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A kind of preparation method of high-purity electromagnetic pure iron

An electromagnetic pure iron, high-purity technology, applied in the field of preparation of high-purity electromagnetic pure iron, can solve the problems of high purity, high temperature resistance and wear resistance, which affect the normal use of rotating anode X-ray tubes, rotor and stator gas Gap increase and other problems, to achieve the effect of less impurity content, average chemical composition and microstructure, and reduce segregation

Active Publication Date: 2021-09-21
SHAANXI SIRUI ADVANCED MATERIALS CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] At present, the rotating speed of the rotating anode tube rotor is above 3000 rpm, the high-speed rotating anode tube can reach 7200 rpm, and the ultra-high-speed tube can reach above 10,000 rpm. The tube anode rotor speed is It is designed according to the current density of the focal point of the tube. For the tube with the same current, the smaller the focal point, the higher the speed of the rotating anode rotor of the tube. If the rotor speed is abnormal, when the tube is ignited, its output kV and mA The accuracy of the tube will be lower, which will reduce the imaging quality, thereby affecting the medical staff's judgment on the condition. It can be seen that it is important to ensure good heat dissipation of the tube
[0004] Since the rotor is difficult to withstand the high temperature generated by the rotation when it is rotating, it is easy to burn out and affect the normal use of the rotating anode X-ray tube. Therefore, the rotor with high temperature resistance can prevent its temperature from being too high and burning If the rotor is used for a long time, it will wear and tear, which will increase the air gap between the rotor and the stator, which will increase the eddy current and increase the operating current to a certain extent, and the purity of the material used to prepare the rotor parts will also affect the performance of the rotor. The existing rotors are still lacking in high purity, high temperature resistance and wear resistance, and need to be improved

Method used

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  • A kind of preparation method of high-purity electromagnetic pure iron

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Experimental program
Comparison scheme
Effect test

Embodiment 1

[0024] Utilizing the method of the present invention to prepare high-purity electromagnetic pure iron mainly comprises the following steps:

[0025] (1) Vacuum induction smelting: Take industrial pure iron with a purity of 99.9% and put it into a vacuum induction furnace, vacuumize it until the vacuum degree reaches 5×10 -1 Pa, the ceramic crucible is heated, and when the industrial pure iron in the crucible gradually melts, add 0.035% by weight of rare earth element La and 0.025% by weight of rare earth element Ce to the melt, and then carry out electromagnetic stirring; the added rare earth Elements can work synergistically with other elements to fully refine the grains of the cast structure of electromagnetic pure iron, reduce the generation of segregation, close the vacuum system, fill in an inert protective gas to a vacuum of -0.2Mpa to melt industrial pure iron, and then Pouring is performed to form a precast casting;

[0026] (2) Vacuum consumable remelting: Weld the a...

Embodiment 2

[0030] Utilizing the method of the present invention to prepare high-purity electromagnetic pure iron mainly comprises the following steps:

[0031] (1) Vacuum induction smelting: Take industrial pure iron with a purity of 99.9% and put it into a vacuum induction furnace, vacuumize until the vacuum degree reaches 4×10 -1 Pa, the ceramic crucible is heated, when the industrial pure iron in the crucible gradually melts, add 0.034% by weight rare earth element La and 0.024% by weight rare earth element Ce to the melt, then carry out electromagnetic stirring; the added rare earth element can Synergize with other elements to fully refine the grains of the cast structure of electromagnetic pure iron, reduce the generation of segregation, close the vacuum system, fill in an inert protective gas to a vacuum of 0.01Mpa to melt the industrial pure iron, and then pour it. forming precast castings;

[0032] (2) Vacuum consumable remelting: Weld the above prefabricated castings with the d...

Embodiment 3

[0036] Utilizing the method of the present invention to prepare high-purity electromagnetic pure iron mainly comprises the following steps:

[0037] (1) Vacuum induction smelting: Take industrial pure iron with a purity of 99.9% and put it into a vacuum induction furnace, vacuumize until the vacuum degree reaches 3×10 -1 When Pa, the ceramic crucible is heated, and when the industrial pure iron in the crucible gradually melts, add 0.033% by weight rare earth element La and 0.023% by weight rare earth element Ce to the melt, and then carry out electromagnetic stirring; the added rare earth element can Synergize with other elements to fully refine the grains of the cast structure of electromagnetic pure iron, reduce the generation of segregation, close the vacuum system, fill in an inert protective gas to a vacuum of 0.02Mpa to melt the industrial pure iron, and then pour it. forming precast castings;

[0038] (2) Vacuum consumable remelting: Weld the above prefabricated castin...

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Abstract

The invention discloses a method for preparing high-purity electromagnetic pure iron, which belongs to the technical field of pure iron preparation. It includes the steps of vacuum induction smelting, vacuum self-consumption remelting, billet rolling, and aging treatment; the present invention selects industrial pure iron with a purity higher than 99% as a raw material, and adopts the "double vacuum smelting" method in the production process, The ability of vacuum induction furnace melting to remove gases, non-metal assimilates and harmful elements has been fully demonstrated. At the same time, through vacuum self-consumption remelting and secondary purification, electromagnetic purity with high purity, good density, and average chemical composition and microstructure can be obtained. Iron; through vacuum magnetron sputtering and glow nitriding treatment on rolled profiles, the surface hardness, wear resistance and high temperature resistance of electromagnetic pure iron can be effectively improved.

Description

technical field [0001] The invention belongs to the technical field of pure iron preparation, and in particular relates to a preparation method of high-purity electromagnetic pure iron. Background technique [0002] X-ray tubes are widely used in X-ray imaging technology. There are two types of common X-ray tubes on the market, one is a fixed anode tube, and the other is a rotating anode tube with increased heat capacity. The rotating anode X-ray tube is a high-vacuum electric vacuum device. Its working principle is that the rotor is fixed on the bearing seat at one end of the vacuum glass tube, and the outer stator of the vacuum glass tube can drive it to rotate. The filament is fixed on the Set on the cathode at the other end of the vacuum glass tube, respectively apply negative piezoelectricity to the filament and positive piezoelectricity to the anode, and the electrons emitted by the filament hit the anode to generate X-rays. [0003] At present, the rotating speed of ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C21C3/00C21D8/12C21C7/10
CPCC21C3/00C21C7/10C21D8/1222C21D8/1244C21D8/1283
Inventor 陈梅杨平侯蕊王小明
Owner SHAANXI SIRUI ADVANCED MATERIALS CO LTD