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Lubricating oil viscosity-temperature improver

A technology of improver and lubricating oil, which is applied in the field of lubricating oil, can solve problems such as unstable product quality, uncontrollable process, poor dispersion, etc., and achieve the effect of changing viscosity-temperature characteristics, changing viscosity-temperature performance, and good low-temperature performance

Inactive Publication Date: 2020-04-28
湖北奥斯龙科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

If the dry dosage is increased and the temperature is increased, the process cannot be controlled, so the product quality is unstable and the dispersion in use is poor. This is a major disadvantage of the thermal oxidation preparation method

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0013] Add 18 tons of solvent hexane to a 90m3 polymerization reaction vessel, add it to 10°C, and continuously feed ethylene, propylene, styrene and hydrogen into the reactor, and the molar ratio of hydrogen, ethylene, propylene, and styrene is 0.1:0.45 : 1: 0.8, stir reaction for 1 hour, add 1.8kg main catalyst benzoyl peroxide and 3.6kg cocatalyst triethylaluminum, stop stirring after the reaction, add methanol to terminate, wash with NaOH alkaline solution, and vacuum dry to obtain The product ethylene propylene styrene copolymer.

Embodiment 2

[0015] Add 20 tons of solvent hexane to a 90m3 polymerization reaction vessel, add it to 20°C, and continuously feed ethylene, propylene, styrene and hydrogen into the reactor, and the molar ratio of hydrogen, ethylene, propylene, and styrene is 0.3:0.5 : 1:1, stirring reaction for 2 hours, adding 20kg main catalyst benzoyl peroxide and 80kg cocatalyst triethylaluminum, stopping stirring after the reaction, adding methanol to terminate, washing with NaOH alkaline solution, and vacuum drying to obtain product ethylene propylene styrene copolymer.

Embodiment 3

[0017] Add 25 tons of solvent hexane to a 90m3 polymerization reaction vessel, heat to 30°C, and continuously feed ethylene, propylene, styrene and hydrogen into the reactor, and the molar ratio of hydrogen, ethylene, propylene, and styrene is 0.2: 1: 1: 0.8, stirring and reacting for 2.5 hours, adding 125kg main catalyst benzoyl peroxide and 875kg cocatalyst triethylaluminum, stopping stirring after the reaction, adding methanol to terminate, washing with NaOH alkaline solution, and vacuum drying to obtain the product Ethylene propylene styrene copolymer.

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PUM

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Abstract

The invention belongs to the field of lubricating oil, and particularly relates to a lubricating oil viscosity-temperature improver. The preparation method disclosed by the invention comprises the following steps of: adding a solvent hexane into a polymerization reaction container, heating to 10-50 DEG C, and continuously introducing ethylene, propylene, styrene and hydrogen, wherein a molar ratioof hydrogen to ethylene to propylene to styrene is (0.1-0.3):(0.45-1):1:(0.8-1); carrying out a stirring reaction for 1-3 hours, and adding a main catalyst benzoyl peroxide and a cocatalyst triethylaluminum, wherein the addition amount of the main catalyst is 0.01-1% (weight) of the addition amount of the solvent, and the amount of the cocatalyst is 2-10 times the weight of the main catalyst; andstopping stirring after the reaction is finished, adding methanol to terminate, washing with an alkaline solution, and carrying out vacuum drying to obtain the product ethylene-propylene-styrene copolymer. According to the invention, with the lubricating oil viscosity-temperature improver, the viscosity-temperature characteristic, the thickening capacity, the low-temperature performance, the dispersity and other comprehensive indexes of lubricating oil can be changed, and are obviously superior to the viscosity-temperature characteristic, the thickening capacity, the low-temperature performance, the dispersity and other comprehensive indexes of the existing similar products.

Description

technical field [0001] The invention belongs to the field of lubricating oil, and particularly relates to a lubricating oil viscosity-temperature improver. Background technique [0002] Viscosity-temperature improver is one of the indispensable additives for multi-grade engine oil, and its proportion is second only to detergent and dispersant. US statistics show that the amount of viscosity index improver is increasing at an annual rate of 12%. The function of the viscosity-temperature improver is to improve the viscosity-temperature performance of the oil, so that the oil has a higher viscosity index, so as to ensure that the engine can start smoothly at low temperature, and the oil has sufficient viscosity at high temperature to ensure good lubrication. . At the same time, it is required that the viscosity-temperature improver does not have obvious harmful effects on the oxidation stability and detergency of the oil, and the multi-grade engine oil has less viscosity loss ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C10M143/00C08F212/08C08F210/16C08F210/06C10N30/08C10N30/04
CPCC08F210/06C08F212/08C10M143/00C10M2205/022C10M2205/024C10M2205/046C08F210/16
Inventor 赵书军
Owner 湖北奥斯龙科技有限公司
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