Nano material as well as preparation method and application thereof
A technology of nanomaterials and polymerization reaction, applied in the field of viscous reduction of heavy oil, which can solve problems such as increased oil production costs, difficulty in finding gas sources, and migration loss of surfactants
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Embodiment 1
[0054] The preparation of embodiment 1 nanometer material 1#
[0055] 1. Weigh 15g monomeric AOS (α-olefin sulfonate sodium) and 15g monomeric acrylamide, 20g monomeric maleic anhydride organic hydrophilic monomer, 10g coupled montmorillonite into a three-necked flask, add 900g deionized water, stir to dissolve, pass nitrogen gas for 30 minutes, and remove the oxygen in the solution;
[0056] 2. Take by weighing 0.25g of initiator potassium persulfate, add 50g of deionized water, stir and dissolve, and ventilate nitrogen for 30min to get rid of oxygen in the solution (initiator concentration 0.5wt%);
[0057] 3. Mechanically stir the solution in 1 at 250rpm, start heating, and set the heating temperature to 55°C;
[0058] 4. When the temperature of the solution in the flask reaches 45°C, add the potassium persulfate in 2 dropwise with a constant pressure funnel, and at the same time set the reaction temperature to 80°C, drop the initiator in 7-10 minutes, and start after the te...
Embodiment 2
[0059] The preparation of embodiment 2 nanometer material 2#
[0060] 1. Weigh 15g monomeric AOS (α-olefin sulfonate sodium) and 15g monomeric acrylamide, 20g monomeric maleic anhydride organic hydrophilic monomer, 20g coupled montmorillonite into a three-necked flask, add 900g deionized water, stir to dissolve, pass nitrogen gas for 30 minutes, and remove the oxygen in the solution;
[0061] 2. Take by weighing 0.25g of initiator potassium persulfate, add 50g of deionized water, stir and dissolve, and ventilate nitrogen for 30min to get rid of oxygen in the solution (initiator concentration 0.5wt%);
[0062] 3. Mechanically stir the solution in 1 at 250rpm, start heating, and set the heating temperature to 55°C;
[0063] 4. When the temperature of the solution in the flask reaches 45°C, add the potassium persulfate in 2 dropwise with a constant pressure funnel, and at the same time set the reaction temperature to 80°C, drop the initiator in 7-10 minutes, and start after the ...
Embodiment 3
[0064] The preparation of embodiment 3 nanometer material 3#
[0065] 1. Weigh 15g monomer AOS (α-olefin sulfonate sodium) and 15g monomer acrylamide, 20g monomer maleic anhydride organic hydrophilic monomer, 30g coupled montmorillonite to a three-necked flask, add 900g deionized water, stir to dissolve, pass nitrogen gas for 30 minutes, and remove the oxygen in the solution;
[0066] 2. Take by weighing 0.25g of initiator potassium persulfate, add 50g of deionized water, stir and dissolve, and ventilate nitrogen for 30min to get rid of oxygen in the solution (initiator concentration 0.5wt%);
[0067] 3. Mechanically stir the solution in 1 at 250rpm, start heating, and set the heating temperature to 55°C;
[0068] 4. When the temperature of the solution in the flask reaches 45°C, add the potassium persulfate in 2 dropwise with a constant pressure funnel, and at the same time set the reaction temperature to 80°C, drop the initiator in 7-10 minutes, and start after the temperat...
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