Endoluminal device and polymer
A composition and prepolymer technology, which can be applied in the direction of human tubular structure devices, surgical adhesives, blood vessels, etc., can solve problems such as short recovery period
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Embodiment 1
[0128] Embodiment 1: the preparation of organogel
[0129] Organogels are prepared by mixing together two solutions, C1 and C2. First, separate C1 and C2 solutions are prepared by mixing together appropriate amounts of the appropriate ingredients until the solutions are uniform and any solid material that was part of the formulation is completely dissolved. Then add C1 to C2 (or C2 to C1) and mix the two components together under constant stirring for 5 to 15 seconds. Alternatively, fill two barrel cartridges, barrel 1 and barrel 2, with C1 and C2 respectively, and mix the solutions together during dispensing of the solutions into appropriate containers by a static mixer. The final mixed solution was placed in a 37°C water bath and monitored until gelation was complete. An illustration of the formation of the organogel composition is as Figure 6 shown.
[0130]
[0131] *CHP is supplied @80%, the other 20% are aromatic solvents.
[0132] Additional organogels were pre...
Embodiment 2
[0161] Example 2: Characterization of organogels
[0162] The compression modulus of the prepared organogel was measured by a single column material testing system (Instron Model Number 3343) using ASTM Standard D575-91 Rubber Compression Standard Test Method, which is incorporated herein by reference.
[0163] Table 1 summarizes the gel setting time and compressive modulus of the prepared organogels.
[0164] Table 1
[0165]
Embodiment 3
[0166] Embodiment 3: stability test
[0167] The organogels prepared above were screened for shelf-life stability of the individual polymer system components (Cl and C2 solutions) under accelerated conditions at 60° C. for a comparable time corresponding to 18 months at room temperature. The results showed that the component solutions were stable and once combined formed organogels suitable for the intended application.
[0168] The organogel of Composition 1 was tested with an inner bag (Endologix) as a component of an endovascular aneurysm repair system surrounding a stent placed in an abdominal aortic aneurysm (AAA). The inner bag was prefilled and flushed with saline to remove air and determine the fill volume. After flushing, the two-component polymer system from Composition 1 was injected into the inner bag using a 2-barrel cartridge, dispensed using a ratchet gun at 180 mm Hg pressure. The inner pocket maintained its preset shape, thus illustrating the stability of th...
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