Formaldehyde-removing, corrosion-preventing and environment-friendly agriculture and forestry residue fiberboard and preparation method thereof
A technology of residue and fiberboard, applied in the field of biomass composite decoration materials, can solve the problems of formaldehyde pollution, limited application, easy corruption of soybean protein adhesive, etc., achieve low production cost and expand the application range
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Embodiment 1
[0036] 1) Preparation of agricultural and forestry residues: purchase 50g of branches produced in the process of forest tending and 50g of straw produced in agricultural production according to the process requirements.
[0037]2) Preparation of chitosan nanoparticles: 1 g of chitosan was dissolved in 200 mL of 1% acetic acid solution, and magnetically stirred for 3 hours under a nitrogen atmosphere until a transparent chitosan solution was obtained. At room temperature, the pH value of the chitosan solution was adjusted to 4 with 1 M hydrochloric acid solution, and magnetically stirred at 500 rpm at 70° C. for 7 hours. Dissolve 0.2g of citric acid in 10mL of distilled water, adjust the pH value of the citric acid solution to 4 with a concentration of 1M sodium hydroxide solution, and add the citric acid solution drop by drop to the chitosan solution with a pH value of 4 , the resulting product was centrifuged at 4000 rpm for 40 minutes, and freeze-dried at -50° C. for 36 hour...
Embodiment 2
[0047] 1) Preparation of agricultural and forestry residues: purchase 50g of branches produced in the process of forest tending and 50g of straw produced in agricultural production according to the process requirements.
[0048] 2) Preparation of chitosan nanoparticles: 2 g of chitosan was dissolved in 400 mL of 1% acetic acid solution, and magnetically stirred for 3 hours under a nitrogen atmosphere until a transparent chitosan solution was obtained. At room temperature, the pH value of the chitosan solution was adjusted to 4 with 1 M hydrochloric acid solution, and magnetically stirred at 500 rpm at 70° C. for 7 hours. Dissolve 0.4g citric acid in 20mL distilled water, adjust the pH value of the citric acid solution to 4 with a concentration of 1M sodium hydroxide solution, and add the citric acid solution drop by drop to the chitosan solution with a pH value of 4 , the resulting product was centrifuged at 4000 rpm for 40 minutes, and freeze-dried at -50° C. for 36 hours to ...
Embodiment 3
[0058] 1) Preparation of agricultural and forestry residues: purchase 50g of branches produced in the process of forest tending and 50g of straw produced in agricultural production according to the process requirements.
[0059] 2) Preparation of chitosan nanoparticles: 3 g of chitosan was dissolved in 600 mL of 1% acetic acid solution, and magnetically stirred for 3 hours under a nitrogen atmosphere until a transparent chitosan solution was obtained. At room temperature, the pH value of the chitosan solution was adjusted to 4 with 1 M hydrochloric acid solution, and magnetically stirred at 500 rpm at 70° C. for 7 hours. Dissolve 0.6g of citric acid in 30mL of distilled water, adjust the pH of the citric acid solution to 4 with a concentration of 1M sodium hydroxide solution, and add the citric acid solution drop by drop to the chitosan solution with a pH of 4 , the resulting product was centrifuged at 4000rpm for 40min, and freeze-dried at -50°C for 36 hours to obtain chitosa...
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