Preparation method of oil-water separation fabric and oil-water separation fabric prepared thereby
A technology of oil-water separation and fabric, which is applied in the preparation of oil-water separation functional fabrics, the preparation method of oil-water separation fabrics and the field of oil-water separation fabrics, which can solve the problems of ineffective separation and reduced oil-water separation efficiency, and achieve high production efficiency, Good fiber capillary effect and short process flow
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Embodiment 1
[0037] S1. Hydrolyzing tetrabutyl titanate to obtain titanium dioxide sol.
[0038] S11. Adding tetrabutyl titanate into the absolute ethanol solution to obtain the tetrabutyl titanate absolute ethanol solution, the concentration of the tetrabutyl titanate absolute ethanol solution is 200-400 g / L;
[0039] S12. At room temperature, add 100ml of tetrabutyl titanate absolute ethanol solution with a concentration of 300g / L dropwise to a mixed solution consisting of 80ml of absolute ethanol, 20ml of glacial acetic acid and 20ml of deionized water, while adding While stirring, continue to stir at room temperature after the dropwise addition until the solution appears light blue, and a titanium dioxide sol is prepared.
[0040] S2. Adding siloxane into the titanium dioxide sol for reaction to obtain a modified titanium dioxide sol.
[0041] 13 ml of hexadecyltrimethoxysilane was added dropwise into the titanium dioxide sol, and stirred and reacted at 30° C. for 6 hours to obtain a ...
Embodiment 2
[0048] S1. Hydrolyzing tetrabutyl titanate to obtain titanium dioxide sol.
[0049] S11. Adding tetrabutyl titanate into the absolute ethanol solution to obtain the tetrabutyl titanate absolute ethanol solution, the concentration of the tetrabutyl titanate absolute ethanol solution is 200-400 g / L;
[0050] S12. At room temperature, add 100ml of tetrabutyl titanate absolute ethanol solution with a concentration of 300g / L dropwise to a mixed solution consisting of 80ml of absolute ethanol, 20ml of glacial acetic acid and 20ml of deionized water, while adding While stirring, continue to stir at room temperature after the dropwise addition until the solution appears light blue, and a titanium dioxide sol is prepared.
[0051] S2. Adding siloxane into the titanium dioxide sol for reaction to obtain a modified titanium dioxide sol.
[0052] 20 ml of hexadecyltrimethoxysilane was added dropwise to the titanium dioxide sol, and stirred at 30° C. for 6 hours to obtain a modified titan...
Embodiment 3
[0061] S1. Hydrolyzing tetrabutyl titanate to obtain titanium dioxide sol.
[0062] S11. Adding tetrabutyl titanate into the absolute ethanol solution to obtain the tetrabutyl titanate absolute ethanol solution, the concentration of the tetrabutyl titanate absolute ethanol solution is 200-400 g / L;
[0063] S12. At room temperature, add 100ml of tetrabutyl titanate absolute ethanol solution with a concentration of 300g / L dropwise to a mixed solution consisting of 80ml of absolute ethanol, 20ml of glacial acetic acid and 20ml of deionized water, while adding While stirring, continue to stir at room temperature after the dropwise addition until the solution appears light blue, and a titanium dioxide sol is prepared.
[0064] S2. Adding siloxane into the titanium dioxide sol for reaction to obtain a modified titanium dioxide sol.
[0065] 6 ml of hexadecyltrimethoxysilane was added dropwise into the titanium dioxide sol, and stirred and reacted at 30° C. for 6 hours to obtain a m...
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