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A kind of high-strength ceramic product and its preparation process

A technology of ceramic products and preparation process, applied in the field of ceramics, can solve problems such as single performance, and achieve the effects of uniform slurry, improved strength and uniform dispersion

Active Publication Date: 2021-11-23
FUJIAN WILL CERAMIC CO LTD +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the performance of ceramic materials composed of a single zirconia is relatively single, which cannot be used in many fields. In order to effectively improve its performance, it is necessary to optimize its ceramic composition and improve the comprehensive performance of ceramic materials. a hotspot in the field

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0024] Embodiment one: a kind of preparation technology of high-strength ceramic product, concrete steps are:

[0025] S1: Preparation of fiber ceramic balls:

[0026] S11: Fiber precursor: in parts by weight, put 5 parts by weight of silicate fiber, 3 parts by weight of aramid fiber, 4 parts by weight of copper fiber and 4 parts by weight of glass fiber into a ball mill for grinding for 1 hour, then Adding 50 parts by weight of paraffin to obtain a fiber precursor;

[0027] S12: Fiber ceramic powder balls: Put 20 parts of fiber precursor, 40 parts of ceramic powder and 5 parts of graphite particles into a ball mill for 5 hours by weight, mix the three kinds of powders, and then add 15-20 parts After sulphite pulp waste liquid is granulated, the particle size of the obtained fiber ceramic powder balls is 30~50mm;

[0028] S13: Pre-sintering: Send the fiber ceramic powder balls obtained by granulation into a sintering furnace, pre-sinter at 360°C, keep for 2 hours, and anneal...

Embodiment 2

[0033] Embodiment two: a kind of preparation technology of high-strength ceramic product, concrete steps are:

[0034] S1: Preparation of fiber ceramic balls:

[0035] S11: Fiber precursor: in parts by weight, put 5 parts by weight of silicate fiber, 3 parts by weight of aramid fiber, 4 parts by weight of copper fiber and 4 parts by weight of glass fiber into a ball mill for grinding for 1 hour, then Add the paraffin wax that is 55 parts by weight, obtain fiber precursor;

[0036] S12: Fiber ceramic powder balls: put 25 parts of fiber precursor, 50 parts of ceramic powder and 8 parts of graphite particles into a ball mill and grind for 5 hours according to parts by weight. After mixing the three kinds of powders, add 20 parts of sulfurous acid After the pulp waste liquid is granulated, the particle size of the fiber ceramic powder obtained by granulation is 30~50mm;

[0037] S13: Pre-sintering: Send the fiber ceramic powder balls obtained by granulation into a sintering furn...

Embodiment 3

[0042] Embodiment three: a kind of preparation technology of high-strength ceramic product, concrete steps are:

[0043] S1: Preparation of fiber ceramic balls:

[0044] S11: Fiber precursor: in parts by weight, put 5 parts by weight of silicate fiber, 3 parts by weight of aramid fiber, 4 parts by weight of copper fiber and 4 parts by weight of glass fiber into a ball mill for grinding for 1 hour, then Adding the paraffin wax that is 52 parts by weight, obtains the fiber precursor;

[0045] S12: Fiber ceramic powder balls: Put 23 parts of fiber precursor, 45 parts of ceramic powder and 7 parts of graphite particles into a ball mill and grind for 5 hours according to parts by weight. After mixing the three kinds of powders, add 18 parts of sulfurous acid After the pulp waste liquid is granulated, the particle size of the fiber ceramic powder obtained by granulation is 30~50mm;

[0046]S13: Pre-sintering: send the fiber ceramic powder balls obtained by granulation into a sinte...

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Abstract

The invention provides a high-strength ceramic product and a preparation process thereof. The specific steps of the preparation process are: S1: preparing fiber ceramic balls; S2: mixing materials: by weight fraction, 40-50 parts of ceramic powder, 5 parts of magnetite ‑10 parts, 6‑12 parts of chromite and 3‑7 parts of phenolic resin, put into a ball mill and grind for 1 hour, then add 30‑40 parts of fiber ceramic balls in step 1, and continue ball milling for 9‑10 hours to make ceramics Blank; S3: mold loading: fill the ceramic blank in step S2 in the mold, after extrusion molding, demoulding into a green body; S4: sintering: the made green body is first dried in a drying room, and then in a sintering furnace Sintered to obtain ceramic products. In the preparation process of the high-strength ceramics of the present invention, fiber ceramic balls are obtained by pre-sintering and decomposing, and then synthetic ceramics are obtained through mixing, molding and sintering, and the dispersion is uniform, and the strength and toughness are also improved.

Description

technical field [0001] The invention relates to the technical field of ceramics, in particular to a high-strength ceramic product and a preparation process thereof. Background technique [0002] With the development of science and technology, various new materials have sprung up, and ceramic materials are one of them. Ceramic materials are a kind of inorganic non-metallic materials made of natural or synthetic compounds through molding or high-temperature calcination. There are many types of ceramics and different uses. With the development of modern science and technology, many new ceramic varieties have emerged in the past century, and structural ceramics are one of them. In terms of structural ceramics, zirconia ceramics are widely used in the field of structural ceramics due to their high toughness, high flexural strength, high wear resistance, excellent heat insulation performance, and thermal expansion coefficient close to steel. Mainly include: Y-TZP grinding balls,...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C04B35/80C04B35/14C04B35/622C04B35/626
CPCC04B35/14C04B35/622C04B35/62605C04B2235/3241C04B2235/3272C04B2235/5232C04B2235/5216C04B2235/96C04B2235/602
Inventor 危连进
Owner FUJIAN WILL CERAMIC CO LTD
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