A kind of preparation method of high-purity electromagnetic pure iron
An electromagnetic pure iron, high-purity technology, applied in the field of preparation of high-purity electromagnetic pure iron, can solve the problems of high purity, high temperature resistance and wear resistance, which affect the normal use of rotating anode X-ray tubes, rotor and stator gas Gap increase and other problems, to achieve the effect of less impurity content, average chemical composition and microstructure, and reduce segregation
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Embodiment 1
[0024] Utilizing the method of the present invention to prepare high-purity electromagnetic pure iron mainly comprises the following steps:
[0025] (1) Vacuum induction smelting: Take industrial pure iron with a purity of 99.9% and put it into a vacuum induction furnace, vacuumize it until the vacuum degree reaches 5×10 -1 Pa, the ceramic crucible is heated, and when the industrial pure iron in the crucible gradually melts, add 0.035% by weight of rare earth element La and 0.025% by weight of rare earth element Ce to the melt, and then carry out electromagnetic stirring; the added rare earth Elements can work synergistically with other elements to fully refine the grains of the cast structure of electromagnetic pure iron, reduce the generation of segregation, close the vacuum system, fill in an inert protective gas to a vacuum of -0.2Mpa to melt industrial pure iron, and then Pouring is performed to form a precast casting;
[0026] (2) Vacuum consumable remelting: Weld the a...
Embodiment 2
[0030] Utilizing the method of the present invention to prepare high-purity electromagnetic pure iron mainly comprises the following steps:
[0031] (1) Vacuum induction smelting: Take industrial pure iron with a purity of 99.9% and put it into a vacuum induction furnace, vacuumize until the vacuum degree reaches 4×10 -1 Pa, the ceramic crucible is heated, when the industrial pure iron in the crucible gradually melts, add 0.034% by weight rare earth element La and 0.024% by weight rare earth element Ce to the melt, then carry out electromagnetic stirring; the added rare earth element can Synergize with other elements to fully refine the grains of the cast structure of electromagnetic pure iron, reduce the generation of segregation, close the vacuum system, fill in an inert protective gas to a vacuum of 0.01Mpa to melt the industrial pure iron, and then pour it. forming precast castings;
[0032] (2) Vacuum consumable remelting: Weld the above prefabricated castings with the d...
Embodiment 3
[0036] Utilizing the method of the present invention to prepare high-purity electromagnetic pure iron mainly comprises the following steps:
[0037] (1) Vacuum induction smelting: Take industrial pure iron with a purity of 99.9% and put it into a vacuum induction furnace, vacuumize until the vacuum degree reaches 3×10 -1 When Pa, the ceramic crucible is heated, and when the industrial pure iron in the crucible gradually melts, add 0.033% by weight rare earth element La and 0.023% by weight rare earth element Ce to the melt, and then carry out electromagnetic stirring; the added rare earth element can Synergize with other elements to fully refine the grains of the cast structure of electromagnetic pure iron, reduce the generation of segregation, close the vacuum system, fill in an inert protective gas to a vacuum of 0.02Mpa to melt the industrial pure iron, and then pour it. forming precast castings;
[0038] (2) Vacuum consumable remelting: Weld the above prefabricated castin...
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Abstract
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