Preparation method of tungsten-nickel-iron alloy material

A tungsten-nickel-iron alloy and mixed powder technology, applied in the field of alloys, can solve problems such as low processing yield, achieve the effects of realizing environmental protection production, reducing exhaust gas emissions, and improving pressing efficiency

Inactive Publication Date: 2020-08-04
无锡乐普金属科技有限公司
View PDF8 Cites 0 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] Aiming at the problems in the prior art, the present invention provides a preparation method of tungsten-nickel-iron alloy material, which solves the problem of low processing yield in the existing process, and uses the staggered layer filling and pressing method of the porous plate to fill the gaps to achieve lifting and pressing Efficiency, effectively reduces the difficulty of pressing, and does not require the use of molding agents

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0022] A preparation method of a tungsten-nickel-iron alloy material, comprising the steps of:

[0023] Step 1, putting tungsten powder, nickel powder and iron powder into a ball mill for wet ball milling, drying to obtain mixed powder;

[0024] Step 2, adding polyvinylpyrrolidone to absolute ethanol, then adding it to the mixed powder, stirring evenly, putting it into a mold and pressing it at a constant temperature to form a pressing plate;

[0025] Step 3, immerse the first pressing plate in absolute ethanol and vibrate with microwave for 2-5 hours, then take it out, wash it with absolute ethanol, and dry it to obtain a porous plate;

[0026] Step 4, hydraulically pressing several porous plates to form a green body, and then putting the green body into a sintering furnace for liquid phase sintering to obtain a prefabricated alloy plate;

[0027] Step 5, spraying the mixed powder on the surface of the prefabricated alloy plate, spraying the surface for 10-20 minutes after t...

Embodiment 2

[0035] A preparation method of a tungsten-nickel-iron alloy material, comprising the steps of:

[0036] Step 1, putting tungsten powder, nickel powder and iron powder into a ball mill for wet ball milling, drying to obtain mixed powder;

[0037] Step 2, adding polyvinylpyrrolidone to absolute ethanol, then adding it to the mixed powder, stirring evenly, putting it into a mold and pressing it at a constant temperature to form a pressing plate;

[0038] Step 3, immerse the first pressing plate in absolute ethanol and vibrate with microwave for 2-5 hours, then take it out, wash it with absolute ethanol, and dry it to obtain a porous plate;

[0039] Step 4, hydraulically pressing several porous plates to form a green body, and then putting the green body into a sintering furnace for liquid phase sintering to obtain a prefabricated alloy plate;

[0040]Step 5, spraying the mixed powder on the surface of the prefabricated alloy plate, spraying the surface for 10-20 minutes after th...

Embodiment 3

[0048] A preparation method of a tungsten-nickel-iron alloy material, comprising the steps of:

[0049] Step 1, putting tungsten powder, nickel powder and iron powder into a ball mill for wet ball milling, drying to obtain mixed powder;

[0050] Step 2, adding polyvinylpyrrolidone to absolute ethanol, then adding it to the mixed powder, stirring evenly, putting it into a mold and pressing it at a constant temperature to form a pressing plate;

[0051] Step 3, immerse the first pressing plate in absolute ethanol and vibrate with microwave for 2-5 hours, then take it out, wash it with absolute ethanol, and dry it to obtain a porous plate;

[0052] Step 4, hydraulically pressing several porous plates to form a green body, and then putting the green body into a sintering furnace for liquid phase sintering to obtain a prefabricated alloy plate;

[0053] Step 5, spraying the mixed powder on the surface of the prefabricated alloy plate, spraying the surface for 10-20 minutes after t...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

PUM

No PUM Login to view more

Abstract

The invention discloses a preparation method of a tungsten-nickel-iron alloy material. The preparation method comprises the following steps: putting tungsten powder, nickel powder and iron powder intoa ball mill, carrying out wet ball milling, and carrying out drying to obtain mixed powder; adding polyvinylpyrrolidone into absolute ethyl alcohol, then adding the product into the mixed powder, carrying out uniform stirring, putting the mixture into a mold, and carrying out pressing at a constant temperature to form pressing plates; soaking the first pressing plates in absolute ethyl alcohol, carrying out microwave vibration for 2-5 h, then taking out the first pressing plates, washing the first pressing plates with absolute ethyl alcohol, and carrying out drying to obtain porous plates; carrying out oil pressure pressing on a plurality of porous plates, thus a green body is formed, placing the green body into a sintering furnace for liquid-phase sintering, and thus a prefabricated alloy plate is obtained; and spraying the mixed powder on the surface of the prefabricated alloy plate, carrying out rolling pressing treatment, carrying out surface flame spraying treatment for 10-20 min, so that a rough alloy plate is obtained, and carrying out polishing to obtain the tungsten-nickel-iron alloy plate. With the preparation method, the problem of low processing yield in the prior artis solved, by utilizing a layer-staggered filling pressing method of the porous plates, the pressing efficiency is improved, the pressing difficulty is effectively reduced, and meanwhile, a forming agent is not needed.

Description

technical field [0001] The invention belongs to the field of alloys, and in particular relates to a preparation method of a tungsten-nickel-iron alloy material. Background technique [0002] Tungsten-nickel-iron alloy is an alloy composed of tungsten as the matrix (the tungsten content is 85%-98%), and a small amount of Ni and Fe are added. Its density is as high as 16.5-19.0g / cm 3 , Also known as heavy alloys or high-density alloys. Tungsten-nickel-iron alloy has a series of excellent physical and mechanical properties and serviceability such as high density, high strength and hardness, good electrical conductivity and thermal conductivity, small thermal expansion coefficient, good corrosion resistance and oxidation resistance, good machinability and weldability, etc. Therefore, tungsten-nickel-iron alloy has been widely used in national defense industry and civilian industry, especially W-Ni-Fe alloy is used as a strong damage warhead material in the national defense indu...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

Application Information

Patent Timeline
no application Login to view more
IPC IPC(8): B22F7/02B22F5/00B22F3/11B22F3/02B22F3/10B22F3/24C22C27/04
CPCB22F3/02B22F3/1035B22F3/114B22F3/24B22F5/00B22F7/02B22F2998/10C22C27/04
Inventor 陈永明钟剑锋
Owner 无锡乐普金属科技有限公司
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Try Eureka
PatSnap group products