Method and primer pair for detecting CAG trinucleotide repetition sequence of HTT gene
A nucleotide sequence and trinucleotide technology, applied to a method for detecting the HTT gene CAG trinucleotide repeat sequence and the field of primer pairs, can solve the problem of difficulty in obtaining sequencing maps and high GC content of HTT gene CAG repeat fragments , clinical diagnosis of Huntington's disease and other problems
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Embodiment 1
[0050] Design and synthesize primer sets, including the following steps:
[0051] Step 1.1: According to the HTT gene CAG trinucleotide repeat sequence and related literature, design specific amplification primers, and the forward primer is labeled with the fluorescent group FAM.
[0052] FAM is carboxyfluorescein, as a blue fluorescent labeling dye, synthesized by Huada Genomics Co., Ltd.
[0053] The designed primer sequences are:
[0054] HTT F: 5'-FAM-TGAAGGCCTTCGAGTCCCTCAAGTCCTTC-3'
[0055] HTT R: 5'-CGGCTGAGGAAGCTGAGGAG-3'
[0056] Wherein, F refers to the forward primer, and R refers to the reverse primer.
[0057] Step 1.2: Synthesize the primers designed in 1.1.
Embodiment 2
[0059] Genomic DNA is extracted from the sample to be tested, comprising the following steps:
[0060] Step 2.1: Reagent preparation. Including preparation of absolute ethanol and kit.
[0061] The prepared kit is Blood Genomic DNA Extraction Kit (Tiangen): before use, add absolute ethanol to the rinse solutions PW and GD, and add the volume according to the label on the bottle.
[0062] Step 2.2: Genomic DNA extraction from blood. Specifically, the following steps (1) to (11) may be included:
[0063] (1) Add 200 μL of blood to a 1.5 mL centrifuge tube.
[0064] (2) Add 20 μL Proteinase K solution and mix well.
[0065] (3) Add 200 μL buffer GB, mix thoroughly by inversion, bathe in 70°C water for 10 minutes (the solution should become clear), and centrifuge briefly.
[0066] (4) Add 200 μL of absolute ethanol, shake and mix well for 15 seconds (flocculent precipitation may appear at this time), and briefly centrifuge.
[0067] (5) Add the solution and flocculent precip...
Embodiment 3
[0082] The PCR product amplification method may comprise the following steps:
[0083] Step 3.1: Use the genomic DNA obtained in step 2.2 and 15 CAP samples from 2016-2018 as DNA templates, and use the primers synthesized in step 1.2 to configure a PCR reaction system. The specific composition of this reaction system is shown in Table 2 below.
[0084] Table 2
[0085] Reagent components volume 2×KOD FX Buffer 25 μL 2.0mM dNTPs 10μL HTT-F (10uM) 1.5μL HTT-R (10uM) 1.5μL KOD FX enzyme 1μL dna 1μL DI water 11μL
[0086] The CAP (COLLEGE OF AMERICAN PATHOLOGISTS, College of American Pathologists) laboratory was established in 1946 and is widely recognized as a leader in laboratory quality assurance. The implementation method of CAP external quality assessment is that the organizer provides a set of samples to be tested to the participating laboratories, and the participating laboratories complete the testing of th...
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