A kind of double-layer biomass composite membrane material
A technology of biomass and composite membranes, which is applied in the field of preparation of biomass membrane materials, can solve problems such as insufficient functionality and poor mechanical properties, and achieve the effects of optimizing mechanical properties, increasing barrier properties, and facilitating barriers
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[0050] The preparation technology of described double-layer biomass composite membrane material is:
[0051] (1) Preparation of the bottom chitosan-based blown film layer: put all the raw materials into a high-speed blender and stir for 40min at a speed of 400rpm, and then blow them into a biaxially stretched extrusion blow molding machine to form a film; The conditions for extrusion blow molding are: extrusion section temperature 170°C, longitudinal stretching temperature 80°C, stretching ratio 2.4, transverse stretching temperature 55°C, stretching ratio 1.8, heat treatment temperature 70°C;
[0052] (2) Preparation of surface cellulose-based casting film layer: using deionized water as a solvent, cellulose acetate, carboxymethyl chitosan, four-armed polyethylene glycol propionaldehyde, and sodium alginate were sequentially dropped into deionized water , high-speed stirring until uniform dispersion, the mass concentration of the dispersion is 6.5%, the dispersion is cast on ...
specific Embodiment 2
[0063]A double-layer biomass composite film material, comprising a bottom chitosan-based blown film layer and a surface cellulose-based cast film layer;
[0064] Wherein, chitosan-based film layer comprises material and corresponding mass fraction as follows:
[0065] Chitosan 42 parts
[0066] Carboxymethyl chitosan 16 parts
[0067] Nano plant fiber silk 0.8 parts
[0068] 18 parts gelatin
[0069] Poly(beta hydroxybutyrate-co-beta hydroxyvalerate) 18 parts
[0070] Nano-hydroxyapatite 1.5 parts
[0071] Wherein, the cellulose-based cast film layer includes substances and corresponding parts by mass as follows:
[0072] 30 parts cellulose acetate
[0073] Carboxymethyl chitosan 12 parts
[0074] Four-arm polyethylene glycol propionaldehyde 2.2 parts
[0075] Sodium alginate 6.5 parts
[0076] It is also characterized in that: the bottom chitosan-based blown film layer is formed into a film by melting and blending two-way stretch blow molding, and the surface layer o...
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