The invention relates to the technical field of magnetic nano-material preparation, in particular to a preparation method of a
magnetic composite nano-material. The method comprises the preparation processes of Fe3O4
magnetic nanoparticles and Fe3O4@mSiO2 composite
magnetic nanoparticles, and specifically adopts a solvothermal method, namely, after
ferric trichloride is dissolved in
ethylene glycol, reaction is carried out in a high-pressure reaction kettle to obtain Fe3O4
magnetic nanoparticles, and the surfaces of the Fe3O4 magnetic nanoparticles are coated with a SiO2 shell layer. Accordingto the
magnetic composite nano material prepared by the method, not only the
chemical stability of Fe3O4 magnetic nanoparticles is enhanced, the
biocompatibility of the composite magnetic nanoparticles is also improved; and the application of the prepared
magnetic composite nano material can be realized only through adsorption which is low in cost, free of by-product generation and easy to operate, and the composite nano material has important significance in investigating
adsorption kinetics of the magnetic composite nano material to
antibiotics in water and researching an efficient removaltechnology of antibiotic residues in water, and has practical value.