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Chitosan and preparation method thereof

A technology of chitosan and chitosan gel, which is applied in the field of chitosan, can solve the problems of antibacterial properties, air permeability, and ripening of fruits and vegetables that cannot meet people's needs, and achieve the goal of promoting ripening of fruits and vegetables and improving air permeability Effect

Inactive Publication Date: 2021-06-11
HEBEI NORMAL UNIVERSITY OF SCIENCE AND TECHNOLOGY
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

And existing chitosan still can't satisfy people's demand aspect antibacterial property, gas permeability and fruit and vegetable ripening.

Method used

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  • Chitosan and preparation method thereof

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Effect test

Embodiment 1

[0036] A preparation method of chitosan, comprising the following steps:

[0037] S1: Preparation of modified xylitol: take the peel, wash and chop it, use pure water to repeat 3-5 times to obtain deashed crumbs, put the deashed crumbs into the mixed enzyme aqueous solution, heat up to 10-20 ℃, keep it for 10-15h, and obtain the mixed solution of enzymatic hemicellulose and polysaccharide, heat and concentrate the mixed solution of enzymatic hemicellulose and polysaccharide, mix it with 1% sulfuric acid and stir evenly, raise the temperature to 100-110℃, keep 20-40min, to obtain the acid hydrolysis solution, add quicklime and pH regulator to the acid hydrolysis solution, adjust the pH value to 7-9, add activated carbon until the solution is completely decolorized, then separate the solid content, keep the solution, the solution is For the required xylitol solution, put the xylitol solution into a temperature-controlled reaction vat, raise the temperature to 20-25°C, introduce ...

Embodiment 2

[0045] A preparation method of chitosan, comprising the following steps:

[0046]S1: Preparation of modified xylitol: take the peel, wash and chop it, use pure water to repeat 3-5 times to obtain deashed crumbs, put the deashed crumbs into the mixed enzyme aqueous solution, heat up to 10-20 ℃, keep it for 10-15h, and obtain the mixed solution of enzymatic hemicellulose and polysaccharide, heat and concentrate the mixed solution of enzymatic hemicellulose and polysaccharide, mix it with 1% sulfuric acid and stir evenly, raise the temperature to 100-110℃, keep 20-40min, to obtain the acid hydrolysis solution, add quicklime and pH regulator to the acid hydrolysis solution, adjust the pH value to 7-9, add activated carbon until the solution is completely decolorized, then separate the solid content, keep the solution, the solution is For the required xylitol solution, put the xylitol solution into a temperature-controlled reaction vat, raise the temperature to 20-25°C, introduce e...

Embodiment 3

[0054] A preparation method of chitosan, comprising the following steps:

[0055] S1: Preparation of modified xylitol: take the peel, wash and chop it, use pure water to repeat 3-5 times to obtain deashed crumbs, put the deashed crumbs into the mixed enzyme aqueous solution, heat up to 10-20 ℃, keep it for 10-15h, and obtain the mixed solution of enzymatic hemicellulose and polysaccharide, heat and concentrate the mixed solution of enzymatic hemicellulose and polysaccharide, mix it with 1% sulfuric acid and stir evenly, raise the temperature to 100-110℃, keep 20-40min, to obtain the acid hydrolysis solution, add quicklime and pH regulator to the acid hydrolysis solution, adjust the pH value to 7-9, add activated carbon until the solution is completely decolorized, then separate the solid content, keep the solution, the solution is For the required xylitol solution, put the xylitol solution into a temperature-controlled reaction vat, raise the temperature to 20-25°C, introduce ...

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Abstract

The invention discloses chitosan and a preparation method thereof, the main component of chitosan is chitosan gel, and the chitosan gel comprises the following components in parts by weight: 25 parts by weight of chitosan, 13 parts by weight of a lactic acid solution, 12 parts by weight of glycerol, 12 parts by weight of modified xylitol, 7 parts by weight of L-carnitine tartrate, 13 parts by weight of modified acetic acid, 4 parts by weight of ethephon, 1 part by weight of a ginsenoside extract, 1 part by weight of an angelica sinensis extract and the balance of deionized water. According to the preparation method of the chitosan, the modified xylitol and the modified acetic acid are added, the air permeability, antibacterial property and ripening rate of chitosan are greatly improved, and ethephon is added to further promote ripening of fruits and vegetables, so that the problem that existing chitosan cannot meet the requirements of people in the aspects of antibacterial property, air permeability and ripening of fruits and vegetables is solved.

Description

technical field [0001] The invention relates to a chitosan, in particular to a chitosan and a preparation method thereof. Background technique [0002] Chitosan is the product of natural polysaccharide chitin removing part of the acetyl group, chemical name: β-(1→4)-2-amino-2-deoxy-D-glucose, molecular formula: (C6H11NO4)N, molecular weight of the unit For: 161.2, it has various physiological functions such as biodegradability, biocompatibility, non-toxicity, antibacterial, anti-cancer, lipid-lowering, and immune-enhancing. Due to its good physical, chemical and biological properties, chitosan has excellent stability to organic solvents and is convenient for secondary processing. The application prospect is broad. [0003] The amino groups in the chitosan molecular structure are more reactive than the acetamido groups in the chitin molecule, making the polysaccharide have excellent biological functions and can undergo chemical modification reactions. Therefore, chitosan i...

Claims

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Application Information

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IPC IPC(8): A01N43/16A01N37/02A01N65/10A01N65/08A01N27/00A01N57/20A01N59/20A01N59/26A01N59/00A01N25/04A01N37/36A01N37/44A01N33/12A01P21/00A01P1/00A01P3/00C12P7/18A23B7/154A23B7/157
CPCA01N25/04A01N27/00A01N33/12A01N37/02A01N37/36A01N37/44A01N43/16A01N57/20A01N59/00A01N59/20A01N59/26A01N65/00A01N65/08A01N65/10A23B7/154A23B7/157A23V2002/00C12P7/18A23V2200/10A23V2250/022A23V2250/21A23V2250/511A23V2250/6422
Inventor 侯文龙王秀平程才红李云韩玉翠
Owner HEBEI NORMAL UNIVERSITY OF SCIENCE AND TECHNOLOGY