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Cigarette blasting bead coated with water-soluble essence and preparation method thereof

A technology of water-soluble essence and popping beads, which is applied in the fields of tobacco, application, and tobacco treatment. It can solve the problems of short embedding time of water molecules, poor film-forming property, and long polymerization time, so as to overcome the defects of vapor permeability and improve strength. Effects of brittleness and long embedding time

Active Publication Date: 2021-09-03
WUYI UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

CN109012521A provides a method for preparing water-encapsulated capsules by adopting styrene and acrylate as polymerized monomers and adopting heat-induced radical curing, but this method has the disadvantages of long polymerization time and incompletely polymerized styrene liquid having an odor ; Patent CN109222223A provides a kind of adopting wax as wall material, is used for coating aqueous solution and has obtained a kind of water bag capsule, but the wax material that adopts in this method has the defect of poor film-forming property and insufficient film strength
Patent CN111602847A provides a method of using acrylate and its derivatives to prepare a method of coating water-soluble essence by UV light curing, but this method has the disadvantages of short embedding time of water molecules and easy distribution. In about 1 week, the internal solvent will evaporate completely, and the applied blasting effect will not be produced.

Method used

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  • Cigarette blasting bead coated with water-soluble essence and preparation method thereof
  • Cigarette blasting bead coated with water-soluble essence and preparation method thereof

Examples

Experimental program
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Effect test

Embodiment 1

[0031] This embodiment provides a kind of quick-fried beads for cigarettes, comprising a core material and a shell material, the core material comprising the following components by weight: 47 parts of deionized water, 50 parts of alcohol, 2 parts of rose oil, 0.8 parts of ethyl hydroxyethyl base cellulose, 0.7 parts of phenoxyethanol; the shell material includes the following components by weight: 60 parts of butyl acrylate, 30 parts of pentaerythritol triacrylate, 3 parts of 1-hydroxycyclohexyl phenyl ketone, 3 parts of p - Styrenetrimethoxysilane.

[0032] This embodiment also provides a preparation method of popping beads for cigarettes, comprising the following steps:

[0033] (1) Add 47 parts of deionized water, 50 parts of alcohol, 2 parts of rose oil, 0.8 parts of hydroxyethyl cellulose, and 0.7 parts of phenoxyethanol into the core material glue tank in sequence, and stir evenly to make the core material glue The viscosity of the liquid is 400mPa·s;

[0034] (2) Add...

Embodiment 2

[0038]This embodiment provides a kind of quick-fried beads for cigarettes, including a core material and a shell material. A compound of methyl cellulose, 0.5 parts of 5-chloro-2-methyl-4-isothiazolin-3-one and 2-methyl-4-isothiazolin-3-one; the shell material includes the following Components in parts by weight: 50 parts of butyl acrylate, 15 parts of dipentaerythritol hexaacrylate, 5 parts of 2-hydroxy-methylphenylpropane-1-one, 1 part of 3-methacryloxypropylmethyl Dimethoxysilane.

[0039] This embodiment also provides a preparation method of popping beads for cigarettes, comprising the following steps:

[0040] (1) 58 parts of deionized water, 40 parts of alcohol, 0.5 part of jasmine absolute, 0.5 part of hydroxymethylcellulose, 0.5 part of 5-chloro-2-methyl-4-isothiazolin-3-one and 2 -The compound of methyl-4-isothiazolin-3-one is sequentially added into the core material glue tank, and stirred evenly, so that the viscosity of the core material glue is 200mPa·s;

[004...

Embodiment 3

[0045] This embodiment provides a kind of quick-fried beads for cigarettes, comprising a core material and a shell material, the core material comprising the following components in parts by weight: 33 parts of deionized water, 60 parts of alcohol, 5 parts of musk, 1 part of methylol Sodium cellulose, 1 part of a compound of 5-chloro-2-methyl-4-isothiazolin-3-one and 2-methyl-4-isothiazolin-3-one; the shell material comprises the following weight Parts of components: 80 parts of butyl acrylate, 45 parts of pentaerythritol tetraacrylate, 1 part of 2-methyl-1-(4-methylthiophenyl)-2-morpholino-1-propanone, 5 parts of 3 - Methacryloxypropyltrimethoxysilane.

[0046] This embodiment also provides a preparation method of popping beads for cigarettes, comprising the following steps:

[0047] (1) Mix 33 parts of deionized water, 60 parts of alcohol, 5 parts of musk, 1 part of sodium hydroxymethylcellulose, 1 part of 5-chloro-2-methyl-4-isothiazolin-3-one and 2- The compound of methy...

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Abstract

The invention discloses a cigarette blasting bead coated with water-soluble essence and a preparation method thereof, and belongs to the technical field of cigarettes. The cigarette blasting bead comprises a core material and a shell material, wherein the core material comprises the following components in parts by weight: 40-60 parts of alcohol, 0.5-5 parts of water-soluble essence, 0.5-1 part of a thickening agent and 0.5-1 part of a preservative; and the shell material is prepared from the following components in parts by weight: 50 to 80 parts of butyl acrylate, 15 to 45 parts of poly-functional polyether acrylate, 1 to 5 parts of a photo initiator and 1 to 5 parts of a silane coupling agent. The silane coupling agent with an allyl group is introduced on the basis of an existing UV photo-initiation curing shell material, and by means of the hydrolysis curing cross-linking property of the silane coupling agent, the air permeability defect of acrylic resin is overcome, the strength and brittleness of the shell material are improved, and the purpose that the cigarette blasting bead is stably coated with an aqueous solution for a long time is achieved.

Description

technical field [0001] The invention relates to a popping ball for cigarettes coated with water-soluble essence and a preparation method thereof, belonging to the technical field of cigarettes. Background technique [0002] The role of adding flavors and fragrances in cigarettes is to improve the physical and chemical properties of cigarettes, round aroma, modify the taste of cigarettes, improve the taste of smoking, and establish the style of the product, which affects consumers' sense of smell, taste and touch to some extent, and enhance Product acceptability. The existing method of adding flavor is mainly to directly add flavor to shredded tobacco, or add flavor thread rich in flavor to the filter tip. [0003] Although there are related products on the market in China at present, most of the popping beads produced are oil-soluble flavors, and there are almost no popping beads coated with water-soluble flavors. Therefore, the development of quick-fried beads that can co...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A24D3/06A24D3/02A24B15/30
CPCA24D3/061A24D3/02A24B15/30
Inventor 李养令赖志良高敏朱章卫陈满于晖李峥嵘
Owner WUYI UNIV