Preparation method of oil-water separation fabric and oil-water separation fabric prepared thereby
A technology of oil-water separation and fabric, which is applied in the preparation of oil-water separation functional fabrics, the preparation method of oil-water separation fabrics and the field of oil-water separation fabrics, which can solve the problems of ineffective separation and reduced oil-water separation efficiency, and achieve high production efficiency, Good fiber capillary effect and short process flow
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[0036] Example 1
[0037] S1. Hydrolyze tetrabutyl titanate to obtain a titanium dioxide sol.
[0038] S11. Adding tetrabutyl titanate to an anhydrous ethanol solution to obtain a tetrabutyl titanate anhydrous ethanol solution, the concentration of the tetrabutyl titanate in anhydrous ethanol solution is 200-400 g / L;
[0039] S12. Add 100ml of tetrabutyl titanate anhydrous ethanol solution with a concentration of 300g / L dropwise to a mixed solution consisting of 80ml of absolute ethanol, 20ml of glacial acetic acid and 20ml of deionized water at room temperature, while adding dropwise While stirring, continue to stir at room temperature after the dropping is completed until the solution appears light blue to prepare a titanium dioxide sol.
[0040] S2. The siloxane is added to the titanium dioxide sol for reaction to obtain a modified titanium dioxide sol.
[0041] 13ml of hexadecyltrimethoxysilane was added dropwise to the titanium dioxide sol, and the reaction was stirred at 30°C for...
Example Embodiment
[0047] Example 2
[0048] S1. Hydrolyze tetrabutyl titanate to obtain a titanium dioxide sol.
[0049] S11. Adding tetrabutyl titanate to an anhydrous ethanol solution to obtain a tetrabutyl titanate anhydrous ethanol solution, the concentration of the tetrabutyl titanate in anhydrous ethanol solution is 200-400 g / L;
[0050] S12. Add 100ml of tetrabutyl titanate anhydrous ethanol solution with a concentration of 300g / L dropwise to a mixed solution consisting of 80ml of absolute ethanol, 20ml of glacial acetic acid and 20ml of deionized water at room temperature, while adding dropwise While stirring, continue to stir at room temperature after the dropping is completed until the solution appears light blue to prepare a titanium dioxide sol.
[0051] S2. The siloxane is added to the titanium dioxide sol for reaction to obtain a modified titanium dioxide sol.
[0052] 20ml of hexadecyltrimethoxysilane was added dropwise to the titanium dioxide sol, and the reaction was stirred at 30°C for...
Example Embodiment
[0060] Example 3
[0061] S1. Hydrolyze tetrabutyl titanate to obtain a titanium dioxide sol.
[0062] S11. Adding tetrabutyl titanate to an anhydrous ethanol solution to obtain a tetrabutyl titanate anhydrous ethanol solution, the concentration of the tetrabutyl titanate in anhydrous ethanol solution is 200-400 g / L;
[0063] S12. Add 100ml of tetrabutyl titanate anhydrous ethanol solution with a concentration of 300g / L dropwise to a mixed solution consisting of 80ml of absolute ethanol, 20ml of glacial acetic acid and 20ml of deionized water at room temperature, while adding dropwise While stirring, continue to stir at room temperature after the dropping is completed until the solution appears light blue to prepare a titanium dioxide sol.
[0064] S2. The siloxane is added to the titanium dioxide sol for reaction to obtain a modified titanium dioxide sol.
[0065] 6ml of hexadecyltrimethoxysilane was added dropwise to the titanium dioxide sol, and the reaction was stirred at 30°C for ...
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