Oyster fibers

A technology of fiber and oyster shell powder, applied in the field of textile fibers, can solve the problems of restricting the general popularization and application of calcium carbonate, and achieve the effects of large popularization and application potential, alleviation of processing pressure, high strength and toughness

Pending Publication Date: 2020-11-27
爱可比(苏州)新材料有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Different forms of calcium carbonate are suitable for different application scenarios due to the differences in their properties. However, in nature, many biomass raw materials often contain different forms of calcium carbonate. Generally speaking, it

Method used

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  • Oyster fibers

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Experimental program
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Embodiment 1

[0019] In this embodiment, polyamide resin is used as the polyester in the raw material, and methyl ethyl ketone is used as the dispersant, but in other embodiments, other types of polyester can be used according to actual conditions, and other volatile alcohols can be used , ketones, or aromatic compounds as dispersants, not limited to the use of polyamide resin as the polyester in the raw material or the use of butanone as the dispersant.

[0020] 1. Pretreatment steps of oyster shells

[0021] The oyster shells are cleaned, calcined at high temperature, cooled, and pulverized to obtain oyster shell powder.

[0022] 2. Ingredients

[0023] Accurately weigh 3 parts of oyster shell powder, 97 parts of polyamide resin, and 0.15 parts of glycine.

[0024] 3. Preparation of Oyster Fiber

[0025] Step 1: Dissolving oyster shell powder and chitosan in aqueous acetic acid to form a reaction solution with a chitosan concentration of 0.4 g / mL;

[0026] Step 2: adding urea to the r...

Embodiment 2

[0032] In this embodiment, polyamide resin is used as the polyester in the raw material, and methyl ethyl ketone is used as the dispersant, but in other embodiments, other types of polyesters can be used according to actual conditions, and other volatile alcohols, Ketones, or aromatic compounds, etc. are used as dispersants, and are not limited to the use of polyamide resin as the polyester in the raw material or the use of methyl ethyl ketone as the dispersant.

[0033] 1. Pretreatment steps of oyster shells

[0034] The oyster shells are cleaned, calcined at high temperature, cooled, and pulverized to obtain oyster shell powder.

[0035] 2. Ingredients

[0036] Accurately weigh 3 parts of oyster shell powder, 97 parts of polyamide resin, and 0.15 part of 3-alanine.

[0037] 3. Preparation of Oyster Fiber

[0038] Step 1: Dissolving oyster shell powder and chitosan in aqueous acetic acid to form a reaction solution with a chitosan concentration of 0.4 g / mL;

[0039] Step ...

Embodiment 3

[0045] In this embodiment, polyamide resin is used as the polyester in the raw material, and methyl ethyl ketone is used as the dispersant, but in other embodiments, other types of polyesters can be used according to actual conditions, and other volatile alcohols, Ketones, or aromatic compounds, etc. are used as dispersants, and are not limited to the use of polyamide resin as the polyester in the raw material or the use of methyl ethyl ketone as the dispersant.

[0046] 1. Pretreatment steps of oyster shells

[0047] The oyster shells are cleaned, calcined at high temperature, cooled, and pulverized to obtain oyster shell powder.

[0048] 2. Ingredients

[0049]Accurately weigh 3 parts of oyster shell powder, 97 parts of polyamide resin, and 0.15 parts of 5-aminovaleric acid.

[0050] 3. Preparation of Oyster Fiber

[0051] Step 1: Dissolving oyster shell powder and chitosan in aqueous acetic acid to form a reaction solution with a chitosan concentration of 0.4 g / mL;

[0...

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Abstract

The invention provides oyster fibers. The oyster fibers are prepared by the following steps of 1, dissolving oyster shell powder and chitosan in an acetic acid solution to obtain a reaction solution;2, adding a carbonate supply source substance into the reaction solution, so that the reaction solution is converted into a gelatinous solution; 3, heating the gelatinous solution to 80-120 DEG C, keeping the temperature for 10-15 hours, then adding omega-aminoalkanoic acid, and continuously keeping the temperature for 5-10 hours; step 4, adjusting the pH value of the mixed solution obtained afterthe step 3 is completed to be greater than 7.5, and then adding chloroacetic acid into the mixed solution until the chitosan is converted into carboxymethyl chitosan; 5, adding deionized water, carrying out ultrasonic treatment to fully dissolve the carboxymethyl chitosan, filtering, washing filter residues with the deionized water, filtering out washing liquor, and reserving the filter residuesfor later use; and 6, adding a dispersant into the filter residues, grinding, fully dispersing, fully mixing the ground mixed slurry with polyester, granulating, and spinning to obtain a finished product.

Description

technical field [0001] The invention belongs to the field of textile fibers, and in particular relates to an oyster fiber. Background technique [0002] Adding various inorganic particles is a common method in the modification process of polyester and fiber. By adding different inorganic particles, the modified polyester or fiber will have different functions. Calcium carbonate (CaCO 3 ) polyester made of microparticles, which are characterized by: ① The surface properties of polymer particles are improved, which is convenient for polyester film-forming processing; ② Films made of calcium carbonate modified polyester have higher dielectric properties and can meet Application requirements in some occasions; ③Synthetic fibers made of the modified polyester have improved crystallization and tensile properties under the premise of ensuring fiber gloss; ④Make the surface of the fibers microporous without affecting the strength , so that the fiber has new functions such as mois...

Claims

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Application Information

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IPC IPC(8): D01F8/14D01F8/18C08B37/08
CPCC08B37/003D01F8/14D01F8/18
Inventor 王舟朱庆文李中勇
Owner 爱可比(苏州)新材料有限公司
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