Transparent anti-fog PC resin and preparation method thereof
A resin and transparent technology, which is applied in the field of transparent anti-fog PC resin and its preparation, can solve the problems of not considering the light transmittance, etc., achieve the effect of improving durability and wiping resistance, shortening the processing cycle, and optimizing the processing technology
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Embodiment 1
[0026] A preparation method of transparent anti-fog PC resin, the method comprises the following steps:
[0027] (1) Prepare materials according to the following components and parts by weight:
[0028]
[0029] Among them, the PC resin includes ordinary PC and silicon-containing PC, and the ordinary PC resin is mixed with two PCs with MI(300°C, 1.2kg)=4 and MI(300°C, 1.2kg)=23 according to the mass ratio of 1:1 , the total component is 78 parts, the selected silicon-containing PC is organosiloxane and polycarbonate random copolymerized PC whose refractive index is close to that of ordinary PC, the refractive index of silicon-containing PC is n=1.56, and the silicon content is 7%. The number of copies is 20;
[0030] The antioxidant is a mixture of hindered phenols and phosphites, preferably Irganox 168 and Irganox 1076 from Ciba, and the mixing ratio (mass ratio) is 1:1;
[0031] The lubricant is commercially available PETS;
[0032] The UV stabilizer is a benzotriazole...
Embodiment 2
[0036] A preparation method of transparent anti-fog PC resin, the method comprises the following steps:
[0037] (1) Prepare materials according to the following components and parts by weight:
[0038]
[0039]
[0040] (2) Put the above-mentioned PC resin, antioxidant, lubricant, and UV stabilizer in a high-speed mixer according to the formula ratio and stir them. After mixing evenly, send them into the twin-screw extruder through a metering device. The anti-fog additives are metered It is said to be fed into the extruder from the side feeding port, and the temperature of the twin-screw extruder is controlled at 240-260°C. Under the conveying, shearing and mixing of the screws, the materials are melted and compounded, and then extruded through the die , pulling, cooling, and pelletizing steps to obtain transparent anti-fog PC resin.
[0041] Among them, the common PC resin is mixed with two PCs with MI(300°C, 1.2kg)=4 and MI(300°C, 1.2kg)=23 according to the mass rati...
Embodiment 3
[0047] A preparation method of transparent anti-fog PC resin, the method comprises the following steps:
[0048] (1) Prepare materials according to the following components and parts by weight:
[0049]
[0050] (2) Put the above-mentioned PC resin, antioxidant, lubricant, and UV stabilizer in a high-speed mixer according to the formula ratio and stir them. After mixing evenly, send them into the twin-screw extruder through a metering device. The anti-fog additives are metered It is said to be fed into the extruder from the side feeding port, and the temperature of the twin-screw extruder is controlled at 240-260°C. Under the conveying, shearing and mixing of the screws, the materials are melted and compounded, and then extruded through the die , pulling, cooling, and pelletizing steps to obtain transparent anti-fog PC resin.
[0051] Among them, the common PC resin is mixed with two PCs with MI(300°C, 1.2kg)=4 and MI(300°C, 1.2kg)=23 according to the mass ratio of 1:1, and ...
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