A kind of bionic 3D printing aerogel insulation board and preparation method thereof
A thermal insulation board and 3D printing technology, applied in thermal insulation, additive processing, climate change adaptation, etc., can solve the problems of thermal insulation performance and unsatisfactory bulk density of thermal insulation board, and achieve lightweight thermal insulation performance optimization, fast printing, thermal conductivity The effect of coefficient reduction
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Embodiment 1
[0046] A manufacturing method of bionic 3D printing aerogel insulation board, the preparation flow chart is as follows image 3 shown, including the following steps:
[0047] (1) Weigh 20.83g of ethyl orthosilicate, 46.07g of ethanol and 18.02g of deionized water (the molar ratio of ethyl orthosilicate to ethanol and ionized water is 1:10:10), add 1.0415g of polydimethyl methacrylate Siloxane (the mass ratio of ethyl orthosilicate and polydimethylsiloxane is 1:0.05), adjust the pH of the system to 2 with 10% dilute hydrochloric acid, and hydrolyze it at 25°C for 24h to obtain SiO 2 colloidal solution;
[0048] (2) The molar ratio of ammonia water to ethyl orthosilicate is 0.003:1, and the ammonia water is diluted to 2 Equal volume of colloidal solution, SiO before printing 2 The colloidal solution and the dilute ammonia water are respectively transported to the tee pipe through two hoses through the peristaltic pump and mixed to obtain SiO 2 Precursor sol, pH value of mixe...
Embodiment 2
[0055] A method for manufacturing a bionic 3D printed aerogel thermal insulation board, comprising the following steps:
[0056] (1) Weigh 20.83g of ethyl orthosilicate, 23.04g of ethanol and 27.03g of deionized water (the molar ratio of ethyl orthosilicate to ethanol and ionized water is 1:5:15), add 0.8332g of polydimethyl methacrylate Siloxane (the mass ratio of ethyl orthosilicate and polydimethylsiloxane is 1:0.04), adjust the pH value of the system to 2 with 10% dilute hydrochloric acid, and hydrolyze it at 25 ° C for 24 h to obtain SiO 2 colloidal solution;
[0057] (2) The molar ratio of ammonia water to ethyl orthosilicate is 4×10 -3 , the ammonia water was diluted to 2 Equal volume of colloidal solution, SiO before printing 2 The colloidal solution and the dilute ammonia water are respectively transported to the tee pipe through two hoses through the peristaltic pump and mixed to obtain SiO 2 Precursor sol, pH value of mixed system is 6.6, SiO 2 The gel time of ...
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