Compounds for intracellular delivery of molecules
A complex, cargo molecule technology, applied in the field of molecular biology
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Embodiment 1
[0171] Example 1: Evaluation of the endocytic vesicle escape efficiency of the delivery system based on the Split-GFP system
[0172] In the Split-GFP system, the 11 β sheets of GFP are split into large fragments (β1-10) and small fragments (β11), both of which lose their fluorescent activity, but can spontaneously associate and restore GFP if they meet fluorescence properties. Based on this, we constructed HEK293T cells stably expressing Histone-β11, and expressed GFPβ1-10 with nuclear import signal (NLS) as Cargo fusion with the cell-entry delivery system to be evaluated, and then transduced the stable cell line. When the delivery system transduces GFPβ1-10, it can only combine with GFPβ11 to generate complete GFP after successfully escaping from endocytic vesicles and entering the cytoplasm or nucleus. Efficiency is evaluated ( figure 1 ).
[0173] 1.1 Construction of delivery system-GFPβ1-10 protein complex expression vector
[0174] Construct TAT (SEQ ID NO:10), INF7...
Embodiment 2
[0195] Example 2: Application of delivery system in transducing zinc finger protein ZFP
[0196] 2.1 Delivery system-construction of zinc finger protein ZFP9 complex expression vector
[0197] A recombinant protein expression vector containing TAT, INF7, protease cleavage site, and cargo molecule ZFP9 (SEQID NO:27) carrying a nuclear localization signal (NLS) was constructed. The structural schematic diagram of each recombinant protein is as follows Figure 12 As shown, the amino acid sequence of each component is shown in Table 4 below. The construction method is as follows: First, the nucleic acid sequences encoding TAT, INF7, protease cleavage site, and cargo molecule ZFP9 in the delivery system are obtained by PCR amplification, and the various parts are connected through multiple rounds of PCR, and in the last round of PCR In the process, an NdeI restriction site and its overlapping sequence upstream of the NdeI restriction site corresponding to pET-21b(+) were introduce...
Embodiment 3
[0207] Example 3: Application of delivery system in transducin phosphatase Ppm1b
[0208] After TNF-α binds to cell surface receptors, it induces RIP3 phosphorylation and forms a multiprotein complex necrosome (Necrosome). Phosphorylated RIP3 in the necrosome recruits and phosphorylates Mlk1, and the cell enters the necrosis program. During this process, intracellular protein phosphatase 1B (Ppm1b) can dephosphorylate RIP3 to inhibit Necroptosis. In view of the fact that programmed cell necrosis has been found to be closely related to the occurrence of inflammatory diseases, ischemia-reperfusion injury, neurodegenerative diseases and other diseases, Ppm1b protein has shown great potential in the treatment of the above-mentioned diseases related to programmed cell necrosis .
[0209] 3.1 Delivery system-Ppm1b protein complex expression vector construction
[0210] A recombinant protein expression vector containing TAT, INF7, protease cleavage site, and cargo molecule Ppm1b (S...
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