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Water dispersible granule containing solid dispersing agent, and preparation method thereof

A technology of solid dispersant and dispersing granules, applied in the fields of botanical equipment and methods, biocides, fungicides, etc., can solve the problems of poor disintegration and dispersing ability and poor stability of water-dispersible granules, and achieve excellent disintegration and dispersion. The effect of capability and stability, low cost, low cost of use

Inactive Publication Date: 2020-09-15
NANJING WELL BIOCHEM
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] The main purpose of the present invention is to overcome the defects of poor disintegration and dispersibility and poor stability of existing water-dispersible granules, and to provide a water-dispersible granule containing a solid dispersant and a preparation method thereof

Method used

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  • Water dispersible granule containing solid dispersing agent, and preparation method thereof
  • Water dispersible granule containing solid dispersing agent, and preparation method thereof
  • Water dispersible granule containing solid dispersing agent, and preparation method thereof

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preparation example Construction

[0040] According to the method for preparing water-dispersible granules containing a solid dispersant according to the present invention, the method comprises the following steps: (1) preparing a solid dispersant; (2) dispersing the solid prepared in the above step (1) The agent is mixed with the original drug of captan, solid wetting agent and auxiliary materials according to the weight ratio of (2-8):80:(3-7):(5-15), and then extruded and granulated to obtain the solid Water-dispersible granules of dispersants.

[0041] According to the solid dispersant of the present invention, it is prepared according to the following steps: a. Mix fumed silicon dioxide and hexamethylene diisocyanate, then add solvent and catalyst, and react by ball milling for 3 to 5 hours to obtain silicon dioxide / hexamethylene diisocyanate hybrid particles; b. Add fatty alcohol polyoxyethylene ether to the silicon dioxide / hexamethylene diisocyanate hybrid particles obtained above, and add catalyst for ...

Embodiment 1

[0048] Prepare solid dispersant: 100g fumed silica (particle size is 7nm) and 100g hexamethylene diisocyanate are added in planetary ball milling device, then add 500g xylene as solvent and 0.1g stannous octoate as catalyst, ball mill After reacting for 4 hours, silica / hexamethylene diisocyanate hybrid particles were obtained. Add 200g of polyoxyethylene lauryl ether (15EO) to the obtained silica / hexamethylene diisocyanate hybrid particles, add stannous octoate for ball milling reaction for 4 hours, heat up to 70°C, and remove the solvent in vacuo After toluene, add water to dissolve the product to remove unreacted isocyanate groups, and finally dry it by spraying powder to obtain a solid dispersion.

[0049] Preparation of water-dispersible granules: according to 100 parts of total weight, 80 parts of captan former medicine, 5 parts of solid dispersant, 5 parts of solid wetting agent WS-EFW, 10 parts of auxiliary materials (5 parts of gypsum, 1 part of starch, urea 4 parts),...

Embodiment 2

[0051] Prepare solid dispersant: 100g fumed silica (particle size is 7nm) and 90g hexamethylene diisocyanate are added in planetary ball milling device, then add 600g xylene as solvent and 0.1g stannous octoate as catalyst, ball mill After reacting for 5 hours, silica / hexamethylene diisocyanate hybrid particles were obtained. Add 300g tetradecyl polyoxyethylene ether (20EO) to the obtained silica / hexamethylene diisocyanate hybrid particles, add stannous octoate for ball milling reaction for 4 hours, heat up to 60°C, and remove the solvent in vacuo After toluene, add water to dissolve the product to remove unreacted isocyanate groups, and finally dry it by spraying powder to obtain a solid dispersion.

[0052] Preparation of water-dispersible granules: according to 100 parts of total parts, 80 parts of captan former medicine, 5 parts of solid dispersant, 5 parts of solid wetting agent WS-EFW, 10 parts of auxiliary materials (3 parts of kaolin, carboxymethyl cellulose 1 part of...

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Abstract

The invention discloses a water dispersible granule containing a solid dispersing agent, and a preparation method thereof. The dispersible granule is prepared from, by weight, 80% of captan raw medicine, 2-8% of the solid dispersing agent, 3-7% of a solid wetting agent and 5-15% of an auxiliary material. The silicon dioxide-based solid dispersing agent is obtained by modifying the surface of an inorganic material nanometer silicon dioxide with an organic compound, and when the solid dispersing agent is used in water dispersible granule, the disintegration and dispersion capacity of the water dispersible granule can be greatly improved, and the stability of a dispersed suspension is improved.

Description

technical field [0001] The invention relates to the technical field of pesticide preparations, in particular to a water-dispersible granule containing a solid dispersant and a preparation method thereof. Background technique [0002] Water-dispersible granules are new pesticide preparations developed in the early 1980s. They are granulated with natural or synthetic carriers and suitable auxiliaries through special processes. Water-dispersible granules are granular preparations that can disintegrate and disperse quickly when placed in water to form a high-suspension solid-liquid dispersion system. Water-dispersible granules are one of the fastest-growing formulations in recent years, and may become one of the main pesticide formulations in the future. Water-dispersible granules are pesticide formulations that are dry, dust-free, free-flowing, and easy to diffuse in water. The international code is WG. WG mainly has the following advantages: 1) Easy to use; 2) No packaging p...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A01N25/14A01N47/04A01P3/00
CPCA01N25/14A01N47/04
Inventor 刘畅张明沈德方潘超
Owner NANJING WELL BIOCHEM