Coloring composition, color filter substrate using same, and display device
A technology for coloring compositions and color filter substrates, which is applied in the directions of photosensitive materials, instruments, filters, etc. used in optomechanical equipment, can solve the problem of dimming the brightness of liquid crystal display devices, the reduction of light transmittance of green pixels, and the loss of light. Reduce the transmittance and other problems, to achieve the effect of suppressing the decrease in light transmittance, high light transmittance, and high color purity
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[0121] The following examples are given to illustrate the present invention, but the present invention is not limited to these examples. First, evaluation methods in Examples and Comparative Examples will be described.
[0122]
[0123] The coloring composition obtained by Examples 1-13 and Comparative Examples 1-8 was apply|coated on the glass substrate, and it heat-dried at 90 degreeC for 10 minutes after that. The resulting coating film of the colored composition was subjected to i-rays at 200 mJ / cm through a negative-type photomask. 2 After exposure, it develops with 23 degreeC 0.3 mass % tetramethylammonium hydroxide aqueous solution, and forms a desired pattern. Next, heat treatment was performed at 230° C. for 30 minutes to obtain a film having a film thickness of 1.7 μm. However, only Example 13 had a film thickness of 2.5 μm. About this film, the chromaticity x, y, and light transmittance Y were measured with C light source using the spectrophotometer LCF-100MA m...
manufacture example 1
[0129] Production Example 1 (Preparation of Dispersion Liquid (A1))
[0130] C.I. Pigment Yellow 185 ("Paliotol" (registered trademark) Yellow D1155 manufactured by BASF) 150 g, "BYK" (registered trademark) LPN6919 (manufactured by Bic Chemical Co., polymer dispersant solution (60% by mass propylene glycol monomethyl ether solution)) 125 g, 100 g of "Sychroma" (registered trademark) ACA250 (manufactured by Daicel Chemical Co., Ltd., 45 mass % dipropylene glycol monomethyl ether solution) and 625 g of propylene glycol monomethyl ether (PMA) were mixed to prepare a slurry. Connect the beaker containing the slurry to a dyno-mill, use zirconia beads with a diameter of 0.5mm as the medium, and perform dispersion treatment at a peripheral speed of 14m / s for 8 hours to prepare C.I. Pigment Yellow 185 Dispersion (A1).
manufacture example 2
[0131] Production Example 2 (Preparation of Dispersion Liquid (A2))
[0132] In place of C.I. Pigment Yellow 185, except that 150 g of C.I. Pigment Green 58 ("FASTGEN" (registered trademark) Green A110 manufactured by DIC Co., Ltd.) was used, the C.I. Pigment Green 58 dispersion was prepared in the same manner as Production Example 1 (A2).
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