Looking for breakthrough ideas for innovation challenges? Try Patsnap Eureka!

Flame-retardant slow-rebound memory sponge and preparation method thereof

A technology of memory foam and slow rebound, which is applied in the field of slow rebound sponge, can solve the problems of easy burning, thick smoke toxicity, and insufficient safety performance, and achieve the effect of less smoke and environmental friendliness

Active Publication Date: 2021-11-05
高州市铭顺劳保制品有限公司
View PDF8 Cites 1 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

After the air is pushed out of the cell and the cell is flattened, although the external force has been removed and the cell wall has restored elasticity, the air cannot return to the cell quickly due to the small vent holes, and the cell cannot quickly recover its shape. The force of the bomb is suppressed, and the time for the material to deform and recover is prolonged
[0004] Due to its excellent performance, slow rebound memory foam is often used to prepare cushions, pillows, mattresses, pads and other items. Because its main materials are polyurethane, polyether, etc., it lacks good flame retardancy. It is easy to burn when open flames or blazing flames, once burned, it is difficult to extinguish, and the smoke produced is also toxic to a certain extent, resulting in insufficient safety performance, and will cause harm to the environment when burned

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • Flame-retardant slow-rebound memory sponge and preparation method thereof
  • Flame-retardant slow-rebound memory sponge and preparation method thereof
  • Flame-retardant slow-rebound memory sponge and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0036] Prepare flame retardant, this flame retardant additive is made by following steps:

[0037] Step S1: under the conditions of ice bath and nitrogen protection, add 2-furylmethylamine and triethylamine into the flask, add chloroform, stir for 5min, then add the chloroform solution of phosphorus oxychloride dropwise to the flask, and then place in the ice bath React under the same conditions for 3 hours, then raise the temperature to 50°C to continue the reaction for 6 hours, after the reaction is completed, filter, wash with deionized water, and remove the solvent to obtain intermediate 1;

[0038] Step S2: Add p-aminotoluene and acetone into the flask, stir until dissolved at a temperature of 20°C under nitrogen protection, then add intermediate 1 into the flask, maintain the above conditions, react for 2 hours, and perform post-treatment. The steps are: rotary evaporation to remove the solvent, suction filtration, the filtrate was placed at 0°C for 5 hours, suction filt...

Embodiment 2

[0044] Prepare flame retardant, this flame retardant additive is made by following steps:

[0045] Step S1: under the conditions of ice bath and nitrogen protection, add 2-furylmethylamine and triethylamine into the flask, add chloroform, stir for 7.5min, then add the chloroform solution of phosphorus oxychloride dropwise in the flask, and then React under bath conditions for 3 hours, then raise the temperature to 50°C to continue the reaction for 6 hours, after the reaction is completed, filter, wash with deionized water, and remove the solvent to obtain intermediate 1;

[0046] Step S2: Add p-aminotoluene and acetone to the flask, stir until dissolved at a temperature of 22.5°C under nitrogen protection, then add intermediate 1 to the flask, maintain the above conditions, react for 2.5 hours, and perform post-treatment. The treatment steps are: rotary evaporation to remove the solvent, suction filtration, the filtrate was placed at 0°C for 5 hours, and suction filtration aga...

Embodiment 3

[0052] Prepare flame retardant, this flame retardant additive is made by following steps:

[0053] Step S1: under the condition of ice bath and nitrogen protection, add 2-furylmethylamine and triethylamine into the flask, add chloroform, stir for 10min, then add the chloroform solution of phosphorus oxychloride dropwise to the flask, and then place in the ice bath React under the same conditions for 3 hours, then raise the temperature to 50°C to continue the reaction for 6 hours, after the reaction is completed, filter, wash with deionized water, and remove the solvent to obtain intermediate 1;

[0054] Step S2: Add p-aminotoluene and acetone into the flask, stir until dissolved at a temperature of 25°C under nitrogen protection, then add intermediate 1 into the flask, maintain the above conditions, react for 3 hours, and perform post-treatment. The steps are: rotary evaporation to remove the solvent, suction filtration, the filtrate was placed at 0°C for 5 hours, suction filt...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

No PUM Login to View More

Abstract

The invention discloses a flame-retardant slow-rebound memory sponge and a preparation method thereof, and belongs to the technical field of slow-rebound sponges. The flame-retardant slow-rebound memory sponge is prepared from the following raw materials in parts by weight: 50 to 60 parts of polyether polyol, 45 to 55 parts of polyester polyol, 100 to 130 parts of diisocyanate, 0.1 to 0.3 part of tin catalyst, 10 to 20 parts of calcium carbonate, 0.55 to 1.65 parts of cross-linking agent, 1 to 3 parts of dispersing agent, 2.56 to 14.56 parts of foaming agent, 0.5 to 0.7 part of coupling agent and 3.56 to 7.56 parts of flame-retardant aid. The preparation method of the flame-retardant slow-rebound memory sponge comprises the steps of mixing, reacting, foaming and the like. The flame-retardant aid is added, is a phosphorus-based flame-retardant and silicon-based flame-retardant synergistic flame retardant and has a plurality of furan ring structures, and the flame-retardant aid is applied to preparation of the slow-rebound sponge, so that the safety performance of the slow-rebound memory sponge is effectively improved, and the application range of the slow-rebound memory sponge is effectively widened.

Description

technical field [0001] The invention relates to the technical field of slow-rebound sponge, in particular to a flame-retardant slow-rebound memory sponge and a preparation method thereof. Background technique [0002] Slow rebound sponge is also called inert sponge, memory foam, low rebound sponge, slow elastic cotton and zero pressure sponge. It was originally developed as a high-tech material designed by the space program. At present, the main types are polyether foam series and polyurethane molding series. [0003] The main product physical properties of the slow rebound sponge, which means mechanical properties: when the slow rebound sponge is deformed by external force, it will not rebound immediately, but delay for a few seconds and slowly restore, and oppress it The shape of the object has a general memory, and the name "slow rebound sponge" comes from this. The reason for the slow rebound performance of the slow rebound sponge is mainly due to its special honeycom...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
IPC IPC(8): C08L75/04C08K5/544C08J9/14
CPCC08J9/0042C08J9/141C08J2375/04C08J2203/14
Inventor 洪海超王洋张少华
Owner 高州市铭顺劳保制品有限公司
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Patsnap Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Patsnap Eureka Blog
Learn More
PatSnap group products