New application of lentinan extract and skin care composition with anti-smog effect and preparation method thereof
A technology of skin care composition and lentinan, which is applied in the direction of toiletry preparations, skin care preparations, pharmaceutical formulations, etc., can solve the problem of affecting product quality, stability cannot meet the high stability requirements of skin care products, precipitation turbidity and discoloration, etc. problem, to achieve good filtering effect, maintain long-term stable effect, and good stability
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Embodiment 1
[0076] Embodiment 1 Lentinan extract preparation
[0077] (1) Pretreatment: Dried shiitake mushrooms were dried at 50°C, pulverized by a pulverizer, and passed through a 1.5mm aperture screen at 120°C in an anhydrous state, 0.10MPa high temperature and high pressure treatment for 0.5h;
[0078] (2) Extraction: add water to the pretreated raw material for water extraction, the material-liquid ratio m / m is 1:60, and extract at 70°C for 3 hours;
[0079] (3) Coarse filtration: adopt plate and frame filtration equipped with 15 μm aperture filter paper to realize solid-liquid separation, collect the filtrate, and obtain the coarse filtrate;
[0080] (4) Decolorization: add activated carbon with a mass percentage of 1.0% to the crude filtrate, decolorize at 80° C. for 1 h, filter with a plate frame equipped with a 0.3 μm aperture filter paper plate, realize solid-liquid separation, collect the filtrate, and obtain the decolorization filtrate;
[0081] (5) Membrane concentration: th...
Embodiment 2
[0084] Example 2 Preparation of Lentinan Extract
[0085] (1) Pretreatment: dried shiitake mushrooms were dried at 60°C, pulverized by a pulverizer, passed through a sieve with a pore size of 1mm, and then treated under high temperature and high pressure at 125°C and 0.14 MPa in an anhydrous state for 1 hour;
[0086] (2) Extraction: add water to the pretreated raw material for water extraction, the solid-liquid ratio m / m is 1:100, and extract at 95°C for 1 hour;
[0087] (3) Coarse filtration: adopt plate and frame filtration equipped with 20 μm pore diameter filter paper board to realize solid-liquid separation, collect the filtrate, and obtain the coarse filtrate;
[0088] (4) Decolorization: Add 0.5% activated carbon to the crude filtrate, decolorize at 95°C for 0.5h, filter with a plate frame equipped with a filter paper plate with a pore size of 0.4 μm, realize solid-liquid separation, collect the filtrate, and obtain the decolorization filtrate;
[0089] (5) Membrane c...
Embodiment 3
[0092] Embodiment 3 Lentinan extract preparation
[0093] (1) Pretreatment: Dried shiitake mushrooms were dried at 70°C, pulverized by a pulverizer, passed through a sieve with an aperture of 0.5mm, and treated at 121°C and 0.10MPa in an anhydrous state for 2 hours under high temperature and high pressure;
[0094] (2) Extraction: add water to the pretreated raw material for water extraction, the material-liquid ratio m / m is 1:20, and extract at 100°C for 5 hours;
[0095] (3) Coarse filtration: adopt plate and frame filtration equipped with 25 μm aperture filter paper to realize solid-liquid separation, collect the filtrate, and obtain the coarse filtrate;
[0096] (4) Decolorization: add activated carbon with a mass percentage of 3.0% to the crude filtrate, decolorize at 70°C for 0.5h, filter with a plate frame equipped with a filter paper plate with a pore size of 0.5 μm, realize solid-liquid separation, collect the filtrate, and obtain the decolorization filtrate;
[0097...
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