Polymer material for repairing concrete cracks and preparation method thereof
A polymer material and concrete technology, applied in the field of concrete repair, can solve the problems affecting the effectiveness of concrete crack repair, repair interface fatigue damage, and the failure of concrete crack surface repair to meet high durability requirements.
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Embodiment 1
[0052] A polymer material for repairing concrete cracks is prepared through the following process steps:
[0053] 1) Dissolve monomer b1 (140g) in 100g water to make solution (P1); mix a1 (10g) and c1 (6g) to make solution P2; dissolve 0.5g of mercaptopropionic acid and 0.25g of L-ascorbic acid In 50g of water, make solution P3;
[0054] 2) Warm up the solution P1 to 35°C, add 0.45g of hydrogen peroxide to the solution P1, then add the solutions P2 and P3 to the solution P1 at the same time, the time for adding the solution P2 is 3.0h, and the solution P3 Adding time is 3.5h;
[0055] 3) After all the dropwise addition is completed, continue the heat preservation reaction for 1 hour, and then add water to dilute to obtain a transparent liquid with a mass concentration of 40%.
[0056] 4) Add 0.4 g of triethylamine to water to prepare a 10% aqueous solution, quickly add it into 125 g of polymer solution (40%), and stir for 30 seconds to obtain a polymer repair solution.
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Embodiment 2
[0059] A polymer material for repairing concrete cracks is prepared through the following process steps:
[0060] 1) Dissolve monomer b2 (120g) in 100g water to make solution P1; mix monomer a1 (8.5g) and monomer c1 (6g) to make solution P2; mix mercaptopropionic acid 0.5g and L-ascorbic acid Dissolve 0.3g in 50g of water to make solution P3;
[0061] 2) Warm up solution P1 to 35°C, add 0.45g of hydrogen peroxide to P1, then add solutions P2 and P3 to solution P1 at the same time. The time is 4.0h;
[0062] 3) After all the addition is completed, continue the heat preservation reaction for 1 hour, and then add water to dilute to obtain a transparent liquid with a mass concentration of 40%;
[0063] 4) Add 0.25g of triethylamine into water to prepare a 10% aqueous solution, quickly add it into 125g of polymer solution (40%), and stir for 30s to obtain a polymer repair solution.
Embodiment 3
[0065] A polymer material for repairing concrete cracks is prepared through the following process steps:
[0066] 1) Dissolve monomer b1 (140g) in 100g water to make solution P1; mix monomer a2 (11.0g) and monomer c1 (5g) to make solution P2; mix mercaptopropionic acid 0.4g and L-ascorbic acid 0.35 g was dissolved in 50g of water to prepare solution P3;
[0067] 2) Warm up the solution P1 to 35°C, add 0.55g of hydrogen peroxide to the solution P1, then add the solutions P2 and P3 to the solution P1 at the same time, the time for adding the solution P2 is 3.0h, and the solution P3 Adding time is 3.5h;
[0068] 3) After all the addition is completed, continue the heat preservation reaction for 1 hour, and then add water to dilute to obtain a transparent liquid with a mass concentration of 40%;
[0069] 4) Add 0.5 g of triethylamine to water to prepare a 10% aqueous solution, quickly add it into 125 g of polymer solution (40%), and stir for 30 s to obtain a polymer repair solut...
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