12results about How to "Achieving controllable equipment" patented technology

This invention discloses a method for controllable preparation of nanoparticles using a multi-channel microreactor. The method utilizes a microchannel reactor to segment droplets and prepare quantitatively synthesized nanoparticles with controllable particle size. The invention employs capillary action to draw the reaction solution into the microchannel, segmenting one or more droplets (each droplet into 10-100 portions). By changing the width of the microchannel, controllable preparation of nanoparticles within a small range (±3 nm) can be achieved; by changing the length of the microchannel, controllable preparation of nanoparticles within a large range (±10-30 nm) can be achieved. Furthermore, the reactor structure of this invention is simple, enabling highly precise and quantitative synthesis of various nanoparticles. Compared to large-scale reactors, the miniaturization of the synthesis reaction in this invention effectively reduces energy waste and safety hazards, making it highly valuable for applications in safe chemical engineering, green chemical engineering, high-efficiency chemical engineering, microchemical engineering, and precise reaction monitoring.

This invention discloses a method for preparing a laser-clad anti-sticking steel coating on the surface of a vertical roller, comprising: accurately quantifying the surface morphology and laser process parameters of the anti-sticking steel coating on the vertical roller, namely, forming a heat dissipation channel size control equation based on a Gaussian heat source model and an elliptical double-beta spray gun model, and determining the corresponding cladding process parameters according to the dimensional parameters of the coating's relevant service performance requirements, thereby achieving controllable preparation of the spiral anti-sticking steel coating. This invention, through effective control of the coating's spiral diameter and the size and shape of protrusions and grooves, ensures the coating's high-temperature wear resistance while reducing friction between the steel pipe and the vertical roller, preventing steel sticking and extending the service life of the vertical roller.

The application provides a wurtzite boron nitride / diamond composite material and a preparation method and application thereof. The composite material is composed of two phases of wurtzite boron nitride and diamond, and has a stacked sandwich microstructure, which comprises at least one first wurtzite boron nitride layer composed of wurtzite boron nitride, at least one second wurtzite boron nitride layer composed of wurtzite boron nitride, and a diamond layer composed of diamond and sandwiched between the first wurtzite boron nitride layer and the second wurtzite boron nitride layer. The wurtzite boron nitride is a metastable phase stably existing under normal pressure, and the Vickers hardness of the composite material is greater than 50 GPa. The novel wurtzite boron nitride / diamond composite material has high hardness, high toughness and high thermal stability, and the preparation method has low starting material price and simple preparation process.

The application discloses a method for controllable preparation of nanoscale calcium carbonate by taking regenerated micro powder as a calcium source, and comprises the following steps: taking the regenerated micro powder obtained by treating the hydrated cement-based material as the calcium source, dispersing the regenerated micro powder in deionized water or a water solution containing magnesium ions to form a reaction system, performing a wet carbonation reaction by introducing carbon dioxide gas into the reaction system, and realizing the regulation of the crystal form and particle size of the obtained calcium carbonate product by synergistically regulating the process parameters such as the composition of the reaction medium, the reaction temperature, the reaction time, the carbon dioxide flow rate and the stirring speed, so as to prepare nanoscale calcite crystal calcium carbonate or nanoscale calcite / aragonite composite crystal calcium carbonate.

A high-transparency, energy-saving LOW-E glass and its preparation method are disclosed, belonging to the field of LOW-E glass technology. The high-transparency, energy-saving LOW-E glass includes a glass substrate and a composite film layer sequentially deposited thereon. The composite film layer includes a bottom layer, a functional layer, and a protective layer. The bottom layer is an antimony-doped silicon dioxide layer with a gradient doping structure, wherein the doping concentration gradually decreases from bottom to top along the thickness direction. The functional layer includes a first functional sublayer and a second functional sublayer. The first functional sublayer is a fluorine-doped tin oxide layer, and the second functional sublayer is a titanium-doped zinc oxide layer, with a compositional gradient transition region formed between the first and second functional sublayers. The protective layer is a silicon nitride layer. The high-transparency, energy-saving LOW-E glass of this invention has high light transmittance, excellent thermal insulation performance, good chemical stability, and can undergo subsequent deep processing.

The application discloses a preparation method of gamma-phase germanium selenide nanosheets. The application realizes controllable preparation of high-quality gamma-phase germanium selenide nanosheets by adopting a normal-pressure vapor deposition method and based on a rapid cooling strategy. The application realizes controllable growth of gamma-phase germanium selenide nanosheets with different lateral sizes by controlling growth temperature. The application does not need to plate a catalyst such as gold on a substrate surface, and the preparation process is relatively simple. The prepared gamma-phase germanium selenide nanosheets have great application potential in flexible sensors, photoelectric devices, especially near-infrared photoelectric detectors and the like. The gamma-phase germanium selenide nanosheets prepared by the application are still very stable after being placed in air for half a year, and also provide a good experimental platform for subsequent physical property research on the material.

