The invention belongs to the technical field of rubber additives, and particularly discloses a preparation method and application of
cationic polymerization resin with an adjustable
softening point, and the preparation method comprises the following steps: adding a
solvent and a catalyst into a reaction kettle, and adding a
monomer into a high-position dropwise adding tank; cooling the
solvent in the reaction kettle to a specified temperature, setting the dropping speed according to the
softening point requirement of the target
polymer, and starting to drop the overhead tank
monomer; along with continuous dropwise adding of the
monomer, the
viscosity of the
system is gradually increased, the
viscosity is monitored on line, when the
viscosity of the
system reaches 150CP, the monomer is continuously dropwise added, meanwhile, the viscosity of the
system is controlled to be 150-400CP, when the viscosity is greater than 400CP, the
solvent is automatically replenished in the system to dilute the reaction liquid, the
softening point of the resin is regulated and controlled by controlling the viscosity of the system to be 150-400CP, and the temperature fluctuation range in the whole dropwise adding process is + / -5 DEG C; the heat preservation temperature is consistent with the dropwise adding temperature, reacting for 6-10 hours, and then desolventizing and granulating. The regulation and control method and the control mechanism of the
softening point of the resin in the
polymerization stage are defined, so that the resin with the adjustable and controllable
softening point is produced through
process control.