Preparation method of antibacterial polyester fiber in core-spun structure
A skin-core structure and polyester technology, applied in the field of chemical fiber processing, can solve the problems of easy aggregation of silver particles, antibacterial effect, unsustainable antibacterial performance, harm to health and the environment, etc., to achieve excellent antibacterial performance and antibacterial durability, good product quality, Not easy to fall off effect
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Embodiment 1
[0018] The preparation method of the skin-core structure antibacterial polyester involved in the present embodiment comprises the following steps:
[0019] (1) Coating treatment of silver powder: Use trihydroxyethylmethyl quaternary ammonium methyl sulfate and silver powder to mix and stir to eliminate the electrostatic force between silver powder The weight ratio is 0.5:100, and the silver powder particle size is 3-20 μm; mix ethyl orthosilicate with deionized water and ethanol according to the weight ratio of 1:1.5:4, add hydrochloric acid solution to adjust the pH to 3, and At 20°C, react for 45 minutes to obtain a transparent silica sol; add the mixed silver powder into the silica sol for stirring, and when a uniform suspension is formed, add concentrated ammonia water with a mass fraction of 28% until stirring forms gel state, and then washed with deionized water; finally put the obtained gel into a vacuum drying oven for drying treatment, that is, the surface-coated SiO ...
Embodiment 2
[0023] The preparation method of the skin-core structure antibacterial polyester involved in the present embodiment comprises the following steps:
[0024] (1) Coating treatment of silver powder: Use trihydroxyethylmethyl quaternary ammonium methyl sulfate and silver powder to mix and stir to eliminate the electrostatic force between silver powder The weight ratio is 2:100, and the silver powder particle size is 3-20 μm; mix ethyl orthosilicate with deionized water and ethanol according to the weight ratio of 1:2.5:7, add hydrochloric acid solution to adjust the pH to 6, and At 35°C, react for 10 minutes to obtain a transparent silica sol; add the mixed silver powder into the silica sol for stirring, and when a uniform suspension is formed, add concentrated ammonia water with a mass fraction of 28% until stirring forms gel state, and then washed with deionized water; finally put the obtained gel into a vacuum drying oven for drying treatment, that is, the surface-coated SiO 2...
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