Gold/oxide catalyst and application in preparing DHA through catalytic oxidation of glycerol
A technology of oxides and catalysts, applied in gold/oxide catalysts and in the application field of catalytic oxidation of glycerol to prepare DHA, can solve the problems of no research on gold catalysts, achieve good industrial prospects, and the preparation method is simple and easy to operate, and the reaction conditions mild effect
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[0027] Example 1
[0028] The gold / oxide catalyst of this embodiment is prepared by the following method:
[0029] (1) Take 6 g of lilac leaf powder in 100 mL of water, stir at 30°C for 6 hours, then centrifuge and filter to obtain a water extract, which is freeze-dried to obtain a lilac leaf extract;
[0030] (2) Put 12.08g Cu(NO 3 ) 2 ·3H 2 O is dissolved in 200mL deionized water, and 1M Na is added dropwise at the same time 2 CO 3 Adjust pH=10, then put the mixed solution at room temperature and stir for 12h; the obtained mixed solution was filtered and washed to neutrality, and the filter cake was placed in a vacuum oven at 60℃ for 24h. 2 In the atmosphere, the temperature is increased to 350°C at a rate of 2°C / min and fired for 4 hours to obtain the CuO carrier;
[0031] (3) Take 0.99g of CuO carrier in 50mL of deionized water, then add 1.04mL of 48.56mM chloroauric acid solution, stir at 30℃ for 4h, continue to add 100mg of lilac leaf extract, stir for 4h; extract the resulting m...
Example Embodiment
[0035] Example 2
[0036] The gold / oxide catalyst of this embodiment is prepared by the following method:
[0037] (1) Take 6 g of lilac leaf powder in 100 mL of water, stir at 30°C for 6 hours, then centrifuge and filter to obtain a water extract, which is freeze-dried to obtain a lilac leaf extract;
[0038] (2) Put 12.08g Cu(NO 3 ) 2 ·3H 2 O is dissolved in 200mL deionized water, and 1M Na is added dropwise at the same time 2 CO 3 Adjust pH=10, then put the mixed solution at room temperature and stir for 12h; the obtained mixed solution was filtered and washed to neutrality, and the filter cake was placed in a vacuum oven at 60℃ for 24h. 2 In the atmosphere, the temperature is increased to 350°C at a rate of 2°C / min and fired for 4 hours to obtain the CuO carrier;
[0039] (3) Take 0.99g of CuO carrier in 50mL of deionized water, then add 1.04mL of 48.56mM chloroauric acid solution, stir at 30℃ for 4h, continue to add 200mg of lilac leaf extract, stir for 4h; extract the resulting m...
Example Embodiment
[0042] Example 3
[0043] The gold / oxide catalyst of this embodiment is prepared by the following method:
[0044] (1) Take 6g of green peach leaf powder in 100 mL of water, stir at 30°C for 6 hours, then centrifuge and filter to obtain a water extract, which is freeze-dried to obtain a green peach leaf extract;
[0045] (2) Put 12.08g Cu(NO 3 ) 2 ·3H 2 O is dissolved in 200mL deionized water, and 1M Na is added dropwise at the same time 2 CO 3 Adjust pH=10, then put the mixed solution at room temperature and stir for 12h; the obtained mixed solution was filtered and washed to neutrality, and the filter cake was placed in a vacuum oven at 60℃ for 24h. 2 In the atmosphere, the temperature is increased to 350°C at a rate of 2°C / min and fired for 4 hours to obtain the CuO carrier;
[0046] (3) Take 0.99g of CuO carrier in 50mL of deionized water, then add 1.04mL of 48.56mM chloroauric acid solution, stir for 4h at 30℃, continue to add 100mg of Peach leaf extract, stir for 4h; suction filt...
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