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Detection method for simultaneously determining contents of multiple elements in galvanized steel and galvanized steel sheets

A galvanized steel sheet and detection method technology, applied in the preparation of test samples, electrical excitation analysis, material excitation analysis, etc., can solve the problems of unsatisfactory measurement results, long analysis cycle, and various reagents, etc., to reduce the use of chemicals , Sample pre-treatment is simple, solve the effect of long analysis period

Pending Publication Date: 2020-08-28
BENGANG STEEL PLATES
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0003] The traditional chemical wet method can only determine the content of a single element in steel, which has a long analysis period, cumbersome operation steps, various reagents used, and certain pollution to the environment
Routine determination of each element in steel usually uses inductively coupled plasma emission spectrometer, plasma mass spectrometer, infrared carbon-sulfur meter, etc. Usually, the steel sample needs to be broken into chip-like samples and then acid-dissolved for determination, which can analyze single or several elements in steel. Element content, but it is very rare to determine the content of multiple elements at the same time, which cannot meet the fast-paced requirements of modern steelmaking production
The spark direct reading spectrometer can directly measure the bulk sample without crushing and dissolving the sample, but for the thinner galvanized steel plate, the measurement result is not satisfactory

Method used

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  • Detection method for simultaneously determining contents of multiple elements in galvanized steel and galvanized steel sheets
  • Detection method for simultaneously determining contents of multiple elements in galvanized steel and galvanized steel sheets
  • Detection method for simultaneously determining contents of multiple elements in galvanized steel and galvanized steel sheets

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Embodiment

[0029] In the embodiment of the present invention, three pieces of standard substances YSBS11280, YSBS11281 and S9255 with different mass fractions were selected for determination.

[0030] The invention provides a detection method for simultaneous determination of multi-element content in galvanized steel and galvanized steel sheet, comprising the following steps:

[0031] 1) Start the GDS850A glow discharge atomic emission spectrometer and adjust the basic parameters of the GDS850A glow spectrometer: the focal length is 0.75m; the number of grating lines is 2400 / mm; the resolution is 0.025nm; the wavelength is 119-600nm; 58 channels ; The anode diameter is 4mm DC glow discharge source and equipped with 4mm RF glow discharge source; the incident slit is 0.015nm; the exit slit is 0.040nm; the detector is a photomultiplier tube;

[0032] Adjust the discharge parameters of the GDS850A glow discharge atomic emission spectrometer: the anode diameter is 4mm; the analysis work mode ...

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Abstract

The invention provides a detection method for simultaneously determining contents of multiple elements in galvanized steel and galvanized steel sheets. The detection method is characterized by optimizing the working environment, sampling conditions and sample preparation conditions of a glow discharge atomic emission spectrometer, and simultaneously determining the contents of multiple elements ingalvanized steel and galvanized steel sheets on the basis of establishing a standard curve of each element. The detection method has the advantages of short analysis time, simple sample pretreatment,reduction of the use of chemicals, environmental protection and no pollution in the detection process, and simultaneous determination of the contents of multiple elements, and solves the problems oflong analysis period, tedious operation steps, various reagents and certain pollution to the environment in traditional test methods.

Description

technical field [0001] The invention relates to the field of measuring galvanized sheets, in particular to a detection method for simultaneously measuring multi-element contents in galvanized steel and galvanized steel sheets. Background technique [0002] In order to improve the atmospheric corrosion resistance of steel, galvanizing on the surface of the steel plate is the most effective and economical method. The content of alloying elements, trace elements and impurity elements in the substrate of galvanized steel and galvanized steel sheet directly determines the performance of the material, so its composition analysis is an important basic technology to ensure its material. [0003] The traditional chemical wet method can only determine the content of a single element in steel, which has a long analysis period, cumbersome operation steps, various reagents used, and certain pollution to the environment. Routine determination of each element in steel usually uses inducti...

Claims

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Application Information

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IPC IPC(8): G01N1/28G01N21/67
CPCG01N1/28G01N21/67
Inventor 胡维铸陈宇牟英华王伟赵广东杨维秀
Owner BENGANG STEEL PLATES
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