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Super-salt-resistant suspension slickwater resistance reducing agent and preparation method thereof

A technology of slick water and drag reducing agent, which is applied in the direction of chemical instruments and methods, drilling compositions, etc., can solve the problem of the large amount of polymer drag reducing agent and additives, the impossibility of rapid on-site liquid preparation and real-time viscosity, and the impossibility of realizing Saving fresh water resources and environmental protection purposes, etc., to achieve the effects of saving fresh water resources and environmental protection, reducing consumption, and good temperature and shear resistance

Inactive Publication Date: 2021-11-23
西安长庆化工集团有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] The present invention provides a super-salt-resistant suspension slick water drag reducer, whose purpose is to overcome the inability of the slick water system in the prior art to be quickly mixed on site and become viscous in real time, and the amount of polymer drag reducer and additives is large, which cannot be saved. Issues concerning fresh water resources and environmental protection purposes;

Method used

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  • Super-salt-resistant suspension slickwater resistance reducing agent and preparation method thereof
  • Super-salt-resistant suspension slickwater resistance reducing agent and preparation method thereof
  • Super-salt-resistant suspension slickwater resistance reducing agent and preparation method thereof

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preparation example Construction

[0050] A preparation method of a super-salt-resistant suspended slick water drag-reducing agent, comprising the steps of:

[0051] 1) Place the mineral spirits of formula quantity in reaction kettle;

[0052] 2) Raise the temperature in the reactor to 45-50°C, control the stirring speed to 1000-1200r / min, and add the organic bentonite in the formula until the viscosity of the mixture is stable;

[0053] 3) Reduce the temperature in the reactor to 35-40°C, reduce the stirring speed to 500-600r / min, add the formulated amount of dispersant, steering agent, drainage aid, clay stabilizer and oxygen scavenger until fully dissolved;

[0054] 4) Increase the temperature in the reactor to 40°C, increase the stirring speed to 1300-1500r / min, and add the formulated amount of polymer drag reducer powder until the mixture of polymer drag reducer powder and step 3) is evenly mixed.

Embodiment 1

[0056] The polymer drag reducer powder in Example 1 is a zwitterionic polyacrylamide polymer. The zwitterionic polyacrylamide polymer is composed of acrylamide monomers, anionic monomers, cationic monomers, and hydrophobic monomers. Acrylamide The molar ratio of monomer, anionic monomer, cationic monomer and hydrophobic monomer is 8:1:1:0.003, the acrylamide monomer is acrylamide, and the anionic monomer is 2-acrylamide-2-methylpropanesulfonic acid (AMPS), the cationic monomer is dimethyl diallyl ammonium chloride (DMDAAC), and the hydrophobic monomer is a nonionic hydrophobic monomer.

[0057] The preparation method of the polymer drag reducer powder of present embodiment 1 comprises the following steps: acrylamide, dimethyl diallyl ammonium chloride (DMDAAC), 2-acrylamide-2-methylpropanesulfonic acid (AMPS ) with a molar ratio of 8:1:1 to prepare a 30% deionized aqueous solution, add a nonionic hydrophobic monomer with a molar ratio of 8:0.003 to acrylamide, and add ten time...

Embodiment 2

[0092] The polymer drag reducer powder in Example 2 is a zwitterionic polyacrylamide polymer. The zwitterionic polyacrylamide polymer is composed of acrylamide monomers, anionic monomers, cationic monomers and hydrophobic monomers. Acrylamide The molar ratio of monomer, anionic monomer, cationic monomer and hydrophobic monomer is 10:3:1.5:0.001, the acrylamide monomer is acrylamide, the anionic monomer is acrylic acid or methacrylic acid, and the cationic monomer is 2- Methacryloyloxyethyltrimethylammonium chloride or acryloyloxyethyltrimethylammonium chloride, the hydrophobic monomer is a nonionic hydrophobic monomer.

[0093] The preparation method of the polymer drag reducer powder of the present embodiment 2 comprises the following steps: acrylamide, 2-methacryloyloxyethyltrimethylammonium chloride or acryloyloxyethyltrimethylammonium chloride, Acrylic acid or methacrylic acid is prepared into a 30% deionized aqueous solution at a molar ratio of 10:1.5:3, and a nonionic hy...

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Abstract

The invention belongs to the technical field of oil and gas field hydraulic fracturing, and particularly provides a super-salt-resistant suspension slickwater resistance reducing agent and a preparation method thereof. The resistance reducing agent is prepared from polymer resistance reducing agent powder, solvent oil, organic bentonite, a dispersing agent, a diverting agent, a cleanup additive, a clay stabilizer and a deoxidant according to the mass ratio of (30-45):(40-50):(2-4):(2-4):(0.5-2.5):(3-7):(0.5-3.5):(0.5-2.5). According to the invention, the problems of on-site rapid liquid preparation and real-time viscosity change required by a slick water system are solved, the purposes of saving fresh water resources and protecting the environment are achieved by directly preparing the liquid by adopting high-salinity formation water or flowback liquid, and the dosage of a polymer drag reducer and an additive is reduced.

Description

technical field [0001] The invention belongs to the technical field of hydraulic fracturing in oil and gas fields, and in particular relates to a super-salt-resistant suspended slick water drag reducing agent and a preparation method thereof. Background technique [0002] With the depletion of conventional oil and gas resources, unconventional oil and gas resources with low pressure and low permeability have become the key areas of exploration and development. In recent years, shale gas and tight gas have become hot resources for oil and gas development in my country. According to years of field construction experience and theoretical research, using multi-stage and multi-cluster dense cutting volume fracturing technology to shorten the distance between main fractures and increase the dosage of proppant can greatly improve the single well productivity of shale gas or tight gas. In the early stage, this technology requires high-displacement pumping of low-friction fracturing...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C09K8/68C08F220/56C08F226/02C08F220/58C08F220/34C08F220/06C08F212/14
CPCC09K8/68C09K8/882C09K8/885C09K8/90C08F220/56C09K8/608C09K2208/12C08F226/02C08F220/585C08F220/34C08F220/06C08F212/28C08F212/30
Inventor 龙学莉胡军李爱辉李起映丁里黄建宁陈兴官曹璐彤石华强白莹雪张立业万胜勇胡名家赵静尤颖颖
Owner 西安长庆化工集团有限公司