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Large-size neodymium iron boron diffusion magnet and preparation method thereof

A NdFeB, large-size technology, applied in the direction of magnetic objects, inductance/transformer/magnet manufacturing, magnetic materials, etc., can solve the problems of insufficient diffusion power, limited, low percentage of rare earth elements, etc., to shorten the heat treatment time, The effect of flexible process and easy operation

Active Publication Date: 2021-08-24
EARTH PANDA ADVANCE MAGNETIC MATERIAL
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0011] This technology effectively overcomes the problems existing in the previous diffusion technology, but there are still deficiencies, mainly including: ①Comparison of the thickness of rare earth alloy thin strips prepared by stripping method thicker (between 30 and 100 μm), since rare earth alloy thin strips are non-magnetic substances, thicker alloy thin strips will reduce the overall magnetic properties of the magnet; ② in thicker rare earth alloy thin strips, in order to ensure the final magnet The coercive force requires a certain percentage of rare earths. In order to ensure the percentage of rare earths, more rare earth elements need to be added. Otherwise, the percentage of rare earth elements is too low, and the improvement of the coercive force of the final magnet is very limited; ③The alloy used is M-Cu alloy, and M is Pr, Nd or Dy. After alloying, the chemical activity of rare earth elements decreases, the diffusion power is insufficient, and the diffusion effect is limited

Method used

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  • Large-size neodymium iron boron diffusion magnet and preparation method thereof

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preparation example Construction

[0033] The first aspect of the present invention provides a method for preparing a large-size NdFeB diffusion magnet, comprising the following steps:

[0034] forming a heavy rare earth metal layer on the surface of the metal foil to obtain a modified metal foil, the metal foil being aluminum foil or copper foil;

[0035] Combine N pieces of NdFeB magnets to be diffused and sintered with N-1 pieces of the modified metal foil to obtain an assembly, wherein, N≥3, and the modified metal foils are respectively arranged on adjacent NdFeB magnets to be diffused and sintered between boron magnets;

[0036] The combination is heat treated to obtain a large-size NdFeB diffusion magnet.

[0037] In the present invention, the modified metal foil is obtained by forming a heavy rare earth metal layer on the surface of the metal foil, and then the modified metal foil is directly attached to the NdFeB magnet to be diffused and sintered, thereby eliminating the need for coating and coating o...

Embodiment 1

[0050] Get Modified Aluminum Foil

[0051] A modified aluminum foil 1 was obtained by depositing a 3 μm dysprosium metal layer on both surfaces of an aluminum foil with a thickness of 1 μm by thermal evaporation deposition technology.

[0052] get combination

[0053] Pr the performance as N52 6 Nd 24 Fe 69 B The sintered NdFeB magnet is processed into a magnet to be diffused with a minimum size direction of 4mm (denoted as a magnet to be diffused 1), and the direction of the minimum size is parallel to the direction of easy magnetization; insert 3 pieces of modified aluminum foil 1 between the 4 pieces of magnets to be diffused , to obtain assembly 1, wherein the thickness of the first piece and the fourth piece of magnet is 2mm.

[0054] heat treatment

[0055] After heat treatment of assembly 1 at 850°C for 30 hours, the diffusion magnet was subjected to secondary heat treatment at 500°C for 5 hours to obtain a large-sized NdFeB diffusion magnet with a diffusion d...

Embodiment 2

[0057] Get Modified Aluminum Foil

[0058] With embodiment 1.

[0059] get combination

[0060] Pr with performance as 50M 6 Nd 23.5 Dy 0.8 Fe 68.7 B The sintered NdFeB magnet is processed into a magnet to be diffused with a minimum size direction of 3 mm (denoted as a magnet to be diffused 2), and the minimum size direction is perpendicular to the direction of easy magnetization; 4 pieces of modified aluminum foil 1 are inserted between 5 pieces of magnets to be diffused , Obtain assembly 2, wherein the thickness of the first piece and the fifth piece of magnet is 1.5mm.

[0061] heat treatment

[0062] After heat treatment of assembly 2 at 875°C for 10 hours, the diffusion magnet was subjected to secondary heat treatment at 520°C for 5 hours to obtain a large-sized NdFeB diffusion magnet with a diffusion direction size of 12mm, which was designated as sample 2.

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Abstract

The invention discloses a large-size neodymium iron boron diffusion magnet and a preparation method thereof. The preparation method comprises: firstly, forming a heavy rare earth metal layer on the surface of metal foil, and obtaining modified metal foil; then combining N pieces of neodymium-iron-boron magnets to be diffused and sintered with N-1 pieces of modified metal foils to obtain a combined body; and finally, carrying out heat treatment on the combined body to obtain the large-size neodymium iron boron diffusion magnet. The preparation method is simple in process, high in flexibility and low in energy consumption, and diffusion and bonding processes are simultaneously realized in a one-time heat treatment process. The thickness of the metal foil is small, the heavy rare earth participates in diffusion in the form of a metal simple substance, the diffusion effect is better, the performance of the diffused and bonded magnet is higher, and the application prospect is achieved.

Description

technical field [0001] The invention belongs to the field of rare earth permanent magnet materials, and in particular relates to a preparation method of a large-size NdFeB diffusion magnet, and also relates to a large-size NdFeB diffusion magnet obtained by diffusing the preparation method. Background technique [0002] Sintered NdFeB magnets are the strongest magnetic materials so far, and are widely used in aerospace, automotive industry, electronic appliances, medical equipment, energy-saving motors, new energy, wind power and other fields. They are currently the fastest growing and most promising market Good permanent magnet material. Sintered NdFeB magnets have outstanding advantages such as high magnetic energy product, high coercive force, high energy density, high cost performance and good mechanical properties, and have played an important role in the high-tech field. After more than 30 years of research and development, with reasonable alloy composition and mature...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): H01F41/02H01F1/057
CPCH01F41/0293H01F1/0577
Inventor 冯泉妤陈静武周志国衣晓飞刘友好鲍成谭新博刘明辉
Owner EARTH PANDA ADVANCE MAGNETIC MATERIAL
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