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Directional solidification smelting device and method for refractory high-entropy alloy

A directional solidification, high-entropy alloy technology, used in lighting and heating equipment, charging processing types, furnace components, etc., can solve the problem that the smelting raw materials cannot be in a molten state at the same time, the structure of refractory high-entropy alloys is uneven, and it is difficult to ensure uniform stirring. and other problems, to achieve the effect of good electromagnetic field coupling, low cost, and ensuring consistency

Inactive Publication Date: 2019-11-29
NAT UNIV OF DEFENSE TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the heating method of this process is point heating, combined with the bottom water-cooled copper mold to dissipate heat, so the melting raw materials cannot be in a molten state at the same time, so it is difficult to ensure uniform stirring
In addition, the melting points of RHEAs components are quite different, and this heating and heat dissipation method will lead to a large range of liquid-solid two-phase mixing zone in the alloy ingot, and the local area will solidify successively during solidification, resulting in large-scale dispersed shrinkage. Loose and element segregation, the use of arc melting process results in uneven structure of refractory high-entropy alloys, non-concentrated defects and difficult forming

Method used

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  • Directional solidification smelting device and method for refractory high-entropy alloy
  • Directional solidification smelting device and method for refractory high-entropy alloy
  • Directional solidification smelting device and method for refractory high-entropy alloy

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Effect test

Embodiment 1

[0053] A directional solidification smelting device for a refractory high-entropy alloy of the present invention comprises a quartz glass tube 5, a melting crucible 2, an induction coil 10 and a melting power supply 11, the melting crucible 2 is equipped with an alloy raw material 1 and is located inside the quartz glass tube 5, The induction coil 10 is connected to the smelting power supply 11 and sleeved on the outside of the quartz glass tube 5 and is used for melting the alloy raw material 1 in the smelting crucible 2. The directional solidification smelting equipment also includes a lifting device 15, and the induction coil 10 is connected to the lifting device 15. Driven by the device 15, it moves up and down along the quartz glass tube 5.

[0054] In this embodiment, the quartz glass tube 5 is a hollow quartz tube, and the quartz glass tube 5 is vertically fixed on the base 7, and the stainless steel flange presses the rubber ring to expand and fit the wall of the quartz...

Embodiment 2

[0075] The directional solidification smelting equipment for the refractory high-entropy alloy used in this embodiment is the same as that in Embodiment 1.

[0076] The directional solidification and smelting method of a refractory high-entropy alloy in this embodiment is roughly the same as in Embodiment 1, the difference is that during induction smelting, the induction coil 10 rises at a speed v 0 It is 1.2mm / s.

[0077] Cut the longitudinal section of the alloy ingot by wire cutting, and observe the size, shape and distribution of shrinkage cavities on the surface after grinding the metallographic phase. The results are as follows: Figure 8 As shown, it can be seen that the shrinkage cavities are mainly distributed in the upper half of the alloy ingot, and the number of shrinkage cavities in the lower half is relatively small.

Embodiment 3

[0079] The directional solidification smelting equipment for the refractory high-entropy alloy used in this embodiment is the same as that in Embodiment 1.

[0080] The directional solidification and smelting method of a refractory high-entropy alloy in this embodiment is roughly the same as in Embodiment 1, the difference is that during induction smelting, the induction coil 10 rises at a speed v 0 It is 3.6mm / s.

[0081] Cut the longitudinal section of the alloy ingot by wire cutting, and observe the size, shape and distribution of shrinkage cavities on the surface after grinding the metallographic phase. The results are as follows: Figure 9 As shown, it can be seen that the distribution of shrinkage cavities inside the alloy ingot is scattered and the number is large, and the main concentration is in the middle of the alloy ingot.

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PUM

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Abstract

The invention discloses a directional solidification smelting device and method for a refractory high-entropy alloy. The directional solidification smelting device comprises a quartz glass tube, a smelting crucible, an induction coil and a smelting power supply, wherein an alloy raw material fills the smelting crucible and is positioned inside the quartz glass tube; the induction coil is connectedwith the smelting power supply and sleeves the quartz glass tube for smelting the alloy raw material in the smelting crucible; the directional solidification smelting device further comprises a lifting device; and the induction coil is connected with the lifting device and is driven by the lifting device to ascend and descend along the quartz glass tube. The directional solidification smelting device and method for the refractory high-entropy alloy have the advantages that alloy ingots smelted are regular in molding, uniform in internal structure, and concentrated in defects, such as shrinkage cavity and shrinkage porosity.

Description

technical field [0001] The invention relates to the field of alloy smelting, in particular to a directional solidification smelting equipment and smelting method for refractory high-entropy alloys. Background technique [0002] Superalloys are key structural materials in the fields of aerospace and industrial power. They have become an irreplaceable material for military and civilian high-temperature gas turbines, and play a very important role in promoting the progress of industry and human civilization. Especially in the military field, with the continuous improvement of military aircraft performance requirements, the proportion of superalloys in engine materials is getting higher and higher, and higher requirements are also put forward for alloy performance, such as higher high temperature strength and specific strength , higher operating temperature and so on. High-temperature nickel-based alloys are the most mature high-temperature structural materials. After continuou...

Claims

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Application Information

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IPC IPC(8): F27B14/04F27B14/14F27B14/10F27B14/08C22C1/02C22C30/00
CPCC22C1/02C22C30/00F27B14/04F27B14/08F27B14/10F27B14/14F27B2014/045F27M2003/13
Inventor 唐宇李顺白书欣王洁叶益聪万红朱利安刘希月
Owner NAT UNIV OF DEFENSE TECH
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