Method for preparing high-content polyphenol compound functional food from fermented hops
A polyphenolic compound and functional food technology, applied in beer fermentation methods, hop treatment, beer brewing, etc., can solve the problems of non-sterilization, difficult filtration, and few research reports on extraction conditions, and achieve the effect of reducing bitterness
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Embodiment 1
[0033] The preparation of polyphenol freeze-dried powder comprises the following steps:
[0034] (1) Select hops: add 10% lactic acid bacteria in the process of fermenting beer, and use the added hops in dry beer production in beer production. Extract the remaining particles after dissolving into beer;
[0035] (2) Squeeze to remove water: the selected hops of step (1) are squeezed to remove water, so that its water content is less than 15%;
[0036] (3) Degreasing: Use petroleum ether to soak and degrease hops with a water content of less than 15%, wherein the volume ratio of petroleum ether to hops is 10:1; the soaking temperature is 60°C, and the soaking time is 6h; after the degreasing is completed, filter the petroleum ether Remove, and the degreasing agent remaining on the hop surface is removed by nitrogen purging;
[0037] (4) Solvent extraction: Use 70% ethanol to extract the degreased hops. The volume ratio of ethanol to hops is 50:1, the extraction temperature is ...
Embodiment 2
[0045] The preparation of described polyphenol freeze-dried powder comprises the following steps:
[0046](1) Select hops: add yeast in the process of fermenting beer, and the remaining waste parts of hops after extracting α-acid or hop oil;
[0047] (2) Squeeze to remove water: the selected hops of step (1) are squeezed to remove water, so that its water content is less than 15%;
[0048] (3) Degreasing: use ether to soak and degrease hops with a water content of less than 15%, wherein the volume ratio of ether to hops is 10:1; the soaking temperature is 60°C, and the soaking time is 6h; after the degreasing ends, the ether is filtered and removed, and Remove the ether remaining on the surface of hops through natural volatilization;
[0049] (4) Solvent extraction: use 60% ethanol to extract the degreased hops, the volume ratio of 60% ethanol to hops is 50:1, the extraction temperature is 70 °C, and the extraction time is 2 hours; repeated extraction 3 times, collect and mi...
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