Preparation method of antibacterial polyester staple fibers
A polyester staple fiber and polyester chip technology is applied in the preparation field of polyester staple fiber and antibacterial polyester staple fiber, which can solve the problems of easy agglomeration of silver particles, antibacterial effect, non-lasting antibacterial performance, harm to health and environment, etc., and achieve excellent antibacterial performance. And antibacterial persistence, good product quality, not easy to fall off
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Embodiment 1
[0016] The preparation method of the antibacterial polyester staple fiber that present embodiment relates to, comprises the following steps:
[0017] (1) Treatment of silver powder: Mix and stir sodium nonylphenoxypropane sulfonate powder with silver powder to reduce the electrostatic force between silver powders. The weight ratio of sodium nonylphenoxypropane sulfonate to silver powder is 1:100 , the particle size of silver powder is 3-20μm; mix ethyl orthosilicate with deionized water and ethanol according to the weight ratio of 1:1:5, add hydrochloric acid to adjust the pH value of the solution to 3, and react at a temperature of 15°C for 50min , to obtain a transparent silica sol; add the mixed silver powder into the silica sol and stir, and when a uniform suspension is formed, add concentrated ammonia water with a mass fraction of 28% until stirring to form a gel state, and then use Ionized water cleaning; finally put the obtained gel into a vacuum drying oven for drying ...
Embodiment 2
[0021] The preparation method of the antibacterial polyester staple fiber that present embodiment relates to, comprises the following steps:
[0022] (1) Treatment of silver powder: Mix and stir sodium nonylphenoxypropane sulfonate powder with silver powder to reduce the electrostatic force between silver powders. The weight ratio of sodium nonylphenoxypropane sulfonate to silver powder is 8:100 , the particle size of silver powder is 3-20 μm; mix ethyl orthosilicate with deionized water and ethanol according to the weight ratio of 1:3:6, add hydrochloric acid to adjust the pH value of the solution to 5, and react for 15 minutes at a temperature of 40°C , to obtain a transparent silica sol; add the mixed silver powder into the silica sol and stir, and when a uniform suspension is formed, add concentrated ammonia water with a mass fraction of 28% until stirring to form a gel state, and then use Ionized water cleaning; finally put the obtained gel into a vacuum drying oven for d...
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