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Method for preparing graphene reinforced glass material by melting and sintering

A technology of strengthening glass and graphene, which is applied in glass forming, glass pressing, glass manufacturing equipment, etc., to achieve the effect of promoting application and enhancing impact strength

Pending Publication Date: 2021-07-09
张玉琪
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

For the glass market, glass products have penetrated all aspects of people's lives. Lightweight production requires the thickness of glass products to be thinner and thinner, which improves the convenience of people's lives, but at the same time, thin-layer glass The preparation of products poses new challenges. At the same time, meeting the process requirements and ensuring the impact strength, flexural strength, and surface hardness of the products are an important issue for the person in charge of the glass products industry.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0019] A kind of melting and sintering method of the present embodiment prepares graphene-reinforced glass material, raw material comprises the following components by weight:

[0020] 120 parts of silicon dioxide;

[0021] 70 parts of vanadium oxide;

[0022] 20 parts of diboron trioxide;

[0023] 12 parts of titanium nitride;

[0024] 3 parts of barium chloride;

[0025] 3 parts of aluminum oxide;

[0026] 6 parts of lignocellulose;

[0027] 3 parts of magnesium oxide;

[0028] 6 parts of selenium powder;

[0029] Graphene 16 parts.

[0030] The sheet thickness of the graphene is ≤50nm, and the sheet diameter is ≤80μm.

[0031] The surface compressive stress of the glass material is ≥450MPa.

[0032] The method comprises the steps of:

[0033] Step 1, after mixing silicon dioxide, vanadium oxide, diboron trioxide, titanium nitride, barium chloride, aluminum oxide, lignocellulose, magnesium oxide, selenium powder and graphene, grind them, and sieve to obtain a parti...

Embodiment 2

[0038] A kind of melting and sintering method of the present embodiment prepares graphene-reinforced glass material, raw material comprises the following components by weight:

[0039] 110 parts of silicon dioxide;

[0040] 60 parts of vanadium oxide;

[0041] 14 parts of diboron trioxide;

[0042] 8 parts of titanium nitride;

[0043] 2 parts of barium chloride;

[0044] 2 parts of aluminum oxide;

[0045] 4 parts lignocellulose;

[0046] 2 parts of magnesium oxide;

[0047] Selenium powder 4 parts;

[0048] Graphene 12 parts.

[0049] The sheet thickness of the graphene is ≤50nm, and the sheet diameter is ≤80μm.

[0050] The surface compressive stress of the glass material is ≥450MPa.

[0051] The method comprises the steps of:

[0052] Step 1, after mixing silicon dioxide, vanadium oxide, diboron trioxide, titanium nitride, barium chloride, aluminum oxide, lignocellulose, magnesium oxide, selenium powder and graphene, grind them, and sieve to obtain a particle siz...

Embodiment 3

[0057] A kind of melting and sintering method of the present embodiment prepares graphene-reinforced glass material, raw material comprises the following components by weight:

[0058] 130 parts of silicon dioxide;

[0059] 80 parts of vanadium oxide;

[0060] 26 parts of diboron trioxide;

[0061] 16 parts of titanium nitride;

[0062] 4 parts of barium chloride;

[0063] 4 parts of aluminum oxide;

[0064] 8 parts of lignocellulose;

[0065] 4 parts of magnesium oxide;

[0066] 8 parts of selenium powder;

[0067] Graphene 18 parts.

[0068] The sheet thickness of the graphene is ≤50nm, and the sheet diameter is ≤80μm.

[0069] The surface compressive stress of the glass material is ≥450MPa.

[0070] The method comprises the steps of:

[0071] Step 1, after mixing silicon dioxide, vanadium oxide, diboron trioxide, titanium nitride, barium chloride, aluminum oxide, lignocellulose, magnesium oxide, selenium powder and graphene, grind them, and sieve to obtain a parti...

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Abstract

The invention discloses a method for preparing a graphene reinforced glass material by melting and sintering. The method comprises the following steps: step 1, mixing silicon dioxide, vanadium oxide, diboron trioxide, titanium nitride, barium chloride, aluminum oxide, lignocellulose, magnesium oxide, selenium powder and graphene, grinding, and sieving to obtain mixed powder with the particle size of 100-200 meshes; step 2, the mixed powder obtained in the step 1 is subjected to heat preservation sintering for 1-2 h under the condition of 400-600 DEG C, the temperature is increased to 800-900 DEG C at the heating rate of 2-5 DEG C / min, heat preservation sintering is conducted for 45-60 min, and compression molding is conducted; step 3, naturally cooling to room temperature; and step 4, grinding and polishing the glass profile naturally cooled in the step 3 to obtain the graphene reinforced glass material. The glass material prepared by the method has enhanced impact strength, breaking strength and surface hardness, and is beneficial to popularization and application.

Description

technical field [0001] The invention belongs to the technical field of glass materials, and in particular relates to a method for preparing graphene-reinforced glass materials by melting and sintering. Background technique [0002] At present, with the improvement of people's living standards, the requirements for lightweight products are increasing. For the glass market, glass products have penetrated all aspects of people's lives. Lightweight production requires the thickness of glass products to be thinner and thinner, which improves the convenience of people's lives, but at the same time, thin-layer glass The preparation of products poses new challenges. At the same time, meeting the process requirements and ensuring the impact strength, flexural strength, and surface hardness of the products are an important issue for the person in charge of the glass products industry. [0003] Reinforced glass products are an effective way to improve the quality of glass products and...

Claims

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Application Information

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IPC IPC(8): C03C6/06C03B11/00
CPCC03B11/00C03C1/00
Inventor 不公告发明人
Owner 张玉琪
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