This invention discloses a method for preparing an ultrathin ordered macrocyclic molecular membrane. The method involves synthesizing macrocyclic molecules with high polymerization activity and amphiphilic guest molecules. The inclusion complexes formed by the macrocyclic molecules and guest molecules are orderedly assembled using Langmuir-Blodgett (LB) technology. Photopolymerization is then employed to achieve ordered cross-linking of the macrocyclic molecules, resulting in an ultrathin ordered macrocyclic molecular membrane. The macrocyclic molecular membrane prepared by this invention is monomolecular in thickness and possesses good mechanical strength. With the assisted orientation of the amphiphilic guest molecules, the macrocyclic molecules achieve ordered assembly at the water-air interface. The membrane preparation process proposed in this invention is simple, cost-effective, versatile, and easily scalable, making it significant for the field of high-performance separation membranes.

This invention provides a method and application for the controllable recovery of a specific cobalt-nickel ratio product from a cobalt-nickel mixed solution. The method includes the following steps: adding a complexing agent to the cobalt-nickel mixed solution and adjusting the pH of the solution to acidic, thus obtaining an electrolyte; using the electrolyte as the working electrolyte in an electrodeposition system, performing an electrodeposition reaction under constant potential conditions, causing the specific cobalt-nickel ratio product to deposit on the cathode surface; wherein the cobalt-nickel mixed solution contains cobalt ions and nickel ions. The recovery method of this invention is simple in procedure, reduces production costs, improves recovery efficiency and environmental friendliness, and has good prospects for industrial application.

This invention belongs to the field of electronic component technology, and discloses a SnTe material for a nitrogen dioxide gas sensor, its preparation process, and its application. The SnTe material is synthesized via a solvothermal method. The nitrogen dioxide gas sensor mainly consists of a gas-sensitive material and gold interdigitated electrodes. The gas-sensitive material is coated on the surface of the gold interdigitated electrodes with a coating thickness of approximately 15mm to 75mm. The gas-sensitive material is SnTe. This invention provides a simple, low-cost, safe, and controllable TMDC nanomaterial preparation scheme. Using ethanolamine as a solvent and coordinating agent, and potassium hydroxide aqueous solution as a tellurium source activator, this invention synthesizes SnTe nanomaterials in one step via a solvothermal method. The SnTe nanomaterials prepared by this invention achieve a small nanoscale size. A large number of small-sized nanomaterials can effectively increase the sufficient contact between the material and gas molecules, improving the residence rate of gas molecules on the nanomaterial surface.

The application discloses a kind of modular hydrogel based on liquid shaping technology, preparation method and application thereof.The method first utilizes the plasticity of liquid rubber clay, and obtains the temporary mold of specific shape by pressing or cutting, which is composed of micro-nano particle shell;The mixture containing photosensitive hydrogel precursor, nanoclay and functional factor is injected into the mold and light-cured to form a hydrogel module;Optionally, after removing the particle mold, a functionalized hydrogel module with specific morphology, non-adhesion to the substrate and adjustable mechanical properties is obtained;Finally, different functional modules are bonded and cured by hydrogel precursor to integrate into a modular hydrogel with spatial heterostructure.The application uses micro-nano particle shell as a shapeable and removable temporary mold, realizes the adjustable design of hydrogel macroscopic morphology, mechanical properties and spatiotemporal sequence of drug release, and has wide application prospect in the field of tissue engineering and regenerative medicine.

The invention belongs to the technical field of nano material preparation, and particularly relates to a method for preparing a few-atomic-layer ultrathin SnSe nanosheet based on an intercalation compound precursor. The invention discloses a method for preparing a low-atomic-layer ultra-thin (lt; lt) material by taking ethanolamine as an intercalator based on an intercalation-de-intercalation strategy. According to the method, ethanol amine is used as an intercalator through a hydrothermal method, an ethanol amine intercalated SnSe hybrid precursor is firstly synthesized, then the ultrathin SnSe nanosheet is obtained through deintercalation treatment, the thickness of the prepared nanosheet can reach the atomic level (about 2-3 atomic layers), and the method is simple in process, low in cost, high in product quality and suitable for industrial production. The problems that an existing process is complex, and product size and thickness are difficult to control are solved. In addition, the ultrathin SnSe nanosheet prepared by the method shows excellent application prospects in the fields of piezoelectric devices, photoelectric detection, flexible electronics, energy conversion and the like.

The application discloses a kind of micro-jet continuous preparation methods of micro-pleated spherical silver powder, to solve the problem that traditional stirring reaction method is difficult to continuously prepare high sphericity, high dispersibility and surface has regular micro-pleated structure silver powder using micro-jet mixing reaction mode.The method comprises: configuration and filtration silver precursor and reducing agent solution;Temperature is controlled to 15-35 DEG C respectively;Two solutions are pumped into Y type micro-jet reactor with flow ratio 1:1 by metering pump, and high-speed collision mixing is formed at a certain flow and angle at the reactor outlet, efficient mixing and reaction are realized;Add total addition amount is 1% of silver nitrate weight Gelatin and stearic acid as dispersion stabilizer to inhibit agglomeration and control wrinkle morphology;After suction filtration, washing and vacuum drying, the product is obtained.By using the above technical scheme, continuous, high-stability preparation of micro-pleated high-sphericity silver powder can be realized, and the process method is easy to expand production by modularization.