Non-aqueous electrolyte secondary battery negative electrode and non-aqueous electrolyte secondary battery using same
A non-aqueous electrolyte and secondary battery technology, which is applied in the field of negative electrodes for non-aqueous electrolyte secondary batteries and non-aqueous electrolyte secondary batteries, and can solve the problems of large expansion and contraction of negative electrodes and reduced cycle life of electrodes.
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[0174] Hereinafter, the present invention will be described in more detail using examples and comparative examples. However, the technical scope of the present invention is not limited only by the following examples. It should be noted that, unless otherwise specified, "parts" means "parts by mass". In addition, the steps up to the preparation of the nonaqueous electrolyte secondary battery were all performed in a dry room.
manufacture example 1
[0177] To a personal synthesizer (manufactured by EYELA, ChemiStation) of a 100 mL test tube container equipped with a stirrer, a temperature sensor, a nitrogen line, a decompression line, and a reflux adapter, 1.0 g of methacrylic acid-modified butadiene rubber (KURARAY Co. Manufactured, L-1253, number average molecular weight 7000 (polystyrene conversion value by GPC), having a methacryloyl group at one end), 7.0 g of acrylic acid, 14 g of toluene, and 14 g of DMF were used to prepare a monomer mixed liquid. Then, while stirring the prepared monomer mixed liquid at a stirring rate of 400 rpm, nitrogen gas was blown in for 1 minute, and then a depressurization operation was performed for 1 minute. The above operation was repeated 5 times for nitrogen replacement. Thereafter, the monomer liquid mixture was heated to 65°C, and the initiator liquid mixture obtained by dissolving 0.01 g of 2,2'-azobis(2,4-dimethylvaleronitrile) in 1 g of toluene and 1 g of DMF Added and free rad...
manufacture example 2
[0185] To a personal synthesizer (manufactured by EYELA, ChemiStation) equipped with a stirrer, a temperature sensor, a nitrogen line, a decompression line, and a reflux adapter in a 100 mL test tube container, 0.1 g of methacrylic acid-modified butadiene rubber (KURARAY Co. Manufactured, L-1253, number average molecular weight 7000 (polystyrene conversion value by GPC), having a methacryloyl group at one end), 7.9 g of acrylic acid, 14 g of toluene, and 14 g of N,N-dimethylformamide (DMF) To prepare the monomer mixture. Then, while stirring the prepared monomer mixed liquid at a stirring rate of 400 rpm, nitrogen gas was blown in for 1 minute, and then a depressurization operation was performed for 1 minute. The above operation was repeated 5 times for nitrogen replacement. Thereafter, the monomer mixture was heated to 65°C, and the initiator mixture obtained by dissolving 0.01 g of 2,2'-azobis(2,4-dimethylvaleronitrile) in 1 g of toluene and 1 g of DMF was added to , to ca...
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