Heteropolyacid air bactericide as well as preparation method and application thereof
A technology of heteropolyacid and bactericide, which is applied in the field of heteropolyacid air bactericide and its preparation, can solve the problems of negative ion air sterilizing effect not obvious, human respiratory system damage, large amount of ozone, etc., and achieve high catalytic ability and selectivity Good stability, guaranteed stability, and good thermal stability
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Embodiment 1
[0028] A heteropoly acid air bactericide, comprising the following raw materials in parts by weight: 1 part of N,N-dimethylformamide, 1.5 parts of propionic acid, 2.5 parts of phosphotungstic acid, 3 parts of silane coupling agent, 10 parts of di Chlorine oxide, 30 parts of water.
[0029] A preparation method of heteropolyacid air bactericide, comprising the following steps:
[0030] (A) After mixing N,N-dimethylformamide and propionic acid in proportion, add water in proportion and stir to dissolve it completely to obtain a mixed solution; the stirring time is 30min, the stirring speed is 800rpm, and the temperature is 45- 65°C.
[0031] (B) Under the protection of inert gas, add phosphotungstic acid and silane coupling agent in proportion to the mixed solution obtained in step (A), then pour it into the reaction tank for reaction, and stir; the reaction time is 0.5h, and the reaction temperature is 100°C, during the reaction process, a pH regulator should be used to contr...
Embodiment 2
[0034] A kind of heteropolyacid air sterilizer, comprises the raw material of following parts by weight: 5 parts of N,N-dimethylformamide, 5 parts of propionic acid, 3 parts of phosphomolybdic acid, 10 parts of silane coupling agent, 30 parts of di Chlorine oxide, 45 parts of water.
[0035] A preparation method of heteropolyacid air bactericide, comprising the following steps:
[0036] (A) After mixing N,N-dimethylformamide and propionic acid in proportion, add water in proportion, stir to dissolve it completely, and obtain a mixed solution; the stirring time is 60min, the stirring speed is 2000rpm, and the temperature is 45- 65°C.
[0037] (B) Under the protection of an inert gas, add phosphomolybdic acid and a silane coupling agent in proportion to the mixed solution obtained in step (A), then pour it into a reaction tank for reaction, and stir; the reaction time is 1h, and the reaction temperature is 255 ℃, in the reaction process, a pH regulator needs to be used to cont...
Embodiment 3
[0040] A kind of heteropolyacid air sterilizer, comprises the raw material of following parts by weight: 3 parts of N, N-dimethylformamide, 3.25 parts of propionic acid, 2.75 parts of silicotungstic acid, silicon molybdenum acid silicon (tungstic acid and silicon molybdenum The addition ratio of acid is 1:1), 6.5 parts of silane coupling agent, 20 parts of chlorine dioxide, and 37.5 parts of water.
[0041] A preparation method of heteropolyacid air bactericide, comprising the following steps:
[0042] (A) After mixing N,N-dimethylformamide and propionic acid in proportion, add water in proportion and stir to dissolve it completely to obtain a mixed solution; the stirring time is 45min, the stirring speed is 1400rpm, and the temperature is 45- 65°C.
[0043] (B) Under the protection of inert gas, add silicotungstic acid, silicomolybdic acid and silane coupling agent in proportion to the mixed solution obtained in step (A), then pour it into the reaction tank for reaction, and...
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