Method for manufacturing photovoltaic matched PVC tile by using weather-resistant reinforced modified filler
A modified and photovoltaic technology, applied in the field of polymer materials, can solve problems affecting service life, accelerating material pulverization, affecting mechanical properties, etc.
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Embodiment 1
[0035] Described weathering aid comprises the following steps to make:
[0036] Step S1: Add chlorobenzene and anhydrous aluminum trichloride into the reaction kettle, stir at a constant speed and raise the temperature to 50°C, add benzoyl chloride dropwise while stirring, then raise the temperature to 100°C, stir at a constant speed and react for 6 hours, after the reaction is completed Pour into ice water with pH=6, stir evenly and let it stand for 4 hours, remove the water layer, wash with water until neutral, and dry to obtain the reactant, then add it to 10% sodium hydroxide solution by mass fraction, add cuprous oxide and Raise the temperature to 220°C, stir at a constant speed and react for 3 hours, purify to obtain intermediate 1, control the molar ratio of chlorobenzene and benzoyl chloride to 1:1, and the consumption of anhydrous aluminum trichloride is 3% of the weight of chlorobenzene, The consumption ratio of reactant, sodium hydroxide solution and cuprous oxide i...
Embodiment 2
[0041] Described weathering aid comprises the following steps to make:
[0042] Step S1: Add chlorobenzene and anhydrous aluminum trichloride into the reaction kettle, stir at a constant speed and raise the temperature to 50°C, add benzoyl chloride dropwise while stirring, then raise the temperature to 100°C, stir at a constant speed and react for 6 hours, after the reaction is completed Pour into ice water with pH=6, stir evenly and let it stand for 4 hours, remove the water layer, wash with water until neutral, and dry to obtain the reactant, then add it to 10% sodium hydroxide solution by mass fraction, add cuprous oxide and Raise the temperature to 220°C, stir at a constant speed and react for 3 hours, purify to obtain intermediate 1, control the molar ratio of chlorobenzene and benzoyl chloride to 1:1, and the consumption of anhydrous aluminum trichloride is 3% of the weight of chlorobenzene, The consumption ratio of reactant, sodium hydroxide solution and cuprous oxide i...
Embodiment 3
[0047] Described weathering aid comprises the following steps to make:
[0048] Step S1: Add chlorobenzene and anhydrous aluminum trichloride into the reaction kettle, stir at a constant speed and raise the temperature to 50°C, add benzoyl chloride dropwise while stirring, then raise the temperature to 100°C, stir at a constant speed and react for 6 hours, after the reaction is completed Pour into ice water with pH=6, stir evenly and let it stand for 4 hours, remove the water layer, wash with water until neutral, and dry to obtain the reactant, then add it to 10% sodium hydroxide solution by mass fraction, add cuprous oxide and Raise the temperature to 220°C, stir at a constant speed and react for 3 hours, purify to obtain intermediate 1, control the molar ratio of chlorobenzene and benzoyl chloride to 1:1, and the consumption of anhydrous aluminum trichloride is 3% of the weight of chlorobenzene, The consumption ratio of reactant, sodium hydroxide solution and cuprous oxide i...
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