Heavy release film for OCA optical adhesive
A technology of re-release and release film, applied in the field of OCA optical adhesive, can solve the problems of unclear release force explanation, inability to obtain OCA optical adhesive re-release film, no detailed explanation, etc., to achieve excellent release performance, The effect of high adhesion and strong release force
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Embodiment 1
[0032] With the polybutadiene polyurethane of 50 weight parts, the polyacrylate resin of 50 weight parts, the 1 of 20 weight parts, 3-dioxane, the tetramethyltetravinyl cyclotetrasiloxane of 20 weight parts, 25 Parts by weight of octadecyl methacrylate active monomer diluent, 20 parts by weight of tetrahydrofuran are uniformly mixed, adding 1 part by weight of initiator is 2-hydroxyl-2-methyl-1-phenyl-1-propanone , magnetically stirred for 120 seconds to obtain a release agent.
[0033] The release agent is evenly coated on the surface of the PET release film substrate 21 with a thickness of 80 μm, vacuum defoaming for 1 hour, N 2 The release agent layer 22 was formed after being irradiated with ultraviolet light for 180 seconds under certain conditions, and the thickness of the release agent layer 22 was measured to be 1.5 μm.
[0034] After testing, the release agent layer 22 of this embodiment has good stability below 120°C, without decomposition and detachment, and still ...
Embodiment 2
[0036] The polybutadiene polyurethane of 150 weight parts, the polyacrylate resin of 90 weight parts, the 1,3-dioxane of 40 weight parts, the tetramethyltetravinyl cyclotetrasiloxane of 50 weight parts, 55 Parts by weight of octadecyl methacrylate reactive monomer diluent, 40 parts by weight of tetrahydrofuran are uniformly mixed, adding 5 parts by weight of initiator is 2-hydroxyl-2-methyl-1-phenyl-1-propanone , magnetically stirred for 120 seconds to obtain a release agent.
[0037] The release agent is evenly coated on the surface of the PET release film substrate 21 with a thickness of 150 μm, vacuum defoaming for 1 hour, N 2 The release agent layer 22 was formed after being cured by ultraviolet light irradiation for 180 seconds under certain conditions. The thickness of the release agent layer 22 was measured to be 5.5 μm.
[0038] After testing, the release agent layer 22 of this embodiment has good stability below 120°C, without decomposition and detachment, and still ...
Embodiment 3
[0040] With the polybutadiene polyurethane of 100 weight parts, the polyacrylate resin of 65 weight parts, the 1,3-dioxane of 30 weight parts, the tetramethyltetravinyl cyclotetrasiloxane of 35 weight parts, 40 Parts by weight of octadecyl methacrylate active monomer diluent, 30 parts by weight of tetrahydrofuran are uniformly mixed, adding 3 parts by weight of initiator is 2-hydroxyl-2-methyl-1-phenyl-1-propanone , magnetically stirred for 120 seconds to obtain a release agent.
[0041] The release agent is evenly coated on the surface of the PET release film substrate 21 with a thickness of 100 μm, vacuum defoaming for 1 hour, N 2 The release agent layer 22 was formed after being cured by ultraviolet light irradiation for 180 seconds under certain conditions, and the thickness of the release agent layer 22 was measured to be 3.5 μm.
[0042] After testing, the release agent layer 22 of this embodiment has good stability below 120°C, without decomposition and detachment, and...
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