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A wetting gradient honeycomb structure fiber membrane for medical protection and its preparation method

A technology of honeycomb structure and fiber membrane, which is applied in fiber processing, textiles and papermaking, coating, etc., can solve the problems of ignoring the reverse osmotic pressure of materials, difficulty in meeting the actual application requirements in the protection field, and fiber blocking capillary channels, etc., to achieve branch Enhanced chemical reaction, increased electrostatic repulsion, and strong controllability

Active Publication Date: 2021-09-17
DONGHUA UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] However, the above materials focus on improving their unidirectional moisture transfer performance, ignoring the reverse osmotic pressure of the material, and the thickness of the fiber membrane is generally <0.5mm. In the case of a lot of sweating, the fiber is easy to absorb water and swell to block the capillary channels, which is difficult to meet the practical application in the field of protection. need

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0048] A method for preparing a wetting gradient honeycomb structure fiber membrane for medical protection, the steps are as follows:

[0049] (1) Electrospinning the spinning solution I composed of hydrophilic polymer, nano-scale metal-organic framework, crosslinking agent I and solvent I, and using the insulating material that has been decharged as the receiving substrate to prepare Obtain a hydrophilic type honeycomb structure fiber membrane;

[0050] The preparation process of spinning solution I is as follows: firstly add the metal-organic framework to the solvent I, and after ultrasonic dispersion for 3 hours, then add the hydrophilic polymer and cross-linking agent I, and continuously stir for 12 hours at room temperature with a magnetic stirring device ;

[0051] In the spinning solution I, the mass content of the hydrophilic polymer is 5%, the mass content of the metal-organic framework is 20%, and the mass content of the crosslinking agent I is 2.5%;

[0052] The h...

Embodiment 2

[0075] A method for preparing a wetting gradient honeycomb structure fiber membrane for medical protection, the steps are as follows:

[0076] (1) Electrospinning the spinning solution I composed of hydrophilic polymer, nano-scale metal-organic framework, crosslinking agent I and solvent I, and using the insulating material that has been decharged as the receiving substrate to prepare Obtain a hydrophilic type honeycomb structure fiber membrane;

[0077] The preparation process of spinning solution I is as follows: firstly add the metal-organic framework to the solvent I, after ultrasonic dispersion for 4 hours, then add the hydrophilic polymer and cross-linking agent I, and continuously stir with a magnetic stirring device for 24 hours at room temperature ;

[0078] In the spinning solution I, the mass content of the hydrophilic polymer is 8%, the mass content of the metal-organic framework is 24%, and the mass content of the crosslinking agent I is 5%;

[0079] The hydroph...

Embodiment 3

[0102]A method for preparing a wetting gradient honeycomb structure fiber membrane for medical protection, the steps are as follows:

[0103] (1) Electrospinning the spinning solution I composed of hydrophilic polymer, nano-scale metal-organic framework, crosslinking agent I and solvent I, and using the insulating material that has been decharged as the receiving substrate to prepare Obtain a hydrophilic type honeycomb structure fiber membrane;

[0104] The preparation process of spinning solution I is as follows: firstly add the metal-organic framework to the solvent I, after ultrasonic dispersion for 3 hours, then add the hydrophilic polymer and cross-linking agent I, and continuously stir with a magnetic stirring device at 60°C 18h;

[0105] In the spinning solution I, the mass content of the hydrophilic polymer is 6%, the mass content of the metal-organic framework is 24%, and the mass content of the crosslinking agent I is 3%;

[0106] The hydrophilic polymer is polyacr...

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PUM

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Abstract

The invention relates to a wetting gradient honeycomb structure fiber membrane for medical protection and a preparation method thereof. Spinning solution I is electrospun, and the insulating material that has been treated with decharge is used as the receiving substrate to obtain film I, and then the spinning solution II composed of intermediate polymer, crosslinking agent II and solvent II is subjected to electrospinning , and film I was used as the receiving substrate to prepare film II, and then the spinning solution III composed of hydrophobic polymer, crosslinking agent III and solvent III was electrospun, and film II was used as the receiving substrate to prepare The membrane III is obtained, and the composite fiber membrane is obtained, and finally the composite fiber membrane is heat-treated to obtain the wetting gradient honeycomb structure fiber membrane for medical and health protection; the final membrane has a three-layer composite structure, and the microscopically has a three-dimensional honeycomb-like interconnected pore structure , One-way moisture transfer performance and reverse barrier liquid penetration performance is excellent.

Description

technical field [0001] The invention belongs to the technical field of electrospinning functional fiber materials, and relates to a wetting gradient honeycomb structure fiber membrane for medical protection and a preparation method thereof. Background technique [0002] With the development of science and technology and the improvement of hygiene level, people have higher and higher requirements for the safety, comfort and protection of clothing fabrics. In some cases, it is necessary to use protective clothing to avoid or reduce the damage of toxic and harmful substances in the environment to the human body. For example, medical protective clothing is used to prevent external blood splashes and protect medical staff from infectious substances such as viruses. However, the existing medical protective materials are usually unable to take into account the high-efficiency safety protection and moisture absorption and perspiration performance. Commonly used protective materials ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): D04H1/728D01D5/00D04H1/559D04H3/02D04H3/14D04H13/00
CPCD01D5/003D01D5/0084D04H1/559D04H1/728D04H3/02D04H3/14D04H13/00D10B2509/00
Inventor 丁彬王先锋张宇菲林燕燕俞建勇
Owner DONGHUA UNIV
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