High-temperature lubricant for thermal simulation experiment and preparation method thereof
A high-temperature lubricant and experimental technology, applied in lubricating compositions, additives, petroleum industry, etc., can solve the problems of affecting the accuracy of measurement, affecting the results of high-temperature experiments, large frictional resistance, etc. Accurate results and the effect of reducing the coefficient of friction
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[0027] The present invention further provides a method for preparing the above-mentioned high-temperature lubricant for thermal simulation experiments, which comprises the following steps:
[0028] A. After mixing 500-700 parts of graphite powder and 100-200 parts of mineral oil, use ultrasonic mixing and dispersion technology for surface pretreatment;
[0029] B. Take 60-80 parts of graphite powder and 100 parts of mineral oil, and mix them evenly to obtain graphite slurry;
[0030] C, the mixture obtained by surface pretreatment in step A is mixed with the graphite slurry obtained in step B after the surface pretreatment, and is dispersed and ground to obtain graphite emulsion;
[0031] D. After the graphite emulsion obtained in step C is mixed with 5-200 parts of nickel powder, microwave treatment is used until the nickel powder in the emulsion is uniformly dispersed, then mixed with 50-100 parts of lithium soap, and ground to obtain a lubricant.
[0032] The method of the...
Embodiment 1
[0038] A. Weigh 500 grams of graphite powder, add the graphite powder to 150g of mineral oil, and apply ultrasonic mixing and dispersion technology at a frequency of 20KHZ to carry out surface pretreatment for 10 minutes;
[0039] B, take by weighing 60 graphite powder, add in 100g mineral oil, make graphite slurry;
[0040] C. Treat the mixture obtained through surface pretreatment in a pressure vessel with a pressure of 10 kg for 5 hours, then add graphite slurry, fully disperse and grind for 5 hours, until the mixture becomes a graphite emulsion;
[0041] D. Add 100 g of nickel powder to the graphite emulsion, and treat it with microwaves at 450 ° C for 15 minutes until the nickel powder in the emulsion is uniformly dispersed, and add 70 g of lithium stearate soap to the emulsion mixture uniformly dispersed with the nickel powder, and continue grinding 3h, the high-temperature lubricant of the present invention can be obtained.
[0042] This high-temperature lubricant is s...
Embodiment 2
[0044] A. Weigh 500g of graphite powder, add graphite powder to 100g of mineral oil, and apply ultrasonic mixing and dispersion technology at a frequency of 20KHZ for surface pretreatment for 10 minutes;
[0045] B, take by weighing 60g graphite powder, add in 100g mineral oil, make graphite slurry;
[0046] C. Treat the mixture obtained by surface pretreatment in a pressure vessel with 10kg pressure for 5 hours, then add graphite slurry, fully disperse and grind for 5-7 hours, until the mixture becomes a graphite emulsion;
[0047] D. Add 5-10g of nickel powder to the graphite emulsion, and treat it with microwave at 400°C for 15 minutes until the nickel powder in the emulsion is evenly dispersed, and add 60g of lithium stearate soap to the emulsion mixture evenly dispersed with the nickel powder. Continue grinding for 2.5 hours to obtain the high-temperature lubricant of the present invention.
[0048] This high-temperature lubricant is suitable for experiments similar to The...
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Abstract
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