Antibacterial and antiviral natural detergent and preparation method thereof

A detergent and anti-virus technology, applied in antibacterial and anti-virus natural detergent and its preparation field, can solve the problems of unsatisfactory pass rate and poor antibacterial effect, and achieve low pollution and easy self-degradation Effect

Inactive Publication Date: 2020-12-29

ZAOZHUANG UNIV +1

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AI-Extracted Technical Summary

Problems solved by technology

The chemical residues in detergent may directly or indirectly affect human health, so it is necessary to develop a low-toxic, effective, non-irritating natural plant-based antibacterial detergent

[0003] The...

Abstract

The invention belongs to the technical field of daily chemical products, and particularly relates to an antibacterial and antiviral natural detergent and a preparation method thereof. The antibacterial and antiviral natural detergent is prepared from the following raw materials: elsholtzia ciliata volatile oil, saponin, sterile water, 24% AES, benzenesulfonic acid, caustic soda, urea, 20% sodium chloride and benzoic acid. According to the invention, the natural detergent is prepared by compounding elsholtzia ciliata and saponin and combining the auxiliary effect of other additives, and is a low-toxicity, effective and non-irritant natural plant type antibacterial liquid detergent. The invention also provides a preparation method of the detergent, and the sterilization effect of the detergent.

Application Domain

Inorganic/elemental detergent compounding agentsBiocide +5

Technology Topic

Anti bacterialElsholtzia ciliata +7

Image

Examples

Experimental program(3)
Comparison scheme(2)

Example Embodiment

[0025]Example 1

[0026]1. Extraction of active ingredients

[0027](1) Extraction of Elsholtzia volatile oil

[0028]Collect the dried whole plant of Elsholtzia elegans, remove dust and wash, dry in shade, chop (less than 2cm), weigh 5 kg, add 8 times the amount of water to soak for 1 h, microwave solid-liquid extraction for 0.5 h, and obtain volatile oil-water emulsion, Add NaCl to saturation, stir and let stand for 24 hours, add ether to extract 3 times, separate the oil layer, and dry with anhydrous sodium sulfate to obtain a light yellow-green transparent oily liquid with special odor. Seal the volatile oil and store at 4°C. For the test.

[0029](2) Extraction of saponin

[0030]Extraction of saponin from Camellia oleifera: Take 1kg of crushed Camellia oleifera seed cake, add 60% ethanol and extract for 2 h at 80°C, filter and concentrate, add organic decolorant, macroporous adsorption resin, 85% ethanol elution , Concentrated and dried to obtain a light yellow oil tea saponin sample.

[0031], Product ingredient preparation

[0032] Component Mass score/% Caustic soda 3.20 Urea 8.00 20% sodium chloride 4.60 benzoic acid 0.06 Volatile oil 2 Saponin 2.24 96% benzenesulfonic acid 6.30 24% AES 13.20 Deionized water margin

[0033]According to the formula above, take 302.00 g of deionized water and 11.2 g of saponin in a 500 mL beaker; put 16.00 g of caustic soda into the water and slowly stir to make it completely dissolved; add 31.50 g of 96% benzenesulfonic acid and stir well , Adjust the pH to between 6.5-7.5; slowly add 24% AES 66.00 g and urea 40.00 g to completely dissolve it; add 0.06 g of benzoic acid and stir evenly; add 10 g of Elsholtzia volatile oil and stir, and finally add 23.00 g of 20% sodium chloride, Shake well while adding, and serve until it is thick.

Example Embodiment

[0034]Example 2

[0035]1. Extraction of active ingredients

[0036](1) Extraction of Elsholtzia volatile oil

[0037]Collect the dried whole plant of Elsholtzia vulgaris, remove dust and wash, dry in shade, chop (less than 3cm), weigh 5 kg, add 8 times the amount of water to soak for 1.5 h, microwave solid-liquid extraction for 1 h, and obtain volatile oil-water emulsion, Add NaCl to saturation, stir and let stand for 24 hours, add ether to extract 3 times, separate the oil layer, and dry with anhydrous sodium sulfate to obtain a light yellow-green transparent oily liquid with special odor. Seal the volatile oil and store at 4°C. For the test.

