Preparation method of filtering material for mask
A filter material and mask technology, applied in the field of medical materials, can solve problems such as inability to meet demand and general filtration performance, and achieve excellent filtration effect, high filtration efficiency, and reduced expiratory resistance and inhalation resistance.
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[0038] A method for preparing a filter material for a mask, comprising the following steps:
[0039] (1) Preparation of lignin microfibers:
[0040] Mix wood powder and sodium hydroxide solution together, then heat to 90-95°C, heat and stir for 3 hours, filter, remove impurities, and obtain filter pulp;
[0041] Add the filter slurry obtained above into the autoclave, first adjust the pH of the system to 7.0, then add absolute ethanol, stir evenly, then seal the autoclave, adjust the temperature to 145-148°C, and adjust the pressure to 12- 16MPa, stirred and reacted for 2 hours, then released the pressure, cooled naturally to room temperature, and obtained the pretreated slurry;
[0042] Concentrating the pretreated slurry obtained above to one-half of the original volume to obtain a concentrate;
[0043] adding the concentrate to a ball mill for ball milling to obtain a ball mill liquid;
[0044] Vacuum freeze-drying the ball milling solution obtained above to obtain ligni...
Embodiment 1
[0070]A method for preparing a filter material for a mask, comprising the following steps:
[0071] (1) Preparation of lignin microfibers:
[0072] Mix wood flour and sodium hydroxide solution together, then heat to 90°C, heat and stir for 3 hours, filter, remove impurities, and obtain filter slurry; add the filter slurry obtained above into a high-pressure reactor, and adjust the pH of the system to 7.0, then add absolute ethanol, after stirring evenly, then seal the autoclave, adjust the temperature to 145°C, adjust the pressure to 12MPa, stir and react for 2 hours, then release the pressure, naturally cool to room temperature, and obtain the pretreated slurry; Concentrate the pretreatment slurry obtained above to one-half of the original volume to obtain a concentrate; add the concentrate to a ball mill for ball milling to obtain a ball mill liquid; vacuum freeze-dry the ball mill liquid obtained above to obtain wood Plain microfiber; The wood powder is a mixture of paulow...
Embodiment 2
[0079] A method for preparing a filter material for a mask, comprising the following steps:
[0080] (1) Preparation of lignin microfibers:
[0081] Mix wood flour and sodium hydroxide solution together, then heat to 95°C, heat and stir for 3 hours, filter, remove impurities, and obtain filter slurry; add the filter slurry obtained above into a high-pressure reactor, and adjust the pH of the system to 7.0, then add absolute ethanol, after stirring evenly, then seal the autoclave, adjust the temperature to 148°C, adjust the pressure to 16MPa, stir and react for 2 hours, then release the pressure, naturally cool to room temperature, and obtain the pretreatment slurry; Concentrate the pretreatment slurry obtained above to one-half of the original volume to obtain a concentrate; add the concentrate to a ball mill for ball milling to obtain a ball mill liquid; vacuum freeze-dry the ball mill liquid obtained above to obtain wood Plain microfiber; The wood powder is a mixture of pau...
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Abstract
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