incomplete decolorization and poor resin strength. [0003] In the prior art, the application situation of the stevia decolorizing resin described in the patent CN102020745A feedback that the resin has good decolorization performance but still has the problems of general resin anti-pollution performance, short service life, and the problem of high cost of the resin and large pollu...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C08F218/08C08F212/36C08F8/12C08F8/00C08F8/32C08F218/10C07H15/256C07H1/06
CPCC08F8/32C08F8/00C08F8/12C08F218/08C08F218/10C07H15/256C07H1/06C08F212/36
Inventor 刘庆文蒋筱玮罗文军李建国杨申永
Owner AMICOGEN CHINA BIOPHARM CO LTD
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