[0038](2) Extraction of saponin

[0039]Extraction of saponin from Camellia oleifera: Take 1kg of crushed Camellia seed cake, add 60% ethanol and extract for 2.5 h at 80°C, filter and concentrate, add organic decolorizing agent, macroporous adsorption resin, 85% ethanol elution , Concentrated and dried to obtain a light yellow oil tea saponin sample.

[0040], Product ingredient preparation

[0041] Component Mass score/% Caustic soda 1 Urea 5 20% sodium chloride 8 benzoic acid 0.1 Volatile oil 5 Saponin 1 Benzenesulfonic acid 10 24% AES 10 Deionized water margin

[0042]According to the above formula, take 299.50 g of deionized water and 5.00 g of saponin in a 500 mL beaker; put 5.00 g of caustic soda into the water and slowly stir to make it completely dissolved; add 50.00 g of 96% benzenesulfonic acid and stir well , Adjust the pH to between 6.5-7.5; slowly add 24% AES 50.00 g and urea 25.00 g to completely dissolve it; add 0.5 g of benzoic acid and stir evenly; add 25.00 g of Elsholtzia volatile oil and stir, and finally add 20% sodium chloride 40.00 g , Shake well while adding, until the product becomes viscous.

Example Embodiment

[0043]Example 3

[0044]1. Extraction of active ingredients

[0045](1) Extraction of Elsholtzia volatile oil

[0046]Collect the dried whole plant of Elsholtzia elegans, remove dust and wash, dry in shade, chop (less than 2cm), weigh 5 kg, add 8 times the amount of water to soak for 1 h, microwave solid-liquid extraction for 0.5 h, and obtain volatile oil-water emulsion, Add NaCl to saturation, stir and let stand for 24 hours, add ether to extract 3 times, separate the oil layer, and dry with anhydrous sodium sulfate to obtain a light yellow-green transparent oily liquid with special odor. Seal the volatile oil and store at 4°C. For the test.

[0047](2) Extraction of saponin

[0048]Extraction of saponin from Camellia oleifera: Take 1kg of crushed Camellia oleifera seed cake, add 60% ethanol and extract for 3 h at 80°C, filter and concentrate, add organic decolorizing agent, macroporous adsorption resin, 85% ethanol elution , Concentrated and dried to obtain a light yellow oil tea saponin sample.

[0049], Product ingredient preparation

[0050] Component Mass score/% Caustic soda 5 Urea 10 20% sodium chloride 2 benzoic acid 0.01 Volatile oil 1 Saponin 5 96% benzenesulfonic acid 2 24% AES 17 Deionized water margin

[0051]According to the above formula, take 289.95 g of deionized water and 25.00 g of saponin in a 500 mL beaker; put 25.00 g of caustic soda into the water and slowly stir to make it completely dissolved; add 10.00 g of 96% benzenesulfonic acid, and stir well , Adjust the pH to between 6.5-7.5; slowly add 24% AES 85.00 g and urea 50.00 g to completely dissolve; add 0.05 g of benzoic acid and stir evenly; add elm oleracea volatile oil 5.00 g and stir, and finally add 20% sodium chloride 10.00 g , Shake well while adding, until the product becomes viscous.

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Classification and recommendation of technical efficacy words

reduce pollution

Antibacterial and antiviral natural detergent and preparation method thereof

A detergent and anti-virus technology, applied in antibacterial and anti-virus natural detergent and its preparation field, can solve the problems of unsatisfactory pass rate and poor antibacterial effect, and achieve low pollution and easy self-degradation Effect

AI-Extracted Technical Summary

Problems solved by technology

Abstract

Image

Examples

Example Embodiment

Example Embodiment

Example Embodiment

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Description & Claims & Application Information

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