Disposable nano-antibacterial soap paper as well as preparation method and application thereof
A disposable, soap paper technology, applied in the fields of botanical equipment and methods, soap detergents and other compounding agents, applications, etc., can solve the problems that do not meet the requirements of safety and health, traditional soap is not easy to carry, no antibacterial and antiviral, etc. It can solve the problem of unclean hand washing, excellent antibacterial properties and good antibacterial properties.
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Embodiment 1
[0035] Disposable nano antibacterial soap paper, the specific steps of preparation are as follows:
[0036] (1) First inject sodium hydroxide solution in the container, vibrate, then heat and boil; after pouring out the sodium hydroxide, wash it with distilled water for later use, add 20mL concentration to the container and be 0.05mmol / mL silver nitrate solution; Under stirring, add ammonia water drop by drop to 20 mL of silver nitrate solution with a concentration of 0.05 mmol / mL until the precipitate just dissolves to obtain a silver ammonia solution;
[0037] (2) adding the silver ammonia solution that step 1 obtains to 20mL concentration is that 0.05mmol / mL sodium carboxymethyl cellulose solution is mixed, then dripped into the 0.5wt% montmorillonite solution that has been swelled by water absorption, Microwave stirring reaction (reaction time 30min, reaction temperature 60°C, power 500W) to obtain silver-loaded sodium carboxymethylcellulose / montmorillonite antibacterial m...
Embodiment 2
[0043] Disposable nano antibacterial soap paper, the specific steps of preparation are as follows:
[0044] (1) First inject sodium hydroxide solution in the container, vibrate, then heat and boil; after pouring out the sodium hydroxide, wash it with distilled water for later use, add 20mL concentration to the container and be 0.05mmol / mL silver nitrate solution; Under stirring, add ammonia water drop by drop to 20 mL of silver nitrate solution with a concentration of 1 mmol / mL until the precipitate just dissolves to obtain a silver ammonia solution;
[0045] (2) adding the silver ammonia solution obtained in step 1 to 200 mL concentration of 1 mg / mL sodium carboxymethyl cellulose solution and mixing, then dripping into 10 mL concentration of 1 wt% montmorillonite solution that has been swollen by water absorption, microwave stirring Reaction (reaction time 70min, reaction temperature 85°C, power 800W) to obtain silver-loaded sodium carboxymethylcellulose / montmorillonite antib...
Embodiment 3
[0051] Disposable nano antibacterial soap paper, the specific steps of preparation are as follows:
[0052] (1) First inject sodium hydroxide solution in the container, vibrate, then heat and boil; after pouring out the sodium hydroxide, wash it with distilled water for later use, add 20mL concentration to the container and be 0.05mmol / mL silver nitrate solution; Under stirring, add ammonia water drop by drop to 20 mL of silver nitrate solution with a concentration of 3 mmol / mL until the precipitate just dissolves to obtain a silver ammonia solution;
[0053] (2) Add the silver ammonia solution that step 1 obtains to 600mL concentration and mix in 3mg / mL sodium carboxymethyl cellulose solution, then drop into 6mL concentration that has been swelled by water absorption and be 3wt% in the montmorillonite solution, microwave stirring Reaction (reaction time 80min, reaction temperature 90°C, power 1000W) to obtain silver-loaded sodium carboxymethylcellulose / montmorillonite antibac...
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