Styrene volatilization inhibitor based on cholesterol derivative, and preparation method thereof

A technology of derivatives and cholesterol, which is applied in the field of styrene volatilization inhibitor and its preparation, can solve the problems of increasing the cost and high price of unsaturated resin, and achieve excellent styrene volatilization inhibition effect, guarantee of health, and fast drying Effect

Active Publication Date: 2019-09-03
CHANGZHOU HUAKE POLYMERS
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

At present, BYK-S 740, BYK-S 750, BYK-S 760 and products from other companies are more popular in the market, but without exception, the prices are quite expensive, and the use of these styrene volatilization inhibitors will greatly increase the Cost of Saturated Resin

Method used

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  • Styrene volatilization inhibitor based on cholesterol derivative, and preparation method thereof
  • Styrene volatilization inhibitor based on cholesterol derivative, and preparation method thereof
  • Styrene volatilization inhibitor based on cholesterol derivative, and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0022] The composition of the styrene volatilization inhibitor of this embodiment is shown in the following table:

[0023] Specific components Weight / g Cholesterol derivative C166 Xylene30 54# Paraffin4

[0024]

[0025] (1) Add the cholesterol derivative (chemical structural formula as shown in C1) and xylene into a reactor equipped with a heating device and a stirring device, turn on the stirring, and stir evenly at an ambient temperature of 25°C;

[0026] (2) Add the crushed 54# paraffin to the reaction kettle and continue to stir evenly at 45°C;

[0027] (3) Filter the above materials with a 200-mesh filter bag to obtain the styrene volatilization inhibitor.

Embodiment 2

[0029] The composition of the styrene volatilization inhibitor of this embodiment is shown in the following table:

[0030] Specific components Weight / g Cholesterol derivative C270 Styrene24 52# Paraffin6

[0031]

[0032] (1) Add the cholesterol derivative (chemical structural formula as shown in C2) and styrene into a reactor with a heating device and a stirring device, turn on the stirring, and stir evenly at an ambient temperature of 30°C;

[0033] (2) Add the crushed 52# paraffin to the reaction kettle and continue to stir evenly at 50°C;

[0034] (3) Filter the above materials with a 400-mesh filter bag to obtain the styrene volatilization inhibitor.

Embodiment 3

[0036] The composition of the styrene volatilization inhibitor of this embodiment is shown in the following table:

[0037] Specific components Weight / g Cholesterol derivative C350 No. 120 solvent oil20 Diallyl phthalate30 paraffin0

[0038]

[0039] (1) Add cholesterol derivatives (chemical structure as shown in C3), solvent oil No. 120 and diallyl phthalate into a reactor with a heating device and a stirring device, turn on the stirring, and set it at 20°C Stir evenly at the ambient temperature;

[0040] (2) Filter the above materials with a 100 mesh filter bag to obtain the styrene volatilization inhibitor.

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Abstract

The invention discloses a styrene volatilization inhibitor based on a cholesterol derivative, and a preparation method thereof, wherein the styrene volatilization inhibitor comprises, by weight, 20-70parts of a cholesterol derivative, 0-5 parts of paraffin, and 30-80 parts of a diluent. The preparation method comprises: uniformly mixing a cholesterol derivative, paraffin and a diluent, and filtering. According to the present invention, the styrene volatilization inhibitor constructed based on the cholesterol derivative is added to a unsaturated resin, and the styrene volatilization inhibitorcan float on the surface and form a film during the resin standing and curing, such that the volatilization rate of styrene can be significantly reduced while the interlayer adhesion of the unsaturated resin product cannot be affected, the good leveling property can be achieved, the appearance of the product cannot be affected, and the weather resistance is good.

Description

Technical field [0001] The invention relates to the field of chemical additives, in particular to a styrene volatilization inhibitor based on cholesterol derivatives and a preparation method thereof. Background technique [0002] Unsaturated polyester resin has good comprehensive physical properties, convenient processing, and low cost, so it is widely used in rail transit, wind power energy, construction and home decoration, automobile interior and exterior decoration, shipbuilding, coatings and other national economic fields. Unsaturated polyester resin contains 25-50% styrene, and styrene is volatile, which is easy for customers to lose materials and cause waste. More importantly, styrene has a pungent odor and is a potential carcinogen, which will cause a large smell in the production workshop, serious environmental pollution, and seriously endanger the physical and mental health of workers. For this reason, downstream customers have gradually increased their demand for low ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C08L67/06C08L91/06C08K5/101C08K5/01C08K5/527C08L91/00C08K5/06C08K5/12C08L101/00C08K5/18C08L63/10C08K5/109C08K5/103
CPCC08L63/10C08L67/06C08L101/00C08L2205/025C08L2205/03C08L91/06C08K5/101C08K5/01C08K5/527C08L91/00C08K5/06C08K5/12C08K5/18C08K5/109C08K5/103
Inventor 周锋蒋红娟钱永嘉居卫赵银
Owner CHANGZHOU HUAKE POLYMERS
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