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Preparation method of antiviral regenerated cellulose fibres, and fibres thereof

A regenerated cellulose and anti-virus technology, applied in the direction of artificial filaments made of viscose, can solve the problem that copper ions are difficult to disperse evenly, achieve long-term antibacterial and anti-virus effects, strong binding force, maintain uniformity and The effect of stability

Active Publication Date: 2020-06-05
河北艾科瑞纤维有限公司 +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0008] The technical problem to be solved by the present invention is to overcome the deficiencies of the prior art, provide a method for preparing antiviral regenerated cellulose fibers and the fibers thereof, and solve the problem that copper ions are difficult to disperse uniformly in spinning glue, and the copper ions combine Strong, the prepared fiber contains polymorphic valence copper, which has long-term antibacterial and antiviral functions

Method used

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  • Preparation method of antiviral regenerated cellulose fibres, and fibres thereof
  • Preparation method of antiviral regenerated cellulose fibres, and fibres thereof

Examples

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Embodiment 1

[0048] This embodiment provides a method for preparing antiviral regenerated cellulose fibers, comprising the following steps:

[0049] (1) Mix 10 parts of nano-cuprous oxide with 10 parts of carbon nanotubes, add 1 part of dispersant 9320 and 0.5 parts of stabilizer acrylic alkali swelling thickener, adjust the pH to 12 with 78.5 parts of ammonia water, and then use nano high-speed grinding machine for grinding and mixing to prepare copper ion antiviral slurry; the copper content in the copper ion antiviral slurry is 8.8%, and the particle size of the particles in the slurry is 0.4 μm;

[0050] (2) adopt double injection mode to add copper ion antiviral slurry and urea in the cellulose spinning glue, wherein the relative add-on of copper ion antiviral slurry is 0.5%, and the relative add-on of urea is 0.03%, then extruded, coagulated, and drawn to obtain antiviral regenerated cellulose fibers.

[0051] In this example, the obtained antiviral regenerated cellulose fiber has a...

Embodiment 2

[0053] This embodiment provides a method for preparing antiviral regenerated cellulose fibers, comprising the following steps:

[0054] (1) Mix 5 parts of nano-cuprous oxide with 13 parts of carbon nanotubes, add 0.5 parts of dispersant 9320 and 0.2 parts of stabilizer acrylic alkali swelling thickener, adjust the pH to 10 with 81.3 parts of ammonia water, and then use nano high-speed grinding machine for grinding and mixing to prepare copper ion antiviral slurry; the copper content in the copper ion antiviral slurry is 4.4%, and the particle size of the particles in the slurry is 0.4 μm;

[0055] (2) adopt double injection mode to add copper ion antiviral slurry and urea in the cellulose spinning glue, wherein the relative add-on of copper ion antiviral slurry is 2%, and the relative add-on of urea is 0.04%, then extruded, coagulated, and drawn to obtain antiviral regenerated cellulose fibers.

[0056] In this example, the obtained antiviral regenerated cellulose fiber has a...

Embodiment 3

[0058] This embodiment provides a method for preparing antiviral regenerated cellulose fibers, comprising the following steps:

[0059] (1) Mix 20 parts of nano-cuprous oxide with 8 parts of carbon nanotubes, add 1 part of dispersant 9320 and 0.5 parts of stabilizer acrylic alkali swelling thickener, adjust the pH to 12 with 70.5 parts of ammonia water, and then use nano high-speed grinding machine for grinding and mixing to prepare copper ion antiviral slurry; the copper content in the copper ion antiviral slurry is 17.7%, and the particle size of the particles in the slurry is 0.2 μm;

[0060] (2) adopt double injection mode to add copper ion antiviral slurry and urea in the cellulose spinning glue, wherein the relative add-on of copper ion antiviral slurry is 1%, and the relative add-on of urea is 0.05%, then extruded, coagulated, and drawn to obtain antiviral regenerated cellulose fibers.

[0061] In this example, the obtained antiviral regenerated cellulose fiber has a p...

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Abstract

The invention discloses a preparation method of antiviral regenerated cellulose fibres, and fibres thereof. The preparation method comprises the following steps of: (1), mixing a monovalent copper compound with a carrier, adding a dispersing agent and a stabilizing agent, adjusting pH, then, grinding and mixing, and preparing copper ion antiviral paste; and (2), adding the copper ion antiviral paste and a chelating agent into cellulose spinning gel solution in a double injection manner, and then, spinning, so that the antiviral regenerated cellulose fibres are obtained. The antiviral regenerated cellulose fibres prepared by the invention contain polyvalent copper, can effectively inhibit microbial reproduction for a long time, and have relatively antiviral and antibacterial effects; and the fibres in the invention also can be blended and interwoven with other fibres, and used for producing different types of antiviral and antibacterial textiles.

Description

technical field [0001] The invention belongs to the field of functional fibers and textiles, and in particular relates to a preparation method of an anti-virus regenerated cellulose fiber and the fiber thereof, and more specifically relates to a copper ion anti-virus regenerated cellulose fiber and a preparation method thereof. Background technique [0002] Regenerated cellulose fiber is a fiber made from natural cellulose (cotton, hemp, bamboo, tree, shrub, etc.), which has good hygroscopicity, drapability, easy dyeing and biodegradability. Regenerated cellulose fiber has good spinnability. Short fiber can be spun purely or blended with other textile fibers. The fabric is soft, smooth, breathable, comfortable to wear, and has bright color and good color fastness after dyeing. [0003] With the improvement of people's requirements for quality of life and the pursuit of healthy life, textiles that can play antibacterial and antiviral functions are more and more popular. Silv...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D01F2/08
CPCD01F2/08
Inventor 徐佳威吴国清李振峰陈达志董晓宁苏立超张焕志范梅欣吴兴乐
Owner 河北艾科瑞纤维有限公司
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