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Microcapsules and preparation method thereof

A technology of microcapsules and microdroplets, which is applied in the field of microcapsules and its preparation, can solve the problems of poor stability and low oil loading capacity of microcapsules, and achieve the effects of strong binding ability, improved oxidation stability, and good application adaptability

Active Publication Date: 2019-12-03
QINGDAO TECHN COLLEGE
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] In order to solve the technical problems of low oil loading and poor stability of microcapsules in the prior art, the invention provides a microcapsule and a preparation method thereof

Method used

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  • Microcapsules and preparation method thereof
  • Microcapsules and preparation method thereof
  • Microcapsules and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0030] 25g of sodium alginate was dissolved in 5L of water, 500g of DHA microbial oil (Qingdao Youlan Biotechnology Co., Ltd.), and a water jet venturi tube (SSQ-125, 3mm nozzle diameter, 0.7m 3 / h flow rate) is connected with a miniature magnetic pump (MP10R, Shanghai Core Pump Valve Manufacturing Co., Ltd.) through a pressure-resistant vacuum tube, DHA grease is pumped into the inlet of the Venturi tube, and sodium alginate solution is sucked from the suction port of the Venturi tube (see figure 1 ), atomized wet microcapsules into 10L 1% CaCl 2 The capsule wall was solidified in the solution for 1 min. The cured wet microcapsule particles were centrifuged at 1500 rpm at low speed and washed with water, and then entered the fluidized bed (WBF1G, Changzhou Fanjun Drying Equipment Co., Ltd.), using modified starch as the embedding agent. Prepare dry microcapsule powder, spray 200g of modified starch by top spraying method, the inlet air temperature is 60°C, after embedding, us...

Embodiment 2

[0032] 250g of potassium alginate was dissolved in 5L of water, 100g of linseed oil (Inner Mongolia Hongjingyuan Oil Co., Ltd.), and a water jet venturi tube (SSQ-125, 3mm nozzle diameter, 0.7m 3 / h flow rate) is connected with a miniature magnetic pump (MP10R, Shanghai Coolui Pump and Valve Manufacturing Co., Ltd.) through a pressure-resistant vacuum tube. wet microcapsules into 10L of 0.1% CaSO 4 Carry out capsule wall solidification in the solution, solidification time 2min, the wet microcapsule particle after solidification is centrifuged at 1500 rpm at low speed, washed with water, enters fluidized bed (WBF1G, Changzhou Fanjun Drying Equipment Co., Ltd.), uses octenyl succinate Use starch as embedding agent to prepare dry microcapsule powder, spray 180g of octenyl succinic esterified starch into the top spray method, and the inlet air temperature is 70°C. After embedding, use 80°C hot air to dry to obtain the product, and the excess starch is fluidized The beds are recyc...

Embodiment 3

[0034] 100g of ammonium alginate was dissolved in 5L of water, and 166g of tuna oil (Taicang Nuoya Shengnuo Biotechnology Co., Ltd.) was prepared, and a water jet venturi tube (SSQ-125, 3mm nozzle diameter, 0.7m 3 / h flow rate) is connected with the miniature magnetic pump (MP10R, Shanghai Core Pump Valve Manufacturing Co., Ltd.) through a pressure-resistant vacuum tube, the tuna oil is pumped into the inlet of the Venturi tube, and the sodium alginate solution is sucked from the suction port of the Venturi tube (attached figure 1 ), the atomized wet microcapsules enter 20L 2% Ca(NO 3 ) 2 Carry out capsule wall solidification in the solution, solidification time 2min, the wet microcapsule particle after solidification is centrifuged at 1500 rpm at low speed, washed with water, enters fluidized bed (WBF1G, Changzhou Fanjun Drying Equipment Co., Ltd.), uses octenyl succinate Use starch as embedding agent to prepare dry microcapsule powder. Spray 600g of octenyl succinic acid es...

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Abstract

The invention relates to the technical field of fat-containing microcapsules, and discloses microcapsules and a preparation method thereof. According to the preparation method, a wall material I namely water-solubility alginate is adopted for entrapping fat in a venturi entrapping manner, and the obtained alginate encapsulated fat microdroplets are subjected to surface layer solidification by a calcium salt; and finally, a wall material II is used for entrapping and agglomerating the solidified microcapsules, so as to obtain microcapsule powder fat. The alginate is directly formed into microcapsule wall entrapping fat, and dry microcapsule powder is obtained, so that the oil capacity and the capsule wall stability of the obtained microcapsules are improved greatly.

Description

technical field [0001] The invention relates to the technical field of oil-containing microcapsules, in particular to a microcapsule and a preparation method thereof. Background technique [0002] In the food industry, liquid oil cannot be directly added to food in a solid state. Microcapsule technology wraps tiny droplets of oil through a specific wall material to make it a solid powder state, expanding the use of oil in food and nutritional additives. At the same time, the wall material of the microcapsule can protect the oil in it from being oxidized by external oxygen and sensitive substances to a certain extent. [0003] The construction of the microcapsule wall and the screening of the wall material affect the oxidation resistance and stability of the final microcapsule, which is also the main technical problem encountered in the application of microcapsule technology in the food industry. At present, the preparation method of microcapsules is mainly to use wall mater...

Claims

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Application Information

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IPC IPC(8): A23P10/30A23P10/35A23L29/30A23L29/00A23L33/115A23L33/12
CPCA23V2002/00A23L29/015A23L29/30A23L33/115A23L33/12A23P10/30A23P10/35A23V2250/1578A23V2250/5112A23V2250/5114A23V2250/5118
Inventor 赵澎苏娟王文静赵美法吕海金
Owner QINGDAO TECHN COLLEGE