Slick water fracturing fluid for medium-high temperature compact reservoir and preparation method thereof

A tight reservoir, water fracturing technology, applied in the direction of chemical instruments and methods, drilling compositions, etc., can solve problems such as poor temperature resistance and shear resistance, high construction risk, and poor sand-carrying performance. Achieve the effect of good temperature resistance and shear resistance, obvious drag reduction effect, and not easy to curl and deform

Inactive Publication Date: 2019-10-01
PETROCHINA CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, guar gum and its modified products have the inherent disadvantages of easy corruption of vegetable gum, and the composition of the fracturing fluid system is complex. The formation of jelly depends on chemical cross-linking. It is difficult and costly to treat the flowback fluid after gel breaking, and it is feasible to reuse it. poor sex
Since the above defects of plant gum fracturing fluids such as guar gum can neither alleviate the pressure of environmental protection nor meet the above-mentioned on-site construction requirements, polymer fracturing fluids are widely used to solve the above problems
[0004] At present, there are many kinds of acrylamide polymer thickeners, among which the thickeners of guar gum and its derivatives are the most widely used, but there are common problems such as incomplete gel breaking, easy gel return, and high residue content of gel breaking liquid. The problem is that it is easy to cause blockage damage, resulting in a decrease in matrix permeability and fracture conductivity, thereby affecting the fracturing effect. At the same time, the friction of vegetable gum fracturing fluid pipelines is high, resulting in higher wellhead pressure at the same displacement, resulting in More hydraulic power loss and higher construction risk
Synthetic polymer thickeners mainly include polyacrylamide, sodium polyacrylate, polyacrylate and polyvinyl alcohol, etc., which generally have the characteristics of strong thickening ability, good gel breaking performance, and less residue, but the cost is generally high. Use the site to promote the application
At the same time, due to the high temperature of medium-high temperature reservoirs, the polymer fracturing fluid has poor temperature and shear resistance and sand-carrying performance under high-temperature conditions, which cannot meet the construction needs of high-sand concentration stages on site.

Method used

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  • Slick water fracturing fluid for medium-high temperature compact reservoir and preparation method thereof
  • Slick water fracturing fluid for medium-high temperature compact reservoir and preparation method thereof
  • Slick water fracturing fluid for medium-high temperature compact reservoir and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0036] A kind of slick water fracturing fluid for medium-high temperature tight reservoirs, composed of the following components by weight percentage:

[0037]

[0038] In actual use, 50m at the construction site 3 The container is filled with dosing water, and then the thickener is slowly added in proportion to the continuous circulation of the pump, and then the clay stabilizer, temperature-resistant regulator, and gel-breaking degradation agent are added in sequence according to the formula ratio. Continue for 20 minutes to ensure that the liquid is fully mixed to form a uniform solution, and then add structure stabilizers and strength maintenance agents in proportion to form a slippery water fracturing fluid after full circulation.

[0039] The invention is mainly composed of a polymer thickener, a clay stabilizer, a structure stabilizer, a regulator, a gel breaker, etc., and has the characteristics of low viscosity, low friction, low cost, easy backflow, easy recovery,...

Embodiment 2

[0041] A slickwater fracturing fluid for medium-high temperature tight reservoirs, the difference from Example 1 is that the thickener is an acrylamide polymer.

[0042]Preferably, the acrylamide polymer is obtained by the following method: 15% to 30% of acrylamide, 3% to 8% of acrylic acid, 10% to 17% of 2-acrylamide-2- Methylpropanesulfonic acid, 1%-8% sodium polyacrylate, 1%-1.7% hydrogenated polyisoprene, 2%-5% sodium dodecylbenzenesulfonate emulsifier are dissolved in the remaining weight Put it into the purification tank after dissolving in the water of the ratio; pass high-purity nitrogen with a purity of not less than 98%, and control the flow rate of nitrogen at 1-3m 3 Carry out countercurrent nitrogen filling and deoxygenation in 15 minutes, and transfer to the adiabatic polymerizer after 15 minutes; under the action of nitrogen filling, add potassium persulfate-sodium sulfite initiator with a mass ratio of 1% to 1.5%, monitor through a thermometer, and wait for the ...

Embodiment 3

[0045] A slick water fracturing fluid for medium-high temperature tight reservoirs. The difference from Example 1 is that the clay stabilizer is a cationic small molecule multi-charged quaternary ammonium salt with a molecular weight of 10,000-20,000 and a cationic degree of 25-30%: trimethylhydroxypropyl quaternary ammonium chloride, trimethyl hydroxypropyl ammonium chloride, trimethyl tertiary amine, dimethylamine and its hydrochloride react with epichlorohydrin, butane, cyclopentane One or any two of the hydroxypropyl quaternary ammonium bromide products are mixed at a ratio of 1:1-1.5.

[0046] In actual use, the addition of a viscosity stabilizer keeps the fracturing fluid system of a clay stabilizer with a small relative molecular weight and a small molecular size distribution, which can prevent the clay stabilizer from clogging the micropore throats of tight reservoirs and reduce the penetration of low-permeability oil layers. rate damage; the main agent in the clay sta...

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PUM

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Abstract

The invention belongs to the technical field of oil field stimulation, and particularly relates to a slick water fracturing fluid for medium-high temperature compact reservoirs and a preparation method thereof. The slick water fracturing fluid comprises the following components in percentage by weight: 0.30 to 0.45 percent of a thickening agent, 0.03 to 0.05 percent of a clay stabilizer, 0.20 to 0.50 percent of a structural stabilizer, 0.01 to 0.05 percent of a strength maintaining agent, 0.04 to 0.10 percent of a temperature resistant regulator, 0.05 to 0.10 percent of a gel breaker degradingagent and the balance of water. The slick water fracturing fluid has fast dissolution. In 30 seconds, 80% of the final viscosity increase can be achieved, the drag reduction rate can reach more than80%, the core damage rate is less than 10%, well temperature resistance and shear resistance can be satisfied under the medium and high temperature conditions of 90 deg c to 180 deg c, the sand carrying concentration can meet the construction requirements of more than 750 kg / m<3>, the gel breaking is complete, the drainage rate can reach more than 40%, and after simple sand settling treatment, theslick water fracturing fluid can be reused for more than 20 times to maintain more than 90% of the original performance.

Description

technical field [0001] The invention belongs to the technical field of oilfield stimulation, in particular to a slickwater fracturing fluid for medium-high temperature tight reservoirs and a preparation method thereof. Background technique [0002] Fracturing, as the main stimulation measure of oil and gas reservoirs, has been developed rapidly and widely used. Fracturing is the use of pressure to open formations to form fractures and support them with proppant to reduce fluid flow resistance and increase production and injection measures. The purpose of fracturing is to form fractures with conductivity in the formation. The fracturing fluid used determines the fracturing effect to a large extent. At the same time, there are certain requirements for the viscosity of the fracturing fluid so that it can Fluids known as low viscosity flow back easily to avoid damage to hydrocarbon layers in the formation. [0003] The most commonly used fracturing fluids at home and abroad ar...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C09K8/68C09K8/88
CPCC09K8/68C09K8/882C09K2208/26C09K2208/28
Inventor 范华波薛小佳赵振峰陆红军李志忠李楷吴江刘锦郭钢周晓群
Owner PETROCHINA CO LTD
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