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High-temperature lubricant for thermal simulation experiment and preparation method thereof

A high-temperature lubricant and experimental technology, applied in lubricating compositions, additives, petroleum industry, etc., can solve the problems of affecting the accuracy of measurement, affecting the results of high-temperature experiments, large frictional resistance, etc. Accurate results and the effect of reducing the coefficient of friction

Active Publication Date: 2021-03-12
CHENGDU ADVANCED METAL MATERIALS IND TECH RES INST CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

During the deformation process of the sample, there is a large frictional resistance between the two ends of the sample and the indenter, which affects the accuracy of the force measurement of the experimental results
In order to solve the above problems, MoS is generally used at present 2 Or carbon powder is used as the lubricant at the end. When the sample and the indenter are connected horizontally, these two solid lubricants are extremely inconvenient to use, and molybdenum disulfide reduces friction at low temperature and increases friction at high temperature, which affects the results of high temperature experiments.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

preparation example Construction

[0027] The present invention further provides a method for preparing the above-mentioned high-temperature lubricant for thermal simulation experiments, which comprises the following steps:

[0028] A. After mixing 500-700 parts of graphite powder and 100-200 parts of mineral oil, use ultrasonic mixing and dispersion technology for surface pretreatment;

[0029] B. Take 60-80 parts of graphite powder and 100 parts of mineral oil, and mix them evenly to obtain graphite slurry;

[0030] C, the mixture obtained by surface pretreatment in step A is mixed with the graphite slurry obtained in step B after the surface pretreatment, and is dispersed and ground to obtain graphite emulsion;

[0031] D. After the graphite emulsion obtained in step C is mixed with 5-200 parts of nickel powder, microwave treatment is used until the nickel powder in the emulsion is uniformly dispersed, then mixed with 50-100 parts of lithium soap, and ground to obtain a lubricant.

[0032] The method of the...

Embodiment 1

[0038] A. Weigh 500 grams of graphite powder, add the graphite powder to 150g of mineral oil, and apply ultrasonic mixing and dispersion technology at a frequency of 20KHZ to carry out surface pretreatment for 10 minutes;

[0039] B, take by weighing 60 graphite powder, add in 100g mineral oil, make graphite slurry;

[0040] C. Treat the mixture obtained through surface pretreatment in a pressure vessel with a pressure of 10 kg for 5 hours, then add graphite slurry, fully disperse and grind for 5 hours, until the mixture becomes a graphite emulsion;

[0041] D. Add 100 g of nickel powder to the graphite emulsion, and treat it with microwaves at 450 ° C for 15 minutes until the nickel powder in the emulsion is uniformly dispersed, and add 70 g of lithium stearate soap to the emulsion mixture uniformly dispersed with the nickel powder, and continue grinding 3h, the high-temperature lubricant of the present invention can be obtained.

[0042] This high-temperature lubricant is s...

Embodiment 2

[0044] A. Weigh 500g of graphite powder, add graphite powder to 100g of mineral oil, and apply ultrasonic mixing and dispersion technology at a frequency of 20KHZ for surface pretreatment for 10 minutes;

[0045] B, take by weighing 60g graphite powder, add in 100g mineral oil, make graphite slurry;

[0046] C. Treat the mixture obtained by surface pretreatment in a pressure vessel with 10kg pressure for 5 hours, then add graphite slurry, fully disperse and grind for 5-7 hours, until the mixture becomes a graphite emulsion;

[0047] D. Add 5-10g of nickel powder to the graphite emulsion, and treat it with microwave at 400°C for 15 minutes until the nickel powder in the emulsion is evenly dispersed, and add 60g of lithium stearate soap to the emulsion mixture evenly dispersed with the nickel powder. Continue grinding for 2.5 hours to obtain the high-temperature lubricant of the present invention.

[0048] This high-temperature lubricant is suitable for experiments similar to The...

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Abstract

The invention discloses a high-temperature lubricant for a thermal simulation experiment and a preparation method of the high-temperature lubricant, and belongs to the technical field of lubricants. The invention overcomes the defects of poor high-temperature performance stability and the like of the existing lubricant, and provides a high-temperature lubricant for thermal simulation experiments,which comprises the following raw materials in parts by weight: 560-780 parts of graphite powder, 200-300 parts of mineral oil, 5-200 parts of nickel powder and 50-100 parts of lithium soap. Graphitepowder serves as a matrix and is converted into graphite emulsion through mineral oil, then nickel powder is added, grinding treatment is conducted through a high-speed dispersion ball mill, finally,lithium soap is added, grinding is conducted, and the lubricant is prepared. The lubricant provided by the invention provides good lubrication for the end part of a sample during a thermal simulationexperiment, and especially during high-temperature compression, the friction force of the end part of the sample is reduced, so that the experiment result is more accurate.

Description

technical field [0001] The invention belongs to the technical field of lubricants, and in particular relates to a high-temperature lubricant for thermal simulation experiments and a preparation method thereof. Background technique [0002] The physical simulation experiment of metal materials is an indispensable link in the study of material properties and the development of new material preparation processes, among which material thermal simulation is the basic means of physical simulation. At present, only Gleeble thermal simulation equipment has reached 200 units nationwide. Taking Panzhihua Iron and Steel's thermal simulation equipment as an example, the experiment of thermal simulation equipment has reached saturation, and the equipment maintains an average working time of 10 hours a day, which consumes a lot of high-temperature lubricants. [0003] The general process of material thermal simulation is to apply a certain load and current to the experimental sample thro...

Claims

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Application Information

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IPC IPC(8): C10M141/02C10N30/06C10N30/08
CPCC10M141/02C10M2201/041C10M2201/14C10M2201/05C10M2203/10C10M2207/126
Inventor 蔡晓文邢远杨旭杨晓琴
Owner CHENGDU ADVANCED METAL MATERIALS IND TECH RES INST CO LTD
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