Antimicrobial heating regenerated polyester fiber and preparation method thereof
A technology of recycled polyester and fiber, applied in the direction of fiber chemical characteristics, single-component polyester rayon, rayon manufacturing, etc., can solve the problems of environmental pollution, waste of resources, etc., meet market demand, save process and cost Effect
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Embodiment 1
[0045] Embodiment 1: the preparation of 1.67dtex * 38mm antibacterial heating regenerated polyester fiber
[0046] S1: Preparation of antibacterial and exothermic recycled polyester masterbatch
[0047] S1.1 Nano ZrO2 powder pretreatment
[0048] Start the high-speed mixer to run at low speed and then switch to high-speed operation to 900rpm, add nano-ZrO2 powder with an average particle size of 50nm into the high-speed mixer, then add anti-sticking agent calcium stearate powder and mix evenly, the addition amount is nano-ZrO2 0.05% by weight of the powder; then the high-speed mixer is heated up to 125° C., dried for 8 hours, and then the treated nano-zirconia powder is put into a bag and sealed for later use.
[0049] S1.2 Inorganic antibacterial powder pretreatment
[0050] Start the high-speed mixer, first run at low speed and then switch to high-speed operation to 900rpm, add 5% sodium zirconium phosphate copper-loaded antibacterial powder into the high-speed mixer, then...
Embodiment 2
[0066] Example 2 Preparation of 1.56dtex×38mm antibacterial and exothermic regenerated polyester fiber
[0067] S1: Preparation of antibacterial and exothermic recycled polyester masterbatch
[0068] S1.1 Nano ZrO2 powder pretreatment
[0069] Start the high-speed mixer to run at low speed and then switch to high-speed operation to 850rpm, add nano-ZrO2 powder with an average particle size of 50nm into the high-speed mixer, then add anti-sticking agent calcium stearate powder and mix evenly, the addition amount is nano-ZrO2 0.06% by weight of the powder; then the high-speed mixer was heated to 120° C., dried for 9 hours, and then the treated nano-zirconia powder was put into a bag and sealed for later use.
[0070] S1.2 Inorganic antibacterial powder pretreatment
[0071] Start the high-speed mixer, first run at low speed and then switch to high speed to 950rpm, add 4.5% silver-loaded apatite antibacterial powder into the high-speed mixer, then add anti-sticking agent calciu...
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